• Title/Summary/Keyword: Pretreatment temperature

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Effects of High Temperature of Pretreatment on the Color Development and Quality of Satsuma Mandarins (온주밀감의 저장전 고온 예조가 저장중 과실의 착색 및 품질에 미치는 영향)

  • Nam, Ki-Woong;Kwon, Hyeog-Mo
    • Korean Journal of Organic Agriculture
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    • v.10 no.3
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    • pp.57-66
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    • 2002
  • The experiment described in this paper focused on determining the effects of high-temperature(20$^{\circ}$) treatment of Satsuma mandarins, prior to their storage, on their color development and quality. High-temperature treatment promoted fruit skin color during the storage, decreased the weight loss regardless of their color at the time of their harvest and reduced the decay occurrence until the middle of March, but there was no difference between treatments after the end of March. There was a tendency of higher soluble solid and acid levels in the fruit when high-temperature treatment was applied but this difference was not significant.

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An Effective Process for Removing Organic Compounds from Oily Sludge

  • Jing, Guolin;Luan, Mingming;Chen, Tingting;Han, Chunjie
    • Journal of the Korean Chemical Society
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    • v.55 no.5
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    • pp.842-845
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    • 2011
  • Wet air oxidation (WAO) of oily sludge was carried out using $Fe^{3+}$ as catalyst, placed in a 0.5 L batch autoclave in the temperature range of $250-330^{\circ}C$. Experiments were conducted to investigate the effects of temperature, the initial COD, reaction time, concentration of catalyst and $O_2$ excess (OE) on the oxidation of the oily sludge. The results showed that in the WAO 88.4% COD was achieved after 9 min reaction at temperature of $330^{\circ}C$, OE of 0.8 and the initial COD of 20000 mg/L. Temperature was found to have a significant impact on the oxidation of oily sludge. Adding a catalyst significantly improved the COD removal. Homogenous catalyst, $Fe^{3+}$, showed effective removal for pollutants. COD removal was 99.7% in the catalytic wet air oxidation (CWAO) over $Fe^{3+}$ catalyst. The results proved that the CWAO was an effective pretreatment method for the oily sludge.

Diamond Synthesis by Acetylen Flame (아세틸렌 불꽃에 의한 다이아몬드 합성)

  • 이윤석;박윤휘;이태근;정수진
    • Journal of the Korean Ceramic Society
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    • v.29 no.12
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    • pp.926-934
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    • 1992
  • Uniform diamond films in a few $\textrm{mm}^2$ size and locally isolated diamond single crystals in size of 60 $\mu\textrm{m}$ were synthesized on Si-wafer and Al2O3 substrate by the method of acetylene flame. The effects of substrate temperature and flow ratio of oxygen to acetylene on the morphology of deposited diamond were investigated. According to the observations of growth behavior of diamond on Si substrate with respect to substrate surface pretreatment and flow ratio, it was shown that well faceted diamonds could grow uniformly when flow ratio was above 0.9 and substrates were densely scratched. With increasing substrates temperature, the crystal morphology changes from octahedron bounded by only {111} plane below 850$^{\circ}C$ to cubo-octahedron with almost equal development of {111} and {100} plane in the temperature range of 850∼950$^{\circ}C$. Between 950∼1050$^{\circ}C$, the {111} faces become rough and concave. Above 1050$^{\circ}C$, new crystallites begin to grow on concave {111} surface and overall morphology looks like cubo-octahedron with degenerated {111} faces. These changes of morphology can be understood in terms of the different growth mode of each crystallographic plane with respect to the substrate temperature and supersaturation. And the observed phenomena on {111} planes can be related to the face instability and twin generation.

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Thermoplasticization of Wood by Benzylation (벤질화에 의한 목재의 열가소화)

  • Han, Gyu-Seong;Kim, Eun-Kyoung
    • Journal of the Korean Wood Science and Technology
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    • v.22 no.3
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    • pp.32-38
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    • 1994
  • The methods in wood processing are so limited at present that a scope of its utilization is restricted. This often makes wood itself less valuable as a material comparing with other materials, that is, plastics, metals, and glass. Such differences are due to a lack of plasticity in wood, i.e. it cannot be melted, dissolved, or softened sufficiently for molding. However, once plastic properties are added to wood, it becomes more useful material. This further broadens the method in wood processing to a variety of fields. In this way, wooden material which is limited in use can be modified into a high quality product with additional value. Furthermore, utilization of wastes from wood, for example, would be made viable. In this study, thermoplasticization was carried out by benzylation of wood(sawdust). Various factors those affect the reaction were tested to produce benzylated wood with different degrees of substitution. Reaction temperature and time were the quite important factors. Optimum reaction temperature was 110$^{\circ}C$, and weight percent gains(WPG) of final products increased gradually with the increase of reaction time. The pretreatment (or preswelling) of wood with alkaline solution had a critical effect on benzylation. and the concentration of alkaline solution should be above 30% to obtain high weight percent gain. The thermal flow temperature of the benzylated wood decreased with the increase in weight percent gain, that of 80% weight percent gain is about 200$^{\circ}C$.

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Changes of Quality in the Osmotic Dehydration of Cherry-Tomatoes and optimization for the Process (방울토마토의 삼투건조시 품질의 변화와 공정의 최적화)

  • 윤경영;윤광섭;이광희;신승렬;김광수
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.26 no.5
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    • pp.866-871
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    • 1997
  • This study was carried out to determine the effect of osmotic dehydration as pretreatment on the qualities of dried cherry-tomatoes. The weight reduction and solid gain in osmosed cherry-tomato were increased by increasing sugar concentration, immersion temperature and time; among three parameters, the immersion temperature affected more than sugar concentration and immersion time did. The moisture content was decreased as increasing sugar concentration, immersion temperature and time, and it was the lowest at the osmotic conditions of 7$0^{\circ}C$, 60$^{\circ}$Brix and 11hr. To determine the optimum processing condition by RSm, the polynomial optimum models were established. The regression models was significant (p<0.05). It was used contour plots to optimize osmotic dehydration. The optimum condition for osmotic dehydration as pretreatments for drying of cherry-tomatoes were immersion temperature of 47~53$^{\circ}C$, sugar concentration of 39~43$^{\circ}$Brix, and immersion time of 7hr, in which process conditions were 78~86% moisture content, 8.5~10$^{\circ}$Brix sugar content and 80~86% weight reduction.

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An experimental study of hot filament chemical vapor deposition for diamond films (HFCVD에 의한 다이아몬드 박막 증착에 관한 실험적 연구)

  • Kim, Yeong-Jae;Han, Dong-Cheol;Choe, Man-Su
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.22 no.5
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    • pp.563-572
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    • 1998
  • An experimental study of hot filament chemical vapor deposition(HFCVD) has been carried out for the fabrication of diamond thin film. Of particular interest is the measurement of deposition uniformity on large substrates. Experimental apparatus including a vacuum chamber, heating elements, etc. has been designed and manufactured. Deposition profiles for different pretreatment powders and different flow rates have been measured in conjunction with the measurement of substrate temperature distribution on a large substrate surface. As the flow rate increases, deposition rate increases, however, the crystallinity becomes worse. Higher growth rate has been found on the region closer to the center location where substrate temperature is higher. The crystallinity has been improved as gas flow rate decreases. The growth rate and morphology of deposition were identified by SEM and the existence of diamond phase was proved by Raman spectroscopy.

Improvement of Accuracy for Determination of Hydrogen Storage of Sieverts Apparatus (부피법을 이용한 수소 저장 성능 평가 장치의 수소 저장량 측정법 개선)

  • Cho, Won-Chul;Han, Sang-Sub;Park, Chu-Sik
    • Transactions of the Korean hydrogen and new energy society
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    • v.19 no.1
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    • pp.64-70
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    • 2008
  • This paper briefly discusses the main sources of errors and their solutions for measuring hydrogen uptake from gas phase by the Sieverts technique. Correction of volumetric errors of apparatus, density of hydrogen storage material, estimation of temperature gradient are investigated. Systematic errors and the change of density of the host material according to the pressure have been the subject of much controversy in recent years. We considered the standard ball calibration, temperature gradient distribution, pretreatment of hydrogen storage materials to minimize errors. We could lessen the miscalculations after applying those methods to Equilibrium pressure-composition isotherm data.

Diamond Synthesis by W Filament CVD (W Filament CVD에 의한 Diamond의 합성)

  • 서문규;강동균;이지화
    • Journal of the Korean Ceramic Society
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    • v.26 no.4
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    • pp.550-558
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    • 1989
  • Polycrystalline diamond films have been deposited on Si wafer Ly hot W filament CVD method using CH4H2 mixtures. The effects of surface pretreatment, W filament temperature, CH4 volume fraction, and addition of water vapor on the growth rate and morphology of the films were investigated. Surface pretretment was essential for depositing a continuous diamond film. Raising the filament temperature resulted in an increased growth rate and a better crystal quality of the film. As the methane content is varied from 0.5% to 5%, well-faceted crystals gradually transformed into spherical particles of non-diamond phase with a simultaneous increase in the growth rate. Addition of water vapor markedly improved the crystallinity to produce crystalline particles even with 5% methane mixture.

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Updated Pretreatment Technologies for Automotive in Japan

  • Takaknwa, Hideki;Ishii, Hitoshi
    • Corrosion Science and Technology
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    • v.6 no.5
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    • pp.245-250
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    • 2007
  • Recently, to avoid global warming, reduction of $CO_2$ generation has been demanded. Each car manufacture takes positive actions for improvement in fuel consumption by various kinds of countermeasures, e.g. improving engine efficiency, using alternative fuels, lightening the car body. Regarding lightening of the car body, aluminum alloys and high tensile strength steels has been gradually adopted as lightweight materials. However, such materials are normally not easy to be treated with zinc phosphate system. Focusing the pre-treatment processes, low temperature phosphate system could be demanded for energy saving. This time, new surface conditioning process for lightweight materials and low temperature phosphate system shall be discussed.

A Study on Applicability of Carbon Ceramic Disc using Pretreated Carbon Fiber (전처리된 탄소섬유를 이용한 카본 세라믹 디스크 적용 가능성에 대한 연구)

  • Yoo, Tae-Doo;Kim, Hong-Gun;Kwac, Lee-Ku
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.21 no.4
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    • pp.39-45
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    • 2022
  • In this study, it was verified that carbon-ceramic brake discs can replace existing cast-iron brake discs of the same size. In addition, a method of pretreating carbon fiber to secure heat dissipation characteristics while using a small amount of carbon fiber was established. The thermal conductivity and bending strength characteristics were analyzed according to the carbon content, and brake braking tests were conducted. Through pretreatment, the maximum temperature was lowered by 16 ℃ compared to the case using only carbon fiber, and the cooling rate was improved by approximately 10% compared to metal brake discs. However, the total heat capacity increased as the mass increased owing to the reaction. Thus, the measured temperature was higher than that of the metal brake disc; therefore, additional research is required.