• Title/Summary/Keyword: Pure Nickel

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COMPARISON OF THE BOND STRENGTH OF CERAMICS FUSED TO TITANIUM AND Ni-Cr ALLOY (티타늄과 니켈-크롬 합금의 도재결합강도 비교)

  • Park Sae-Young;Jeon Young-Chan;Jeong Chang-Mo
    • The Journal of Korean Academy of Prosthodontics
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    • v.41 no.1
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    • pp.89-98
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    • 2003
  • Titanium requires special ceramic system for veneering. Low fusing dental ceramics with coefficients of thermal expansion matching that of titanium have been developed. The purpose of this study was determine the bond strengths between cast and noncast pure titanium and two commercial titanium porcelains, and to compare the results with a conventional nickel-chromium alloy-ceramic system. The bond strengths were determined using a 3-point flexure test. Three-point flexure specimens $25{\times}3{\times}0.5mm$ were prepared After removal of ${\alpha}-case$ layer, they were veneered with $8{\times}3{\times}1mm$ of ceramics at the center of the bar. Specimens were tested in a universal testing machine. Within the limits of this study, the following conclusions were drawn: 1. The bond strengths between pure titanium and two commercial porcelains exceeded th lower limit of the bonding strength value in ISO 9693(25MPa). 2. There was no significant difference between cast and noncast titanium-porcelain bonds. 3. There was no significant difference between two commercial titanium porcelains. 4. The bond strengths of the titanium-porcelain systems ranged from 73% to 79% of that of the Ni-Cr-conventional porcelain system.

Production of Titanium Powder by Electronically Mediated Reaction (EMR) (도전체 매개반응(EMR)법에 의한 Ti 분말 제조)

  • Park Il;Chu Yong Ho;Lee Chul Ro;Lee Oh Yeon
    • Korean Journal of Materials Research
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    • v.14 no.12
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    • pp.857-862
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    • 2004
  • Production of titanium powder directly from tantalum oxides ($TiO_2$) pellet through an electronically mediated reaction (EMR) by calciothermic reduction has been investigated. Feed material ($TiO_2\;pellet$) and reductant (Ca-Ni alloy) were charged into electronically isolated locations in a molten calcium chloride ($CaCl_2$) bath at $950^{\circ}C$. The current flow through an external circuit between the feed (cathode) and reductant (anode) locations was monitored during the reduction of $TiO_2$. The current approximately 3.2A was measured during the reaction in the external circuit connecting cathode and anode location. After the reduction experiment, pure titanium powder with low nickel content was obtained even though Ca-Ni alloy was used as a reductant. These results demonstrate that titanium powder can be produced without direct physical contact between the feed and reductant. In certain experimental conditions, pure titanium powder with approximately $99.5\;mass\%$ purity was successfully obtained.

Sintering Behavior of Ag-Ni Electrode Powder with Core-shell Structure

  • Kim, Kyung Ho;Koo, Jun-Mo;Ryu, Sung-Soo;Yoon, Sang Hun;Han, Yoon Soo
    • Journal of the Korean institute of surface engineering
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    • v.49 no.6
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    • pp.507-512
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    • 2016
  • Expensive silver powder is used to form electrodes in most IT equipment, and recently, many attempts have been made to lower manufacturing costs by developing powders with Ag-Ni or Ag-Cu core-shell structures. This study examined the sintering behavior of Ag-Ni electrode powder with a core-shell structure for silicon solar cell with high energy efficiency. The electrode powder was found to have a surface similar to pure Ag powder, and cross-sectional analysis revealed that Ag was uniformly coated on Ni powder. Each electrode was formed by sintering in the range of $500^{\circ}C$ to $800^{\circ}C$, and the specimen sintered at $600^{\circ}C$ had the lowest sheet resistance of $5.5m{\Omega}/{\Box}$, which is about two times greater than that of pure Ag. The microstructures of electrodes formed at varying sintering temperatures were examined to determine why sheet resistance showed a minimum value at $600^{\circ}C$. The electrode formed at $600^{\circ}C$ had the best Ag connectivity, and thus provided a better path for the flow of electrons.

Creep Life Prediction for Udimet 720 Material Using the Initial Strain Method (ISM)

  • Kong, Yu-Sik;Yoon, Han-Ki;Oh, Sae-Kyoo
    • Journal of Mechanical Science and Technology
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    • v.17 no.4
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    • pp.469-476
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    • 2003
  • Despite of considerable research results or uniaxial tension creep available for superalloys, few studies have been made on high temperature creep using the Initial Stram Method (ISM) In this paper, the real-time prediction of high temperature creep strength and creep lift for the nickel-based superalloy Udimet 720 (high-temperature and high-pressure gas turbine engine materials) was performed on round-bar type specimens under pure static load at the temperatures of 538$^{\circ}C$. 649$^{\circ}C$, and 704$^{\circ}C$. The predictive equation derived from the ISM in creep tests showed better reliability than those from LMP (Larson-Miller Parameter) and LMP-lSM (Larson Miller Parameter-Initial Strain Method) specially for long time creep prediction (10$^3$∼10$\^$5/h).

Mechanical and Tribological Properties of Pulse and Direct Current Electrodeposited Ni-TiO2 Nano Composite Coatings

  • Gyawali, Gobinda;Woo, Dong-Jin;Lee, Soo-Wohn
    • Journal of the Korean institute of surface engineering
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    • v.43 no.6
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    • pp.283-288
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    • 2010
  • Ni-$TiO_2$ nano composite coatings were fabricated using pulse current electrodeposition technique at 100 Hz pulse frequency with a constant 50% pulse duty cycles and reference was taken with respect to the direct current (dc) electrodeposition. The properties of the composite coatings were investigated by using SEM, XRD, Wear test and Vicker's microhardness test. Pulse electrodeposited composite has exhibited enhancement of (111), (220), and (311) diffraction lines with an attenuation of (200) line. The results demonstrated that the microhardness of composite coatings under pulse condition was significantly improved than that of pure nickel coating as well as dc electrodeposited Ni-$TiO_2$ composite coatings. Wear tracks have shown the less plastic deformation in pulse plated composite. Coefficient of friction was also found to be lower in pulse plated composite coatings as compared to dc plated composite coatings.

Influence of Growth Rate on Biosorption of Heavy Metals by Nocardia amarae

  • Kim, Dong Wook;Daniel K. Cha;Hyung-Joon Seo;Jong Bok Bak
    • Journal of Microbiology and Biotechnology
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    • v.12 no.6
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    • pp.878-881
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    • 2002
  • The goal of the current research was to assess the influence of the growth rate of Nocardia amarae on its overall metal binding capacity. Batch sorption isotherms for cadmium (Cd), copper (Cu), and nickel (Ni) showed that Nocardia cells harvested from chemostat cultures at a dilution rate of $0.33d^-1$ had a significantly higher metal sorption capacity than cells grown at 0.5 and $1d^-1$. The cell surface area estimated using a dye technique indicated that pure N. amarae cells grown at a lower growth rate had a significantly more specific surface area than cells harvested from a higher growth rate operation. Accordingly, this difference in the specific surface area seemed to indicate that the higher metal sorption capacity of the slowly growing Nocardia cells was due to their higher specific surface area.

The Fabrication and Characteristics of White Emission using CCM on Flexible Substrate (플렉시블 무기EL 색변환 백색 발광 소자 제작 및 특성평가)

  • Kim, Gi-Ryoung;Ahn, Sung-Il;Kum, Jeong-Hun;Lee, Heung-Ryeol;Yim, Tae-Hong;Lee, Seong-Eui
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.10
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    • pp.911-915
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    • 2008
  • EL (electro-luminescent) device as a light source has an advantage in embodying large area with great flexibility. On nickel foil as an electrode and backplane, we demonstrated a white EL flexible light source with blue phosphor layer combined with color change layer. A correlation between color change layer and color coordination was analyzed by Gaussian method, and then the color coordinate was controlled near to (0.33, 0.33) of pure white light.

Comparison of Theoretical model with Experiment in Bead Shape of Laser Welding (레이저 용접의 비드 형상에 대한 실험치와 이론 결과의 비교)

  • Kim, J.D.;Kim, J.D.
    • Journal of the Korean Society for Precision Engineering
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    • v.11 no.1
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    • pp.201-210
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    • 1994
  • A theoretical heat-flow model incorporating with a constant moving CO$_{2}$ laser beam has been analyzed to predict depth and the shape of bead section during last beam welding. The laser beam is exponentially attenuated with an abosrption coefficient in the material. The solution can be expressed in terms of normalized variables. The experimental data were generated by usint CW 2 CO$_{2}$ laser with multi beam mode and CW 3 kW CO$_{2}$laser with Gaussian mode. The specimens were made as bead-on-plate welds for SM 10C, STS 304, STS 316, STS 420 and pure Nickel. The maximum possible penetration depth and the shape of beas section for given sources of laser power, travel speed and beam spot size can be prdicted with this model in a given material.

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Creep Properties of Superalloy Udimet 720 in relation to Exposed (초내열합금 U720의 노출시험에 따른 크리프 특성)

  • Kong, Y.S.;Oh, S.K.
    • Journal of Power System Engineering
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    • v.5 no.2
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    • pp.57-62
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    • 2001
  • Gas turbine performance is highly dependent on the engine performance which is closely related to the engine materials since they are exposed to severe working environments, i.e, high temperature and high stresses. For this reason, advanced materials with improved properties are required for the engine. The purpose of this research is to develop key materials technologies for aircraft industry and to tester domestic production of related parts. In this paper, the real-time prediction of high temperature creep strength and creep life for nickel-based superalloy Udimet 720(high-temperature and high-pressure the gas turbine engine materials) was performed on round-bar type specimens under pure load at the temperatures of 538, 649 and $704^{\circ}C$.

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Synthesis of BiSrCaCu(Ni)O Ceramics from the Gel Precursors and the Effect of Ni Substitution

  • Ahn, Beom-Shu
    • Bulletin of the Korean Chemical Society
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    • v.23 no.9
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    • pp.1304-1323
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    • 2002
  • Superconducting BiSrCaCu(Ni)O ceramicss have been prepared by the gel method using an aqueous solution containing a tartaric acid. The aqueous solution of metal salts was concentrated without precipitation. The precursor so prepared was homogeneou s and calcined at $825^{\circ}C$ for 24 h to produce superconducting phase. The thermal decomposition of gels, the formation of superconducting phase, and their ceramic microstructure were studied using IR, TGA, XRD, resistance measurements, and SEM. This method is highly reproducible and leads to powders with excellent homogeneity and small particle size for easy sinterability. The nickel dopant substituting for Cu gives rise to the gradual decrease of the Tc. Phase pure 2212 ceramics were obtained at 825 $^{\circ}C$ for 24 h. SEM pictures showed that liquid phase was formed when the samples were sintered temperatures higher than 825 $^{\circ}C$.