• Title/Summary/Keyword: Quantitative Analysis

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Quantitative analysis of 5-HMF produced from fructose (과당에서 전환된 5-HMF(5-hydroxymethylfurfural)의 정량적 분석)

  • Sim, Jaehoon;Shin, Soo-Jeong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.1
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    • pp.27-34
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    • 2013
  • Quantitative analysis of 5-hydroxymethylfufural (5-HMF) conversion from fructose by dehydration and rearrangement was investigated by $^1H$-NMR spectroscopic method. Fructose was converted to 5-HMF in dimethylsulfoxide (DMSO)-$d^6$ or acidic deuterium hydroxide at controlled reaction temperature and time. With addition of internal standards (biphenyl for DMSO-$d^6$ solvent, and 2,5-dihydroxybenzoic acid for deuterium oxide solvent), conversion from fructose to 5-HMF was analyzed by $^1H$-NMR spectroscopy. Quantitative analysis was run by comparison with peak area integration between of 5-HMF and internal standard. In DMSO solvent, 5-HMF was stable end product but part of 5-HMF was converted to formic and levulinic acid at acidic aqueous medium.

Challenges for QTL Analysis in Crops

  • Long, Yan;Zhang, Chunyu;Meng, Jinling
    • Journal of Crop Science and Biotechnology
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    • v.11 no.1
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    • pp.7-12
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    • 2008
  • Quantitative trait loci, a genetic concept for explaining the inheritance of non-Mendelian traits in 1940s, have been realized as particular fragments of chromosome even unique genes in most crops in 21st century. However, only very a small portion of QTL has been screened out by geneticists comparing to a great number of genes underneath the quantitative traits. These identified QTL even have been seldom used into breeding program because crop breeders may not find the QTL in their breeding populations in their field station. Several key points will be proposed to meet the challenges of QTL analysis today: a fine mapping population and the related reference genetic map, QTL evaluation in multiple environments, recognizing real QTL with small genetic effect, map integration.

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Shearography in Tire Industry (타이어 검사를 위한 Shearogrpahy의 응용)

  • Kim, Koung-Suk;Kang, Ki-Soo;Yoon, Seung-Chul;Yang, Seung-Phil
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.298-303
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    • 2003
  • In recent years, shearogrpahy has significantly improved capabilities in the areas of unbond and separation detection in tires. Although shearography has many advantages for qualitative evaluation, the technique remains the problem of quantitative analysis of inside defects, because shearography needs several effective factors including the amount of shearing, shearing direction and induced load, which exist as barrier for the quantitative analysis of inside defects. Since the factors are highly dependent on inspectors skill and also affect the in-situ workability. The factors were optimized and the size of cracks inside of pipeline and tire has been quantitatively determined.

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Isolation and Quantitative Analysis of Kalopanax-Saponin B from Kalopanacis Cortex (해동피로부터 Kalopanax-saponin B의 분리 및 함량분석)

  • Hong, Seong-Su;Hwang, Ji-Sang;Huh, Jae-Doo;Lee, Kyong-Soon;Ro, Jai-Seup
    • Korean Journal of Pharmacognosy
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    • v.33 no.4 s.131
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    • pp.277-284
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    • 2002
  • For the quality control of Kalopanacis Cortex, saponin compound, kalopanax-saponin B was isolated from the MeOH extract of Kalopanacis Cortex, and identified by the spectroscopic evidences. A quantitative analysis of kalopanaxsapo-nits B using HPLC method showed that the average contents was $1.010{\pm}0.212%$, respectively, in 22 samples collected through-out the regions of Korea.

Development and Application of Image Analysis Program for Investigation of Pore Characteristics in Transverse Surface of Hardwoods

  • Kwon, Oh-Kyung;Lee, Phil-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.26 no.2
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    • pp.29-37
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    • 1998
  • An image analysis program with the function of measuring various quantitative characteristics in the transverse surface of wood was developed using Delphi 2.0. Data on pore characteristics (conditions for image processing, proportion of pores in relationship to other elements, tangential diameter, area, tangential and radial diameter, x and y coordinates of pore center, and geometric coefficients) were saved in text file format. In addition, the pore area histogram in the tangential and radial directions was saved as a BMP (bitmap) type file. Analyses indicated that quantitative characteristics such as the relative radial distribution of pores in a growth ring, pore tangential area histogram, and proportion of pore in lumen area appear to be useful in separating four diffuse-porous woods and four ring-porous woods on the species level.

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Quantitative Evaluation of Fabric Drape Using Image Analysis (화상처리기법을 활용한 천의 드레이프성의 정량적 평가방법)

  • Park, Chang-Kyu
    • Fashion & Textile Research Journal
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    • v.4 no.3
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    • pp.284-288
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    • 2002
  • In this research, a new quantitative fabric drape evaluation system has been developed using image processing technology. The purpose of this research is to get the more detailed information of fabric drapability quantitatively from digital images captured with a digital camera generally commercialized. The shape parameters of a 3-dimensional geometric drape model were defined as the number of nodes, frequency and amplitude. Also, various statistical information of drape shapes can be obtained using image processing technology and frequency analysis as well as traditional drape coefficients. Hardware system to capture drape images is simply composed of three parts including a digital USB (Universal Serial Bus) camera, a frame cover and a stand for camera to attach to traditional drape tester. The evaluation software coded with the MS Visual C++ is operated under the MS windows 9x above.

- Development of a Safety Assessment System Model in the Manufacturing Industry - (제조업에 대한 안전성평가시스템 모델 구축에 관한 연구)

  • 성호경
    • Journal of the Korea Safety Management & Science
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    • v.5 no.2
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    • pp.11-26
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    • 2003
  • While a number of Korean companies have undergone ceaseless restructuring to survive today's rapidly changing global economy, the brick and mortar industry has been exerting their efforts to enhance the productivity through the development of new products, quality improvement, cost reduction measures. At present, various risk-evaluation measures have been taken in the fields at the discretion of an enterpriser, though, the effective methods enabling quantitative analysis are insufficient. Accordingly, this study is intended to contribute to the synthetic safety manage -ment in the factory fields and to suggest the quantitative -risk-analysis system by introducing such safety-estimation steps as assortment of processes, pre-assessment of risk factors, decision of risks, counter measures against studied risks, establishment of remedies.

Quantitative Analysis of Actigraphy in Sleep Research (수면연구를 위한 액티그라피 정량분석 방법론)

  • Kim, Jong Won
    • Sleep Medicine and Psychophysiology
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    • v.23 no.1
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    • pp.10-15
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    • 2016
  • Since its development in the early 70s, actigraphy has been widely used in sleep research and clinical sleep medicine as an assessment tool of sleep and sleep-wake cycles. The validation and reliability of actigraphic measures have been reasonably examined in healthy normal individuals with good sleep patterns. Recent literature suggests that the use of actigraphy could be further extended to monitor insomnia and circadian sleep-wake disturbances, and detect sleep changes associated with drug treatments and non-pharmacologic interventions, although it is generally recommended to use complementary assessments such as sleep diaries and overnight polysomnography when possible. The development of actigraphy includes its improved hardware sensors for better detection of movements and advanced algorithms to score sleep and wake epochs. In this paper, we briefly review the quantitative analysis methods of actigraphy and its potential applications in sleep research.

The Quantitative and Qualitative Plans of an Urban Park In the Landscape Ecological View

  • Ryu Yeun-Soo;Lee Kee-Cheol;Ra Jung-Hwa
    • Journal of the Korean Institute of Landscape Architecture International Edition
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    • no.2
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    • pp.1-8
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    • 2004
  • The purpose of this study is to carry out the quantitative and qualitative analysis of an urban park in the landscape ecological view and to provide the important basic data in the urban development process. The results of this study are as follows. First, in the case of disposition distance analysis in quantitative plans, very necessary regions of the children park are turned out to be 24 sites, of the neighboring park are turned out to be 30 sites, and walking park are turned out to be 22 sites. Second, in the case of undevelopment neighborhood park analysis, priority orders are Daebong Park, Suseong Park Third, in the case of area, shape, and isolation in qualitative plans, interior area of Bummul park is larger than that of Chimsan park and isolation of Bummul park higher than that of Chimmsan.

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Analysis of Drugs and Chemicals by Infrared Absorption Spectrophotometry(II) Quantitative Analysis of Sulfamethoxydiazine and Sulfamethoxypyridazine in Pharmaceutical Preparations. (Infrared spectrophotometry에 의한 의약품의 분석연구 (II) 적외선흡수 Spectra에 의한 Sulfamethoxydiazine 및 Sulfamethoxy-pyridazine의 정량분석)

  • 옥치완;권영훈
    • YAKHAK HOEJI
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    • v.13 no.2_3
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    • pp.51-56
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    • 1969
  • In quantitative analysis of sulfonamide drugs by means of infrared Spectrophotometry, the author tried to analyse Sulfamethoxydiazine and Sulfamethoxypyridazine in their Pharmaceutical Preparations. By the survey of infrared absorption spectra of Sulfamethoxydiazine and Sulfamethoxypyridazine. We found quantitative properties at the peaks of wave number 1150 cm$^{-1}$ (Sulfamethoxydiazine) and 1090 cm$^{-1}$ (Sulfamethoxypyridazine) in the spectra. These peaks obey Beer's Law in a range of 50-150 ug for Sulfamethoxydiazine and 70-350 ${\mu}$g for Sulfamethoxypyridazine in 300 mg KBr disc. By this method, Sulfamethoxydiazine and Sulfamethoxypyridazine could be analyzed less than 2% error.

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