• Journal of the Korean Society of Manufacturing Process Engineers
• /
• v.17 no.4
• /
• pp.76-82
• /
• 2018

3D formed Electrical Discharge Machining (EDM) and hole EDM were conducted for die and mold manufacturing with electrodes which were made by mechanical machining and wire EDM. It is difficult to machine the hardened material after heat treatment and quenching with traditional machining. The only method of machining hardened material is die-sinking EDM. In this research, hole EDM was conducted for heat-treated cold-worked tool steel (SKD11) for use as a die material. The EDM surfaces were analyzed by pulse-on time and peak current of EDM current, according to the machining conditions of EDM. The EDM surface profiles were affected by the peak current. The contribution of each factor is peak current (91.63%) and pulse-on time (0.93%). The best surface roughness was obtained with a $130{\mu}s$ pulse-on time and a 14.2 A peak current. With uniform EDM processing, the surface deteriorated with increasing pulse-on time and peak current. The thickness of the solidified layer induced by EDM was increased as the peak current, crater shapes, and erupted shapes of EDM surfaces were increased. Therefore, microcracking gaps induced by surface tension were increased.

• Journal of Surface Science and Engineering
• /
• v.47 no.4
• /
• pp.192-197
• /
• 2014

Red-emitting nitride phosphors recently attracted considerable attention because of their high thermal stability and high color rendering index properties. For excellent phosphor of white light-emitting-diode, ternary nitride phosphor of $Sr/SmSi_5N_8:Eu^{2+}$ with different $Eu^{2+}$ ion concentration were synthesized by solid state reaction method. In this work, red-emitting nitride $Sr/SmSi_5N_8:Eu^{2+}$ phosphor was successfully synthesized by using multi-step high frequency induction heat treatment. The effects of molar ratio of component and experimental conditions on luminescence property of prepared phosphors have been investigated. The structure and luminescence properties of prepared $Sr/SmSi_5N_8:Eu^{2+}$ phosphors were investigated by XRD and photoluminescence spectroscopy. The excitation spectra of $Sr/SmSi_5N_8:Eu^{2+}$ phosphors indicated broad excitation wavelength range of 300 - 550 nm, namely from UV to visible area with distinct enhanced emission peaks. With an increase of $Eu^{2+}$ ion concentration, the peak position of emission in spectra was red-shifted from 613 to 671 nm. After via multi-step heat treatment, prepared phosphor showed excellent luminescence properties, such as high emission intensity and low thermal quenching, better than commercial phosphor of $Y_3Al_5O_{12}:Ce^{3+}$. Using $Eu_2O_3$ as a raw material for $Eu^{2+}$ dopant with nitrogen gas flowing instead of using commercial EuN chemical for $Sr/SmSi_5N_8:Eu^{2+}$ synthesis is one of characteristic of this work.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.41 no.9
• /
• pp.597-603
• /
• 2017

In this study, experiments were conducted on the MFB(minimum film boiling) point of highly heated vertical metal rod quenched in aqueous surfactant solution at various temperature conditions. The aqueous Triton X-100 solution(100 wppm) and pure water were used as the liquid pool. Their temperatures ranged from $77^{\circ}C$ to $100^{\circ}C$. A stainless steel vertical rod of initial center temperature of $500^{\circ}C$ was used as a test specimen. In both liquid pools, as the liquid temperature decreased, the time to reach the MFB point decreased with a parallel increase in the temperature and heat flux of the MFB point. However, over the whole present temperature range, in the aqueous Triton X-100 solution, the time to reach the MFB point was longer, while the temperature and heat flux of the MFB point were reduced when compared with pure water. Based on the present experimental data, this study proposed the empirical correlations to predict the MFB temperature of a high temperature vertical metal rod in pure water and in aqueous Triton X-100 solution.

• Korean Journal of Agricultural Science
• /
• v.43 no.3
• /
• pp.441-449
• /
• 2016

Agricultural tractors are designed using the empirical method due to the difficulty of measuring precise load cycles under various working conditions and soil types. Especially, directly drives various tractor implements, the power take off (PTO) gear. Therefore, alternative design methods using gear design software are needed for the optimal design of tractors. The objective of this study is to simulate fatigue life of the PTO gear according to the operating point of the tractor engine. The PTO gear was made with SCr415 alloy steel with carburizing and quenching treatments. The fatigue life of the PTO gear was simulated by using bending and contact stress according to the torque of the load levels. The PTO gear simulation was conducted by the KISSsoft commercial software for gear analysis. Bending and contact stress were calculated by the ISO 6336:2006 Method A and B. The simulation of fatigue life was calculated by the Miner's cumulative damage law. The total fatigue life of tractors can be estimated to 3,420 hours; thus, 3,420 hours of fatigue life were used in the simulation of the PTO gear of tractors. The main simulation results showed that the maximum fatigue life of the PTO gear was infinite fatigue life at maximum engine power. Minimum fatigue life of the PTO gear was 19.61 hours at 70% of the maximum engine power. Fatigue life of the PTO gear changed according to load of tractor. Therefore, tractor work data is needed for optimal design of the PTO gear.

• Korean Journal of Materials Research
• /
• v.24 no.7
• /
• pp.351-356
• /
• 2014

A spherical $Sr_4Al_{14}O_{25}:Eu^{2+}$ phosphor for use in white-light-emitting diodes was synthesized using a liquid-state reaction with two precipitation stages. For the formation of phosphor from a precursor, the calcination temperature was $1,100^{\circ}C$. The particle morphology of the phosphor was changed by controlling the processing conditions. The synthesized phosphor particles were spherical with a narrow size-distribution and had mono-dispersity. Upon excitation at 395 nm, the phosphor exhibited an emission band centered at 497 nm, corresponding to the $4f^65d{\rightarrow}4f^7$ electronic transitions of $Eu^{2+}$. The critical quenching-concentration of $Eu^{2+}$ in the synthesized $Sr_4Al_{14}O_{25}:Eu^{2+}$ phosphor was 5 mol%. A phosphor-converted LED was fabricated by the combination of the optimized spherical phosphor and a near-UV 390 nm LED chip. When this pc-LED was operated under various forward-bias currents at room temperature, the pc-LED exhibited a bright blue-green emission band, and high color-stability against changes in input power. Accordingly, the prepared spherical phosphor appears to be an excellent candidate for white LED applications.

• Journal of Biomedical Engineering Research
• /
• v.22 no.6
• /
• pp.511-518
• /
• 2001

In vitro corrosion resistance of the commercially used 76.5wt.%Pd-17.6%Cu-7.2%Ga and 77.3%Pd-6.0%Ga dental Prostheses high-Palladium system alloys in cast, degassing and porcelain-firing heat treatment conditions were evaluated by the potentiodynamic polarization technique in the de-aerated 0.9%NaCl and a modified Fusayama electrolyte. From the corrosion rate experimental results, we found that there is a small difference in the corrosion resistance depending on the microstructure. However. it was so small that there is no significant problem as a dental material. The 77.3%Pd-6.0%Ga showed better corrosion resistance than the 76.5%Pd-11.6%Cu-7.2%Ga dental Prostheses high-palladium system alloys. These experimental observations in 76.5%Pd-11.6%Cu-7.2%Ga alleys are mainly due to a rapid quenching and Cu in the alloy which accelerate the eutectic reaction with a segregation and Precipitates in the microstructure. On the ocher hand, 77.3%Pd-6.0%Ga alloys, which are solid-solution matrix, show much better col·lesion resistance compared with that of 76.5%Pd-11.6%Cu-7.2%Ga alloys.

• Journal of the Korean Society of Food Science and Nutrition
• /
• v.31 no.3
• /
• pp.399-404
• /
• 2002

The fermented fruit and vegetable mixed broth was prepared by using bacteriocin-producing lactic acid bacteria to evaluate the possibility of developing isotonic beverage with anticariogenic activity. Optimum conditions were also established to produce bacteriocin by a mixed culture system consisting of Lc. lactis and Leu. mesenteroides in a fruit and vegetable mixture. Production of bacteriocin was not observed when both strains were simultaneously innoculated, but pH adjustment of the broth fermented by Leu. mesenteroides to nearneutral pH stimulated the production of bacteriocin by Lc. lactis. The concentration of sodium of the fermented broth was higher than those of commercial products. Color change of the fermented broth was not observed during storage. The fermented broth showed strong inhibitory effect against Streptococcus mutans which is an oral inhabitant with a cariogenic activity. Bacteriocin activity in the fermented broth was retained very stable for 4 weeks at 4$\^{C}$. The results indicated that bacteriocin-producing lactic acid bacteria can be used for the preparation of a Korean style thirst-quenching beverage containing bacteriocin.

• Nuclear Engineering and Technology
• /
• v.45 no.3
• /
• pp.323-334
• /
• 2013

During a hypothetical core-disruptive accident (CDA) in a sodium-cooled fast reactor (SFR), degraded core materials can form roughly conically-shaped debris beds over the core-support structure and/or in the lower inlet plenum of the reactor vessel from rapid quenching and fragmentation of the core material pool. However, coolant boiling may ultimately lead to leveling of the debris bed, which is crucial to the relocation of the molten core and heat-removal capability of the debris bed. To clarify the mechanisms underlying this self-leveling behavior, a large number of experiments were performed within a variety of conditions in recent years, under the constructive collaboration between the Japan Atomic Energy Agency (JAEA) and Kyushu University (Japan). The present contribution synthesizes and gives detailed comparative analyses of those experiments. Effects of various experimental parameters that may have potential influence on the leveling process, such as boiling mode, particle size, particle density, particle shape, bubbling rate, water depth and column geometry, were investigated, thus giving a large palette of favorable data for the better understanding of CDAs, and improved verifications of computer models developed in advanced fast reactor safety analysis codes.

• Korean Journal of Pharmacognosy
• /
• v.45 no.3
• /
• pp.227-232
• /
• 2014

The seed of Vigna angularis (Ohwi) Ohwi & Ohashi (= Phaseolus angularis W. F. Wight, Leguminosae) is one of well-known folk foodstuffs in Korea, China and Japan. In the course of screening for antioxidants from natural plants in Korea by measuring the radical scavenging effect on 1,1-diphenyl-2-picrylhydrazyl (DPPH) a methanol extract of the seeds of V. angularis were found to show a potent antioxidant activity. And the ethyl acetate soluble fraction of V. angularis (VAEA) showed the most potent DPPH radical scavenging and superoxide quenching activities. To reveal the effect of antioxidant activities of VAEA, we tested the thermal and oxidative stress tolerances, activities of SOD and catalase, and intracellular ROS level in Caenorhabditis elegans. Consequently, VAEA-fed worms lived longer than control worms under the thermal and oxidative stress conditions. And VAEA elevated SOD and catalase activities of worms, and reduced intracellular ROS accumulation in a dose-dependent manner.

• Journal of the Korean Society for Heat Treatment
• /
• v.18 no.4
• /
• pp.247-255
• /
• 2005

Although heat treatment is a process of great technological importance in order to obtain desired mechanical properties such as hardness, the process was required a tedious and expensive experimentation to specify the process parameters. Consequently, the availability of reliable and efficient numerical simulation program would enable easy specification of process parameters to achieve desired microstructure and mechanical properties without defects like crack and distortion. In present work, the developed numerical simulation program could predict distributions of microstructure and thermal stress in steels under different cooling conditions. The computer program is based on the finite difference method for temperature analysis and microstructural changes and the finite element method for thermal stress analysis. Multi-phase decomposition model was used for description of diffusional austenite decompositions in low alloy steels during cooling after austenitization. The model predicts the progress of ferrite, pearlite, and bainite transformations simultaneously during quenching and estimates the amount of martensite also by using Koistinen and Marburger equation. To verify the developed program, the calculated results are compared with experimental ones of casting product. Based on these results, newly designed heat treatment process is proposed and it was proved to be effective for industry.