• Title/Summary/Keyword: Quenching technique

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PSP Pressure Field Visualization of an Oblique Impinging Jet (경사충돌제트의 PSP 압력장 가시화)

  • Kang Jong Hoon;Lee Sang Joon
    • 한국가시화정보학회:학술대회논문집
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    • 2004.11a
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    • pp.10-13
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    • 2004
  • The PSP(pressure sensitive paint) technique has recently received a large attention as a new revolutionary optical method to measure absolute pressure distribution on a model surface. The PSP technique can be applied to quantitatively investigate flow structure using a CCD camera and image processing technique. In the static calibration, the luminescent intensity of PSP coatings was measured from 0kPa to 11kPa with 0.5, 1, 2kPa increments. In this study, the low-pressure PSP technique was applied to an oblique impinging jet to measure pressure field variations on the impingement plate with varying angle of an oblique jet. The flow structure over the impingement plate was visualized using a surface tracing method. As a result, the detail pressure field distributions of the oblique low-speed impinging jet were visualized effectively using the PSP technique.

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Development of Pressure Sensitive Paint (PSP) Technique for Low-speed Flows and Its Application (저속 유동용 Pressure Sensitive Paint 기술개발과 응용)

  • Kang, Jong-Hun;Lee, Sang-Joon
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.688-693
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    • 2003
  • The PSP technique has been used to measure pressure distribution on a model surface quantitatively. The objective of this study is to develop PSP technique which can be applied to low-speed flows. Four different PSP formulations including two porphyrins (PtOEP and PtTFPP) and two polymers (Poly(TMSP) and RTV-118) were tested and the performance of each combination was checked. In the static calibration, the luminescent intensity of the PSP coatings was measured from 0kPa to 11kPa with 0.5, 1, 2kPa increments. Among 4 PSP formulations tested, the combination of PtOEP and RTV-118 shows the best performance. The PSP technique was applied to an oblique impinging jet to measure the pressure field distribution on the impinging plate.

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Metallurgical Characteristics and Manufacturing Techniques of Ring-Pommel Swords Excavated from Ancient Tombs in Hadae, Ulsan (울산 하대고분 출토 민고리자루칼의 재질 특성과 환두부 제작 방법)

  • Jo, Ha Nui;Kim, Han Seul;You, Ha Rim;Lee, Jae Sung
    • Journal of Conservation Science
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    • v.36 no.3
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    • pp.197-212
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    • 2020
  • This study analyzed the microstructure of ring-pommel swords, excavated from Ancient Tombs, Hadae, Ulsan and examined their production technique, using non-destructive testing and a metallurgical method. The results confirmed that the five ring-pommel swords, unearthed in Ancient Tombs, Hadae, Ulsan, as identified by radiographic non-destructive testing, had been solely manufactured using iron, through forging based on the single-piece technique. Furthermore, these results were compared with previous studies, and the manufacturing techniques of single-piece ring-pommel swords were categorized into three types: pure iron - changing the shape, pure iron - changing the shape - carburization, and steel - changing the shape - quenching. The ring-pommels of four swords had around 0.7% of carbon content, which is as much as for eutectoid steel and higher than for other parts of these swords, such as the backs of their blades and handles. The weapon function of a small ring-pommel sword, under 60cm in length, was maximized by quenching focusing on its blade. Conversely, the martensite quenching structure was not observed in four ring-pommel swords shorter than 75cm. In other words, the same types of single-piece ring-pommel swords(late in 2C~early in 4C) were unearthed from Ancient Tombs, Hadae, and the group who has manufactured these swords is presumed to have limited their effectiveness, functionally depending on purposes, through an iron-making process and heat-treatment techniques.

A Study on the Properties of Laser-Welded Boron Steel for Hot Stamping According to the Heat-Treatment Conditions (핫스탬핑용 보론 강판의 레이저 용접부에 대한 열처리 조건에 따른 특성 연구)

  • Hwang, Seok-Hwan;Nam, Ki-Woo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.3
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    • pp.319-324
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    • 2012
  • The hot-stamping technique is a forming method for manufacturing high-strength parts, in which the part is cooled rapidly after press forming above the austenite transformation temperature. Boron steel, which contains a very small amount of boron, is one of the materials used for hot stamping. The purpose of this study is to investigate the microstructure and mechanical properties according to the heat-treatment conditions. Die-quenching from various temperatures was conducted for different elapsed heat-treatment times. Laser-welded boron steel after quenching has a tensile strength of 1454 MPa and an elongation of 6 %. It has 94 % of the tensile strength of the base metal (1522 MPa). These properties can provide practical information for the use of boron steels for hot stamping.

The Distribution of Barbiturates in Model Membranes of Total Lipids and Total Phospholipids Extracted from Brain Membranes

  • Park, Chang-Sik;Lee, Seong-Moon;Chung, In-Kyo;Kim, Jin-Bom;Son, Woo-Sung;Jang, Hye-Ock;Yun, Il
    • BMB Reports
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    • v.33 no.3
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    • pp.221-227
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    • 2000
  • The distribution of barbiturates in the model membranes of total lipids (SPMVTL) and total phospholipids (SPMVPL) extracted from synaptosomal plasma membrane vesicles was determined by employing a fluorescent probe technique. The two fluorescent probes 2-(9-anthroyl)stearic acid and 12-(9-anthroyl)stearic acid were utilized as probes for the surface and the hydrocarbon interior of the outer monolayer of the SPMVTL and SPMVPL, respectively. The Stern-Volmer equation of fluorescent quenching was modified to calculate the relative distribution. The analysis of preferential quenching of these probes by barbiturates indicates that pentobarbital, hexobarbital, amobarbital and phenobarbital are predominantly distributed on the surface area, while thiopental sodium has an accessibility to the hydrocarbon interior of the outer monolayer of the SPMVTL and SPMVPL. From these results, it is strongly suggested that the more effective penetration into the hydrocarbon interior of the outer monolayer of the membrane lipid bilayer could result in a higher general anesthetic activity.

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An Optical Quenching and Efficiency of Laser for the Virtual Display System (허상 디스플레이에 적용되는 레이저 다이오드의 출력 효율과 파장 변이에 대한 연구)

  • Chi, Yongseok
    • Journal of the Institute of Electronics and Information Engineers
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    • v.53 no.9
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    • pp.129-134
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    • 2016
  • This paper studies the high frequency PWM (pulse width modulation) driving technique to increase an optical efficiency and to prevent an optical color quenching of blue laser for head up display on vehicles using digital micro mirror device (DMD) panel and yellow phosphor wheel. The proposed approach adaptively drives the current pulse width modulated signals of high optical power of blue laser to increase the lifetime and to decrease the stem temperature of laser. This method stabilizes the temperature of laser according to the driving environment and the forward current capacity. By the proposed method, the brightness of blue laser is improved by about 37% compared to the continuous waveform current driving method.

Mechanical Properties and Formability of TWB Boron Steel (TWB 보론강의 기계적 특성 및 성형성)

  • Nam, K.W.;Hwang, S.H.;Kim, D.Y.;Lee, M.Y.;Lee, S.M.
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.10
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    • pp.1221-1226
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    • 2012
  • The hot-stamping technique is a forming method used for manufacturing high-strength parts, in which a part is cooled rapidly after press forming above the austenite transformation temperature. Boron steel, which contains a very small amount of boron, is one of the materials used for hot stamping. The purpose of this study is to investigate the mechanical properties of boron steel according to the heat-treatment conditions and the formability by using an Erichsen cupping test. Die quenching from various temperatures was conducted for different elapsed heat-treatment times. Laser-welded boron steel after quenching at 1173 K-0 s has a tensile strength of 1203 MPa. This is 79% of the tensile strength of the base metal (1522 MPa). The formability of boron steel was not significantly different from that at the mold temperature. However, it decreased with increasing forming speed. These properties provide practical information for the use of boron steels for hot stamping.

Interaction of ct-DNA with 2,4-Dihydroxy Salophen

  • Azani, Mohammad-Reza;Hassanpour, Azin;Bordbar, Abdol-Khalegh;Mirkhani, Valiollah
    • Bulletin of the Korean Chemical Society
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    • v.30 no.9
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    • pp.1973-1977
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    • 2009
  • In the present study, at first, 2,4-Dihydroxy Salophen (2,4-DHS), has been synthesized by combination of 1, 2-diaminobenzene and 2,4-dihydroxybenzaldehyde in a solvent system. This ligand containing meta-quinone functional groups were characterized using UV-Vis and IR spectroscopies. Subsequently, the interaction between native calf thymus deoxyribonucleic acid (ct-DNA) and 2,4-DHS, was investigated in 10 mM Tris/HCl buffer solution, pH 7.2, using UV-visible absorption and fluorescence spectroscopies, thermal denaturation technique and viscosity measurements. From spectrophotometric titration experiments, the binding constant of 2,4-DHS with ct-DNA was found to be (1.1 ${\pm}\;0.2)\;{\times}\;10^4\;M^{-1}.$ The fluorescence study represents the quenching effect of 2,4-DHS on bound ethidium bromide to DNA. The quenching process obeys linear Stern-Volmer equation in extended range of 2,4-DHS concentration. Thermal denaturation experiments represent the increasing of melting temperature of DNA (about 3.5 ${^{\circ}C}$) due to binding of 2,4-DHS. These results are consistent with a binding mode dominated by interactions with the groove of ct-DNA.

Nanoplasmonic Spectroscopic Imaging and Molecular Probes

  • Choe, Yeon-Ho
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.85-85
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    • 2013
  • Label-free, sensitive and selective detection methods with high spatial resolution are critically required for future applications in chemical sensor, biological sensor, and nanospectroscopic imaging. Here I describe the development of Plasmon Resonance Energy Transfer (PRET)-based molecular imaging in living cells as the first demonstration of intracellular imaging with PRET-based nanospectroscopy. In-vivo PRET imaging relied on the overlap between plasmon resonance frequency of gold nanoplasmonic probe (GNP) and absorption peak frequencies of conjugated molecules, which leads to create 'quantized quenching dips' in Rayleigh scattering spectrum of GNP. The position of these dips exactly matched with the absorption peaks of target molecules. As another innovative application of PRET, I present a highly selective and sensitive detection of metal ions by creating conjugated metal-ligand complexes on a single GNP. In addition to conferring high spatial resolution due to the small size of the metal ion probes (50 nm in diameter), this method is 100 to 1,000 folds more sensitive than organic reporter-based methods. Moreover, this technique achieves high selectivity due to the selective formation of Cu2+complexes and selective resonant quenching of GNP by the conjugated complexes. Since many metal ion ligand complexes generate new absorption peak due to the d-d transition in the metal ligand complex when a specific metal ion is inserted into the complex, we can match with the scattering frequency of nanoplasmonic metal ligand systems and the new absorption peak.

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Interaction of Bilobalide and Ginkgolides B with Bovine Serum Albumin: A Fluorescence Quenching Study

  • Chen, Yan;Wang, Ruijun;Wang, Shusheng;Yang, Yi;Li, Shaofei;Kai, Guiqing
    • Bulletin of the Korean Chemical Society
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    • v.32 no.9
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    • pp.3261-3266
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    • 2011
  • The interaction of bilobalide (BB) and ginkgolides B (GB) with bovine serum albumin (BSA) was investigated by fluorescent technique and UV/vis absorption spectroscopy. The results showed that BB and GB could intensively quench the fluorescence of BSA through a static quenching procedure. The binding constants (Ka) and the average binding distance between the donor (BSA) and the acceptor (ginkgolides) were obtained ($r_{BB}$ = 5.33 nm and $r_{GB}$ = 4.20 nm) by the theory of non-radiation energy transfer, and then the thermodynamic parameters such as ${\Delta}S^0$ (0.17-0.32 kJ/mol), ${\Delta}G^0$ (-20.76 ~ -17.79 kJ/mol) and ${\Delta}H^0$ (32.47-76.52 kJ/mol) could be calculated, respectively. All these results revealed that the interaction of BB and GB with BSA were driven mainly by hydrophobie force. The synchronous fluorescence spectroscopy was applied to examine the effect of two ginkgolides on the configuration of BSA. The configuration alteration of BSA could be induced by the hydrophobicitv environment of tyrosine with the increase of the drug concentration.