• 한국지반신소재학회논문집
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• 제20권3호
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• pp.1-10
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• 2021

본 연구는 성토구조체 현장실험을 통해 포항 지역의 제3기 이암을 도로 노체 재료로 활용하기 위한 가능성을 검토하는 제시하는 것이다. 이 이암은 신생대 제 3기층인 연암퇴적층에 분포하고 있는 미고결화 암석으로 슬레이킹, 팽윤 현상, 전단강도 저하와 같은 물리적 문제와 산성배수라는 화학적 문제가 발생한다. 여러 복합적 문제 해결하기 위해 실내 배합 시험을 진행하였으며 제 3기 이암(90%)과 복합슬래그(제강 70%, 고로 30%)와 중화·코팅제 처리의 최적 배합 조건을 도출했으며, 이를 실증하기 위해 실제 규모의 도로 성토구조체를 시공하여 구간별 현장 시험을 진행했다. 사전처리구간은 최적 배합 조건 설계로 인해 안정이 유지되는 반면, 무처리구간은 자연 풍화가 빠르게 진행되어 구조적 문제 발생이 우려되었으며, 가적치구간은 중화·코팅제 효과가 확인됨에 따라 임시 적치 시기에 적용 가능함을 확인했다.

• 한국입자에어로졸학회지
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• 제17권2호
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• pp.21-27
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• 2021

We developed non-metallic electrodes that can replace metallic electrodes of the electrostatic precipitator(ESP) for the purpose of light weight, corrosion resistance, cost reduction. We manufactured three types of collection electrodes made of stainless steel (M), Carbon ink coating layer-Plastic sheet-Carbon ink coating layer (CPC), and Plastic sheet-Carbon ink coating layer-Plastic sheet (PCP). We studied the collection efficiency of a two-stage ESP using oil mist particles with and without collection stage by changing the flow rate, the material of collection electrode, and the applied voltage of the pre-charger module and the collection module. Here we measured concentrations of particles at diameters of 0.45 ㎛ (CMD; count median diameter) and 3.0 ㎛ (MMD : mass median diameter), as well as PM_2.5 and PM₁₀. As a result of the experiment, two-stage ESP had 22~25% higher collection efficiency in PM_2.5 than one-stage ESP at the same applied voltage. The difference in collection efficiency by varying the materials of collection electrodes was less than 5%. The weight of the non-metallic electrode was only one eighth the weight of the metal electrode. CPC electrode had a thickness of 0.27 mm, which was 1.5 times thinner than a thickness of PCP electrode, so when the flow rate increased, the CPC electrodes couldn't be kept at equal intervals due to the fluttering unlike PCP electrodes. In addition, the PCP-CPC collection module of the present experiment followed the theoretical efficiency based on Deutsch equation and Cochet's charging theory.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2001년도 춘계학술발표회 초록집
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• pp.14-14
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• 2001

Nitride films such as TiN, CrN etc. deposited on glass by PVD processes have been developed for many industrial applications. These nitride films deposited on glass were widely used for not only decorative and optical coatings but also wear and corrosion resistance coatings employed as dies and molds made of glass for the example of lens forming molds. However, the major problem of nitride coatings on glass by PVD process is non-uniform film owing to pin-hole and micro crack. It is estimated that nonuniform coating is influenced by a different surface energy between metal nitrides and glass due to binding states. In this work, therefore, for the evaluation of nucleation and growth mechanism of nitride films on glass TiN and CrN film were synthesized on glass with various nitrogen partial pressure by unbalanced magnetron sputtering. Prior to deposition, for the examination of relationship between surface energy and film microstructure plasma pre-treatment process was carried out with various argon to hydrogen flow rate and substrate bias voltage, duty cycle and frequency by using pulsed DC power supply. Surface energy owing to the different plasma pre-treatment was calculated by the measurement of wetting angle and surface conditions of glass were investigated by X-ray Photoelectron Spectroscopy(XPS) and Atomic Force Microscope(AFM). The microstructure change of nitride films on glass with increase of film thickness were analyzed by X-Ray Diffraction(XRD) and Scanning Electron Microscopy(SEM).

• 센서학회지
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• 제15권2호
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• pp.148-152
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• 2006

This paper describes the fabrication of SiCN microstructures for super-high temperature MEMS using photopolymerization of pre-ceramic polymer. In this work, polysilazane liquide as a precursor was deposited on Si wafers by spin coating, microstructured and solidificated by UV lithography, and removed from the substrate. The resulting solid polymer microstructures were cross-linked under HIP process and pyrolyzed to form a ceramic of withstanding over $1400^{\circ}C$. Finally, the fabricated SiCN microstructures were annealed at $1400^{\circ}C$ in a nitrogen atmosphere. Mechanical characteristics of the SiCN microstructure with different fabrication process conditions were evaluated. The elastic modules, hardness and tensile strength of the SiC microstructure implemented under optimum process condtions are 94.5 GPa, 10.5 GPa and 11.7 N/min, respectively. Consequently, the SiCN microstructure proposed in this work is very suitable for super-high temperature MEMS application due to very simple fabrication process and the potential possiblity of sophisticated mulitlayer or 3D microstructures as well as its good mechanical properties.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2010년도 추계학술대회 초록집
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• pp.114.1-114.1
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• 2010

A highly performed Pd-based hydrogen membrane has prepared successfully on a modified porous nickel support. The porous nickel support modified by impregnation method of $Al(NO_3)_3{\cdot}9H_2O$ (Aldrich Co.) over the nickel powder showed a strong resistance to hydrogen embrittlement and thermal stability. Plasma surface modification treatment was introduced as a pre-treatment process instead of conventional HCl wet activation. Ceramic barrier was coated on the external surface of the prepared nickel supports to prevent intermetallic diffusion and to enhance the affinity between the support and membrane. Palladium and copper were deposited at thicknesses of $4\mu}m$ and $0.5{\mu}m$, respectively, on a barrier-coated support by DC sputtering process. The permeation measurement was performed in pure hydrogen at $400^{\circ}C$. The single gas permeation of our membrane was two times higher than that of the previous membrane which do not have ceramic barrier.

• 공업화학
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• 제8권5호
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• pp.784-789
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• 1997

전도성 고분자인 폴리피롤(PPy)을 전해질로 하는 알루미늄(Al)고체전해 캐패시터를 제작하기 위하여 알루미늄 산화피막($Al_2O_3$) 위에 화학산화중합(CP)법으로 얇은 PPy층을 형성시키고, 이 층을 양극으로 이용하여 피롤(Py)을 전해산화중합(EP)시켰다. 캐패시터 특성에 영향을 미치는 중합조건을 조사한 결과, 지지전해질로서 sodium p-toluenesulfonate (TsONa)를 사용하고, 소자당 2.0~4.0 mA의 정전류를 인가, 전해중합 후 제작한 캐패시터의 전기적 특성 및 임피던스 특성이 가장 우수하였다.

• 한국염색가공학회지
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• 제28권4호
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• pp.271-279
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• 2016

This study deals with antibacterial properties of nylon fiber treated with glycidyltrimethylammonium chloride(GTAC) and silver nanoparticles(AgNPs). Nylon fibers were soaked into GTAC(2-30%, v:v) solution for 20 min. After sample was pre-drying at $80^{\circ}C$ for 10min and cured at $180^{\circ}C$ for 5min. The AgNPs coating was accomplished by soaking in silver colloid solution at $45^{\circ}C$ for 90min. The coated nylon fibers were characterized by scanning electron microscopy-energy dispersive spectroscopy(SEM-EDS). EDS analysis indicated that AgNPs and GTAC was attached on nylon fibers. The treated nylon fibers showed antimicrobial properties against Escherichia coli(ATCC 43895), Pseudomonas aeruginosa(ATCC 13388) and Staphylococcus aureus(ATCCBAA-1707).

• Mass Spectrometry Letters
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• 제3권1호
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• pp.25-28
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• 2012

Paint Spray is developed as a direct sampling ionisation method for mass spectrometric analysis of additives in polymer-based surface coatings. The technique simply involves applying an external high voltage (5 kV) to the wetted sample placed in front of the mass spectrometer inlet and represents a much simpler ionisation technique compared to those currently available. The capabilities of Paint Spray are demonstrated herein with the detection of four commercially available hindered amine light stabilisers; TINUVIN${(R)}$770, TINUVIN${(R)}$292, TINUVIN${(R)}$123 and TINUVIN${(R)}$152 directly from thermoset polyester-based coil coatings. Paint Spray requires no sample preparation or pre-treatment and combined with its simplicity requiring no specialised equipment makes it ideal for use by non-specialists. The application of Paint Spray for industrial use has significant potential as sample collection from a coil coating production line and Paint Spray ionisation could enable fast quality control screening at high sensitivity.

• 한국정밀공학회지
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• 제23권3호
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• pp.156-162
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• 2006

Direct fabrication of nano patterns has been studied employing a nano-stereolithography (NSL) process. The needs of nano patterning techniques have been intensively increased for diverse applications for nano/micro-devices; micro-fluidic channels, micro-molds. and other novel micro-objects. For fabrication of high-aspect-ratio (HAR) patterns, a thick spin coating of SU-8 process is generally used in the conventional photolithography, however, additional processes such as pre- and post-baking processes and expansive precise photomasks are inevitably required. In this work, direct fabrication of HAR patterns with a high spatial resolution is tried employing two-photon polymerization in the NSL process. The precision and aspect ratio of patterns can be controlled using process parameters of laser power, exposure time, and numerical aperture of objective lens. It is also feasible to control the aspect ratio of patterns by truncation amounts of patterns, and a layer-by-layer piling up technique is attempted to achieve HAR patterns. Through the fabrication of several patterns using the NSL process, the possibility of effective patterning technique fer various N/MEMS applications has been demonstrated.

• 한국근적외분광분석학회:학술대회논문집
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• 한국근적외분광분석학회 2001년도 NIR-2001
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• pp.1285-1285
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• 2001

For NIR measurements of papers normally diffuse reflectance accessories are used which can provide a large sampling area. The in-line process control FT-NIR spectrometer MATRIX-E enables the contactless measurement of paper samples of low silicone coat weights on label-stocks in a paper converting factory. For this study concentrations of silicone between 0 and 2 g/$m^2$ on various paper substrates were included in a quantitative method. The aim was to achieve an absolute value for the deviation from the target value of 1 g/$m^2$ during continuous movement of the paper with velocities around 400 numinute. Influences from the uncoated paper type due to supplier, color, opacity, area densities, pre-coating as well as different compounds of the agent silicone were investigated and it was found that all these papers can be represented in one PLS-model. Especially the fact that silicone as an element is present in clay coated papers is of no consequence to the measurements with MATRIX-E. Moreover during in-line installations the variation of the moisture contents in the moving paper due to variable machine velocities as well as the reflecting material of the cylinder have to be considered. It is shown that the result of the in-line calibration has the same prediction ability compared to lab scale results(Root Mean Square Error of Cross-Validation RMSECV = 0.034 g/$m^2$).