• Title/Summary/Keyword: Precipitation Separation

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가금부산물인 닭 용골연골로부터 chondroitin sulfate를 포함하는 뮤코다당단백질의 추출에 관한 연구

  • 신승철;김동욱;김관응;안승민;유선종;김성권;안병기;강창원
    • Proceedings of the Korea Society of Poultry Science Conference
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    • 2004.11a
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    • pp.26-27
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    • 2004
  • This study was conducted to evaluate the value of chicken keel cartilage as a source of mucopoly-saccharide-protein containing chondroitin sulfate (CS) and to find the optimum extraction conditions. The hot water extraction and alcalase hydrolysis methods were performed for extraction mucopolysaccharide in lyophilized chicken keel cartilage. The most efficient condition was hydrolysis with 2 % alcalase in 10 volumes of distilled water for 120 min. The yield of hydrolysate and CS content were 75.87 % and 25.61 %, respectively. For further separation of CS from hydrolysate by alcalase, ethanol precipitation was performed. The yield of ethanol precipitate and its CS content were 21.41 % and 46.31 %, respectively.

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Superconducting Magnetic Separator for Purification of Industrial Wastewater (산업폐수의 수처리를 위한 초전도 자기분리 장치 제작)

  • Ha, Dong-Woo;Kwon, Jun-Mo;Ko, Rock-Kil;Baik, Seung-Kyu;Sohn, Myung-Hwan;Lee, Yu-Jin;Kim, Tae-Hyung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.44-44
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    • 2010
  • Conventional water treatment facilities like precipitation process need large-scale equipment and wide space to purify the wastewater of paper factory. In case of massive waste water, high gradient magnetic separation (HGMS) parts are more effective to purify it rapidly and to occupy relatively small space, since large voids at filter with HGMS are adopted. Cryo-cooled Nb-Ti superconducting magnet with room temperature bore in diameter of 100 mm and 600 mm in height was used for magnetic separator. Magnetic filters were designed by the analysis of magnetic field distribution at superconducting magnets.

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Cellulose acetate membrane preparation by phase inversion to estimate optimized parameters and its performance study

  • Katariya, Heena N;Patel, Tejal M
    • Membrane and Water Treatment
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    • v.13 no.3
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    • pp.139-145
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    • 2022
  • Development in advanced separation processes leads to the significant advancement in polymeric membrane preparation methodology. Therefore, present research investigated the preparation and characterization of cellulose acetate membrane by phase inversion separation method to determine optimized operating parameters. Prepared CA membrane's performance was been analyzed in terms of % rejection and flux. Investigation was conducted to study effect of different parameters such as polymer concentration, evaporation rate, thickness of film, coagulation bath properties, temperature of polymer solution and of the coagulation bath etc. CA membrane was fabricated by taking polymer concentration 10wt% and 11wt% with zero second evaporation time and varying film thickness over non-woven polyester fabric. Effect of coagulation bath temperature (CBT) and casting solution temperature were also been studied. The experimental results from SEM showed that the surface morphology had been changed with polymer r concentration, coagulation bath and casting solution temperature, etc. Lower polymer concentration leads to lower precipitation time giving porous membrane. The prepared membrane was tested for advanced waste water treatment of relevant effluent stream in pilot plant to study flux and rejection behavior of the membrane.

Total value recovery in the copper smelting and refining operations

  • Kim Joe. Y.;Kong Bong S.
    • 한국지구물리탐사학회:학술대회논문집
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    • 2003.11a
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    • pp.590-597
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    • 2003
  • Processing and smelting of copper containing sulphide concentrates result in the accumulation of impurities into various process streams. All primary copper smelters and refineries around the world produce significant amounts of slag, dust, sludge, residues and others, which contain copper and precious metals. The recovery of these valuable metals is essential to the overall economics of the smelting process. Physical, chemical and mineralogical characterization of particular slag and Cottrell dusts from primary smelters and $Dor\'{e}$ furnace (TBRC) slag and Pressure Leached Anode slimes from a copper refinery have been carried out to understand the basic behind the recovery processes. Various process options have been evaluated and adapted for the treatment of slag from different smelting furnaces and Cottrell dusts as well as the intermediate products from copper refineries. Besides the hydro- or pyro-metallurgical treatments, the above mentioned physical separation options such as magnetic, gravity separation, flotation and precipitation flotation processes have been successfully identified and adapted as the possible process options to produce a Cu-rich or precious metal-rich concentrates for in-house recycling and other valued by-product for further treatment. The results of laboratory, pilot plant and production operations are presented, and incorporation of several alternative flowsheet is discussed in this paper.

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MINERAL PROCESSING and COPPER EXRACTIVE METALLURGY Complete Metal Recovery

  • Kim, J.Y.
    • Proceedings of the Korean Institute of Resources Recycling Conference
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    • 2003.10a
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    • pp.22-34
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    • 2003
  • Processing and smelting of copper containing sulphide concentrates result in the accumulation of impurities into various process streams. All primary copper smelters and refineries around the world produce significant amounts of slag, dust, sludge, residues and others, which contain copper and precious metals. The recovery of these valuable metals is essential to the overall economics of the smelting process. Physical, chemical and mineralogical characterization of particular slag and Cottrell dusts from primary smelters and Dore furnace (TBRC) slag and Pressure Leached Anode slimes from a copper refinery have been carried out to understand the basic behind the recovery processes. Various process options have been evaluated and adapted for the treatment of slag from different smelting furnaces and Cottrell dusts as well as the intermediate products from copper refineries. Besides the hydro- or pyre-metallurgical treatments, the above mentioned physical separation options such as magnetic, gravity separation, flotation and precipitation flotation processes have been successfully identified and adapted as the possible process options to produce a Cu-rich or precious metal-rich concentrates for in-house recycling and other valued by-product for further treatment. The results of laboratory, pilot plant and production operations are presented, and incorporation of several alternative flowsheet is discussed in this paper.

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Separation and Recovery of Tin and Indium from Spent ITO Sludge (폐 ITO 슬러지로부터 주석과 인듐의 분리·회수)

  • Lee, Ki-Woong;Kim, Hong-In;Son, Hyun-Tae;Ahn, Jae-Woo;Kim, Yong-Hwan
    • Resources Recycling
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    • v.23 no.2
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    • pp.53-60
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    • 2014
  • In order to separate Indium and Tin from spent indium tin oxide (ITO) sludge, direct hydrochloric acid leaching and thermal reduction followed by HCl leaching were applied. In case of direct leaching of spent ITO, leaching rate of In and Sn was 18.5% and 19.95%, respectively. Whereas, in case of thermal hydrogen treatment of ITO sludge at different temperatures such as $700^{\circ}C$, $800^{\circ}C$, $900^{\circ}C$ and $1100^{\circ}C$, followed by HCl leaching, we obtained the result of more than 97% leaching rate of Sn. Specially, thermal treatment at $800^{\circ}C$ showed the highest leaching rate of 98.2% of Sn. Precipitation method was used for separation and recovery of Sn from leached mixed solution. If the solution pH were adjusted 2.0, 99.69% of Sn precipitated and 10.3% of In was precipitated. This confirmed the possibility of separation of Sn and In from leached solution by precipitation method.

Estimation and Assessment of Future Design Rainfall from Non-stationary Rainfall Frequency Analysis using Separation Method (호우분리기법을 적용한 비정상성 빈도해석의 미래확률강우량 산정 및 평가)

  • Son, Chan-Young;Lee, Bo-Ram;Choi, Ji-Hyeok;Moon, Young-Il
    • Journal of Korea Water Resources Association
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    • v.48 no.6
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    • pp.451-461
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    • 2015
  • This study aimed to estimate the future design rainfall through a non-stationary frequency analysis using the rainfall separation technique. First, we classified rainfall in the Korean Peninsula into local downpour and TC-induced rainfall through rainfall separation technique based on the path and size of a typhoon. Furthermore, we performed the analysis of regional rainfall characteristics and trends. In addition, we estimated the future design rainfall through a non-stationary frequency analysis using Gumbel distribution and carried out its quantitative comparison and evaluation. The results of the analysis suggest that the increase and decrease rate of rainfall in the Korean Peninsula were different and the increasing and decreasing tendencies were mutually contradictory at some points. In addition, a non-stationary frequency analysis was carried out by using the rainfall separation technique. The outcome of this analysis suggests that a relatively reasonable future design rainfall can be estimated. Comparing total rainfall with the future design rainfall, differences were found in the southern and eastern regions of the Korean peninsula. This means that climate change may have a different effect on the typhoon and local downpour. Thus, in the future, individual assessment of climate change impacts needs to be done through moisture separation. The results presented here are applicable in future hydraulic structures design, flood control measures related to climate change, and policy establishment.

The Correlation between Groundwater Level and GOI with Snowmelt Effect in Ssangchun Watershed (쌍천유역의 지하수위와 융설 효과를 고려한 GOI의 상괸관계)

  • Yang, Jeong-Seok;Lim, Chang-Hwa;Park, Jae-Hyeon;Park, Chang-Kun
    • Journal of Korea Water Resources Association
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    • v.39 no.2 s.163
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    • pp.121-126
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    • 2006
  • Snowmelt effect is identified from the analysis of the relationship between precipitation and groundwater level(GWL) data and Severe drawdown of GWL is observed in drought. Groundwater dam Operation Index (GOI), which is developed for the optimal operation of groundwater dam, is calculated by taking common logarithm of the moving average(MA) of precipitation data for a certain period. The period can vary from watershed to watershed because the period is decided by picking the maximum correlation coefficient between GWL and GOI of several MAs of precipitation. For Ssangchun watershed, the correlation was the strongest when we apply 70 day MA for GOI calculation. Snowmelt effect is considered by applying the temperature change by elevation($0.5^{\circ}C$ decrease per 100m) and examining the areal distribution of the watershed by elevation. Snow event is assumed when the daily average temperature is below $0^{\circ}C$ and snowmelt is assumed when the temperature is above zero degree Celsius. Total snowmelt is assumed for the day. When the snow event is occurred the precipitation data is separated into two components, snow and rainfall. The areal distribution by elevation is used for the calculation in the separation. The correlation between GWL and GOI is higher when we consider snowmelt effect than we neglected it.

Column Chromatographic Separation of Titanium, Zirconium and Niobium (Ti, Zr 및 Nb의 원통크로마토그라프 분리)

  • Chul Lee;Yung Chang Yim;Koo Soon Chung
    • Journal of the Korean Chemical Society
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    • v.17 no.1
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    • pp.15-19
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    • 1973
  • A method was developed for the separation of titanium, niobium and zirconium together in a group from the coexisting ions of various metals such as iron, cobalt, nickel, yttrium and rare earths by means of the cation exchange column using ${\alpha}$-hydroxyisobutyric acid as the eluent. In the course of the present investigation, it was found that the tailing phenomena of zirconium were attributable to the hydroxide precipitation which was made prior to the elution. For example, if zirconium was precipitated by sodium hydroxide, the tailing of zirconium became very serious in contrast to the results reported by others. This paper describes how these tailing phenomena of zirconium were prevented and how a practical procedure for the separation of these ions was, achieved using ion-exchange method. Using the present method the nuclides of $^{90m}Y$ and $^{90}Y$ were separated with radiochemical purity from the irradiated zirconium.

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Purification of wastewater from paper factory by superconducting magnetic separator (초전도 자기분리에 의한 제지폐수의 정수)

  • Ha, Dong-Woo;Kim, Tae-Hyung;Kwon, Jun-Mo;Sohn, Myung-Hwan;Baik, Seung-Kyu;Oh, Sang-Soo;Ha, Hong-Soo;Ko, Rock-Kil;Kim, Ho-Sup;Kim, Young-Hun;Ha, Tae-Wook
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.342-343
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    • 2009
  • Paper factories use a large amount of water and same amount of wastewater is generated. It is important to purity and recycle the wastewater because of water shortages and water pollution. The existing water treatment facilities like precipitation process need large-scale equipment and wide space to purity the wastewater of paper factory. High gradient magnetic separation (HGMS) system has the merits to purity rapidly because of large voids at filter and to occupy small space. In this paper, two types of superconducting magnets were used for HGMS systems. Cryo-cooled Bi-2223 superconducting magnet system with 70 mm room temperature bore and 200 mm of height was prepared. Cryo-cooled Nb-Ti superconducting magnet with 100 mm room temperature bore and 600 mm of height was used for magnetic separator. Magnetic filters were designed by the analysis of magnetic field distribution at superconducting magnets. The various magnetic seeding reactions were investigated to increase the reactivity of coagulation. The effects of magnetic separation of wastewater were investigated as variation of magnetic field strength and flow rate of wastewater.

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