• 한국분말재료학회지
• /
• 제6권1호
• /
• pp.75-80
• /
• 1999

The formation of $n-TiO_2$ powder by oxidation of Ti-ethoxied vapor in a flat flame burner reactor maintained under 20 torr has been studied. The produced powder were characterized in terms of crystal structure, chemical composition by XRD and TEM. The results showed that the powder consisted of loose agglomerated anatase and rutile particles and their size were about 10 nm and 20 nm, respectively. In the course of synthesis, changes of the flame color were happened to each condition during heating up the bubbler. The flame color transition phenomena reveled that a critical precursor delivery rate was needed for the powder formation (obtainable powder yield). The critical precursor delivery rate was estimated by a simple function of the bubbler temperature and the carrier gas flow rate. The critical precursor delivery rate was reviewed as an important variable of the nanopowder synthesis.

• 한국세라믹학회지
• /
• 제33권4호
• /
• pp.441-447
• /
• 1996

Sb doped SnO2(ATO:Antinomy doped Tin Oxide) thin films were prepared by a DC magnetron spttuering method using oxide target and the deposition characteristics were investigated. The experimental conditions are as follows :Ar flow rate : 100 sccm oxygen flow rates ; 0-100 sccm deposition temperature ; 250 -40$0^{\circ}C$ DC sputter powder ; 150~550 W and sputtering pressure ; ; 2~7 mTorr. Deposition rate greatly depends not on the deposition temperature but on the reaction pressure oxygen flow rate and sputter power,. when the sputter powder is low ATO thin films with (110) preferred orientation are deposited. And when the sputter power is high (110) prefered orientation appeares with decreasing of oxygen flow rate and increasing of suputte-ring pressure.

• 한국분말재료학회지
• /
• 제10권2호
• /
• pp.123-128
• /
• 2003

$TiO_2$ nanopowder was synthesized by chemical vapor condensation (CVC) process and its photocatalytic property depending on microstructure was considered in terns of decomposition rate of organic compound. In order to control microstructure of $TiO_2$ nanopowder such as particle size and degree of agglomeration, precursor flow rate representing number concentration was changed as a process variable. In TEM observation, spherical $TiO_2$ nanoparticles with average size of 20 nm showed gradual increases in particle size and degree of agglomeration with increase of precursor flow rate. Also decomposition rate of organic compound increased with decreasing precursor flow rate. Thus, it was concluded that photocatalytic property was enhanced by targe surface area of disperse $TiO_2$ nanoparticles synthesized at lower precursor flow rate condition in CVC process.

• 한국분말재료학회지
• /
• 제2권2호
• /
• pp.120-134
• /
• 1995

The behavior of the flow about gas atomizers with a supersonic nozzle containing an under-expanded or over-expanded jet is very important with respect to performance and stability characteristics. Since detailed experiments are expensive, computational fluid mechanics have been applied recently to various relating flow field. In this study, a higher order upwind method with the 3rd order MUSCL type TVD scheme is used to solve the full Reynolds Wavier-Stokes equations. To delineate the purely exhaust jet effects, the melt flow is not considered. Comparison is made with some experimental data in terms of density fields. The influence of the exhaust-jet-to freestream pressure ratio and the effect of the protrusion length of the melt orifice are studied. The present study leads us to believe that the computational fluid mechanics should be considered as powerful tool in predicting the gas atomizer flows.

• 한국결정성장학회지
• /
• 제27권5호
• /
• pp.268-273
• /
• 2017

In this study, nickel hydroxide crystalline powders were synthesized by continuous reaction in the taylor fluid flow using nickel chloride, nickel sulphate and sodium hydroxide as raw materials and compared with those prepared by a conventional batch type reaction. The crystallinity of nickel hydroxide prepared by the Taylor fluid flow reaction was higher than that of nickel hydroxide obtained by batch reaction. The particle size of nickel hydroxide decreased about 2.5 to 3.6 times, and the specific surface area was increased.

• 콘크리트학회논문집
• /
• 제16권3호
• /
• pp.433-440
• /
• 2004

In order to improve the performance of concrete, generally, modern cements often incorporate several mineral admixtures. In this study, the experimental included the flow value, air content of mortar containing limestone powder and length change and compressive strength of mortar specimen immersed in sulfate solutions. From the experimental results, the limestone powder cement matrices improved the physical properties and sulfate resistance of cement matrices at $10\%$ replacement ratio of limestone powder. The $30\%$ replacement ratio of limestone powder was significantly deteriorated in sodium sulfate solution. Irrespective of fineness levels of limestone powder, length change and SDF of mortar specimens with only $10\%$ replacement was much superior to the other replacements.

• 한국공작기계학회:학술대회논문집
• /
• 한국공작기계학회 2002년도 춘계학술대회 논문집
• /
• pp.296-301
• /
• 2002

In this study, we investigated the machinability of machinable ceramics which were developed by a research lab. of Inha Univ., Korea. The effect of the nozzle scanning times, the size of patterns and compositions of BN in ceramics on the erosion depth of samples with no mask and samples with three different mask pattern in powder blasting of machinable ceramics. The blasting conditions were the impact angles 90$^{\circ}$, scanning times of noble up to 30 and the stand-off distances 100mm. The widths of mask pattern were 0.1mm, 0.5mm and 1 mm. The powder was alumina sharp particles, WA#600. The mass flow rate of powder during the erosion test was fixed constant at 150g/min and the blasting pressure of powder at 0.25Mpa

• 한국공작기계학회:학술대회논문집
• /
• 한국공작기계학회 2001년도 추계학술대회(한국공작기계학회)
• /
• pp.349-354
• /
• 2001

In this study, we investigated the effect of the impacting ang1e of particles, the scanning times and the stand-off distance on the surface roughness and the weight-loss rate of samples with no mask, and the wall profile and overetching of samples with different mask pattern in powder blasting of soda-lime glass. The varying parameters were the different impact angles between 50$^{\circ}$ and 90$^{\circ}$, scanning times of nozz1e up to 40 and the stand-off distances 70mm and 100mm. The widths of mask pattern were 0.2mm, 0.5mm and 1mm. The powder was alumina sharp particles, WA#600. The mass flow rate of powder during the erosion test was fixed constant at 175g/min and the blasting pressure of powder at 0.2MPa

• 한국건축시공학회:학술대회논문집
• /
• 한국건축시공학회 2016년도 춘계 학술논문 발표대회
• /
• pp.38-39
• /
• 2016

In this research, the possibility of wasted refractory powder pulverized from refractory block as an expansive admixture and additional alkaline stimulant for class two and three blast furnace slag cements (BSC) was assessed with its high content of free CaO or free MgO. As the replacement ratios of wasted refractory powder and blast furnace slag were increased, flow and air content were decreased, while unit volume weight was increased under same conditions. Compressive strength of mortar was increased with increased replacement ratio of wasted refractory powder, especially, in the case of class three BSC, the highest compressive strength was obtained when wasted refractory powder was replaced 10 %.

• 한국건축시공학회:학술대회논문집
• /
• 한국건축시공학회 2019년도 춘계 학술논문 발표대회
• /
• pp.205-206
• /
• 2019

This study investigated the fluidity and compressive strength properties of blast furnace slag based non-cement paste containing ferronickel slag powder to evaluate the possibility of use in for cement replacement materials. As a result, the fluidity of non-cement paste showed a higher flow as the mixing ratio of ferronickel slag powder increased. The compressive strengths similar to those of the non-cement paste using only blast furnace slag powder were obtained when 5 and 10% of ferronickel slag powder were used.