• Title/Summary/Keyword: Pretreatment temperature

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Dimensional Properties of Low Temperature Plasms and Silicone Treated Wool Fabric

  • Kim, Min-Sun;Kang, Tae-Jin
    • Fibers and Polymers
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    • v.2 no.1
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    • pp.152-156
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    • 2001
  • Three different silicone polymer systems, such as aminofunctional, epoxyfunctional, and hydrophilic epoxyfunctional silicone polymers, were applied onto plasma pretreated wool fabric to improve the dimensional properties. The results showed that the plasma pretreatment modified the cuticle surface of the wool fiber and increased the reactivity of wool fabric toward silicone polymers. Felting shrinkage of plasma and silicone treated wool fabric was decreased with different level depending on the applied polymer system. Fabric tear strength and hand were adversely affected by plasma treatment, but these properties were favorably restored on polymer application. Therefore, it has been concluded that the combination of plasma and silicone treatments can achieve the improved dimensional stability, and better performance properties of wool fabric. The surface smoothness appearances of treated fabrics were measured using a new evaluation system, which showed good correspondence with the results of KES-FB4 surface tester.

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Studies on the Characteristics of Humic Acid and its Utilizations (I) (土炭 흄酸의 性狀 및 應用에 關한 硏究 (I) 흄酸의 溶出 및 그 條件에 따른 흄酸性狀의 變異)

  • Kim, Won-Taik
    • Journal of the Korean Chemical Society
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    • v.12 no.4
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    • pp.155-159
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    • 1968
  • On the extraction of humic acid from peat, the optimum conditions were studied and the effects of them on the characteristics of humic acid were also examined by means of infrared spectroscopy. 1. Pretreatment of peat with diluted 6-8% HCl solution for 5 hrs. prior to extraction with alcohol-benzol azeotropic mixture have resulted the better yield of humic acid. The water soluble Na-humates were obtained by the subsequent extraction with one hundred times quantity of caustic soda solutieon for 1hr. at 90 $^{\circ}C$. Thus the pure humic acids have been yielded approximately 40% (by wt.) from the raw peat. 2. In characteristics of humic acid, the chemical structure, mainly the contents of such functional groups as -COOH, -OH (phenol type), $-CH_2CO-$, $-CH_2{\cdot}O{\cdot}CH_2-$ and aromatic rings were varied according to the concentration of alkaline solution, temperature and time when the humic acids were extracted with alkali.

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Effect of Steaming Prior to Roasting of Polygonatum odoratum Roots on Its Water Solubles and Browning (볶음전 증자처리가 둥굴레 근경의 수용성 성분 및 갈색화에 미치는 영향)

  • 권중호;임종호
    • Food Science and Preservation
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    • v.4 no.2
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    • pp.155-162
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    • 1997
  • This work was designed to determine the effect of steaming-Pretreatment on Physicochemical and functional properties of roasted Polygonatum odoratum roots. Steaming treatments led to some reduction in the contents of water solubles, such as total solid, reducing sugar and free-amino nitrogen of the unroasted samples. Moreover, roasting processing caused decrease in reducing sugar and free-amino acid, with increase in total soluble solid and browning color of the samples, which showed the dependence of steaming treatment as well as roasting temperature. Electron-donating ability and nitrite-scavenging ratio of the samples were also highly developed along with roasting processing at 17$0^{\circ}C$ within 35min. Considering the physicochemical and some functional parameters of water extracts of roasted samples, roasting at above 14$0^{\circ}C$ for over 55min or at 17$0^{\circ}C$ for around 35min was recommendable for the higher quality of Polygonatum odoritum tea, which conditions were similarly adapted for both steamed and unsteamed samples.

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Studies on the Transfer Printing of Cotton Fabrics (면직물의 건식전사날염에 관한 연구)

  • Hwang, Jong-Ho;Lee, Seok-Young;Cho, Hwan
    • Textile Coloration and Finishing
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    • v.7 no.3
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    • pp.31-37
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    • 1995
  • Effects of glycol pretreatment conditions such as concentration and molecular weight of glycols and dye types of different constitutions on the degree of transfer were investigated when transfer printed onto the cotton fabric with disperse dyestuffs. Obtained results are as follows ; 1. Although the degree of transfer increases linearly with temperature a time, above a certain critical point, they show decremental aspects for both of C.I. Disperse Orange 3 and C.I. Diperse Violet 1. 2. Degree of transfer increases with molecular weight of glycols, but PEG 200 which has a moleular weight 200 and boiling point of 300$^{\circ}C$ is more effcient than that of lower molecular weight. 3. Degree of tansfer for the C.I. Disperse Orange 3 having constitution of azo benzene type is somewhat higher than that of C.I. Disperse Violet 1 of amino anthraquinone.

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A study on fatigue life of Al 7075/CFRP multilayered hybrid composite materials (Al 7075/CFRP 다적층 하이브리드 복합재료의 피로수명에 대한 연구)

  • 윤한기;김연겸;박준수;이경봉
    • Journal of Ocean Engineering and Technology
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    • v.10 no.4
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    • pp.92-102
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    • 1996
  • In this research, to develope the A1 7075/CFRP multilayered hybrid composites, CRALL(Carbon Reinforced aluminum lamiate) specimens were processed by autoclavecuring system that curing temperature, time, surface pretreatment condition of aluminum were constant. Andthe fatigye life and failure mechanism on CFRP volume fraction and fiber orientation of CRALLspecimens were investigated. A fatigue life was greatly influenced by effect of CFRP fiber volume fraction but it was less effected than those of fiber orientation. The fatigue failure arised from interface delamination of CFRP and aluminum sheet after shear fracture of aluminum layer. The failure mechanism is assumed that the aluminum laminates which divide the CFRP into many thim layers tend to arrest the failure propagation.

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Weight Loss Rates and Physical Properties Changes of Cellulose Fabrics by Cellulase Treatment (셀룰라제처리에 의한 섬유소계직물의 감량률과 물리적성능 변화)

  • Lee Hye-Ja;Chon Hae-Kyung;Yoo Hye-Ja
    • Journal of the Korean Home Economics Association
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    • v.37 no.12 s.142
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    • pp.169-177
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    • 1999
  • This study has examined weight loss rates of Iyoceu, lyocell/cotton, cotton that were treated with cellulase under different concentration, time, temperature and pH. and compared physical properties changes of tensile strength, drape, moisture absorbency, shrinkage and dyeability. The notable results are summarized as follows: Lyocell was in need of pretreatment by NaOH in the side of weight loss, tensile strength and dyeability. Weight loss rates of cellulose fabrics by cellulase treatment were in the order of cotton > lyocell/cotton > lyocell at the same conditions. In case of lyocell and lyocell/cotton, weight loss rates showed up lower than cotton, while strength retention decreased, drape and strength flexibility were highly improved after cellulase treatment.

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A Technique for Increasing Cellulose Hydrolysis (섬유소의 가수분해에 대한 기술 개발 모색(I))

  • 박주정;박성화
    • KSBB Journal
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    • v.4 no.3
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    • pp.235-240
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    • 1989
  • A novel pretreatment of rice straw has been developed to increase the reactivity of cellulose, in particular to increase the rate and extent of cellulose enzymatic hydrolysis. This technique is called ammonia-freeze-explosion method and relies on treatment of the lignocellulosic material with a volatile liquid under pressure followed by pressure release to evaporate the liquid and reduce the temperature by Bme E. Dale of Texas A & M University. Volatile liquids which also chemically explosion and swell lignocellulosic materials are particularly effective when used in this technique. Above four times of conversion of cellulose to glucose has been achived by enzymatic hydrolysis of rice straw with this method.

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SURFACE CHARACTERIZATION OF CU ELECTRODES IN ELECTROCHEMICAL REDUCTION OF $CO_2$ BY CORE LEVEL X-RAY PHOTOELECTRON SPECTROSCOPY AND VALENCE LEVEL PHOTOELECTRON EMISSION MEASUREMENT

  • Terunuma, Y.;Saitoh, A.;Momose, Y.
    • Journal of the Korean institute of surface engineering
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    • v.29 no.6
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    • pp.728-734
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    • 1996
  • To obtain the relation in the electrochemical reduction of $CO_2$ in aqueous $KHCO_3$ colution between an activity for the product and the nature of Cu electrode, the electrode surface was characterized by using two methods: X-ray photoelectron spectroscopy (XPS) and photoelectron emission (PE) measurement. Electrolyses were performed with Cu electrodes pretreated in several ways. The distribution of the products changed drastically with electrolysis time and the pretreatment method. The features in XPS spectra were closely connected with the product distribution. The oxide film at the electrode surface was gradually reduced to bare Cu metal with electrolysis time, resulting in a variation of the product distribution. PE was measured by verying the wavelength of incident light at several temperatures. The dependence of PE on the measurement temperature changed greatly before and after electrolysis.

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The Influence of Electrolytic Condition on Tunnel Etching and Capacitance Gain of High purity Aluminium Foil on capacitor (전해조건이 고순도 알루미늄 박 콘덴서의 터널에칭과 정전용량에 미치는 영향)

  • 이재운;이병우;김용현;이광학;김흥식
    • Journal of the Korean institute of surface engineering
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    • v.30 no.1
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    • pp.44-56
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    • 1997
  • Influence of electrochemical etching conditions on capacitance gain of aluminium electrolytic on capacitor foil has been investigated by etching cubic textured high purity aluminum foil in dilute hydrochloric acid. Uniformly distributed etch pit tunnels on aluminum surface have been obtained by pretreatment aluminium foil in 10% NaOH solution for 5 minutes followed by electrochemical etching. Electrostatic capacitance of etched aluminium foil anodized to high voltage increased with the increase of current density, total charge, temperature and concentration of electrolyte up to maximum CV-value and then deceased. Election optical observation of the etched foil revealed that the density of etch of etch pits increased with the increase of current density and concentration of electrolyte. this increase of etch pit density enlarged of the increase of capacitance. However, abnormal high current density and high electrolyte concentration induced the local dissolution of the foil surface which resulted the decrease of foil capacitance.

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Development of Susceptible Functional Fibers Using Microencapsulation of Susceptible Materials(III) ―Fragrant Functional Fibers― (감성물질의 마이크로캡슐화에 의한 감성기능 섬유의 개발(III) -방향 기능 섬유-)

  • Kim, Moon Sik;Park, Soo Min
    • Textile Coloration and Finishing
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    • v.8 no.4
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    • pp.11-18
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    • 1996
  • Natural functional compound in the textile finishing for health and amenity using fragrant material have been applied by microencapsulation method. The microcapsules containing fragrant materials as functional compound were produced by in situ polymerization using urea-formaldehyde prepolymer. The average diameter of microcapsules is 2.75$\mu$ and particle size ranges over 0.5~10$\mu$. Fragment material is extracted approximatly proportioned from microcapsule at room temperature. The adsorption of microcapsule was improved by pretreatment of cationic agent. Fragrant materials in microcapsule was revealed to have long release time.

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