• 제목/요약/키워드: Powder Explosion

검색결과 108건 처리시간 0.025초

액중 전기선폭발법으로 제조된 구리 나노콜로이드의 특성 평가 (Evaluation of Cu nano-colloid prepared by electrical wire explosion in liquid phase)

  • 윤재철;양상선;유지훈
    • 한국입자에어로졸학회지
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    • 제6권1호
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    • pp.37-46
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    • 2010
  • Cu nano-colloid was prepared by wire electric explosion process under de-mineralized water and anhydrous ethanol. To control the properties of Cu nano-colloid, experimental conditions such as diameter of Cu wire and applied voltage were changed. The optimal Cu nano-colloid was prepared when the 0.1mm diameter of Cu wire with the applied voltage of 2000 V was used. The shape of Cu particles in colloid was spherical and the XRD result revealed that the phase of Cu particles was cubic phase. About 20nm Cu nanoparticles with high crystallinity were successfully prepared using wire explosion process under anhydrous ethanol and they showed more than 100 hours dispersion stability.

Synthesis and Spark-plasma Sinetring of Nanoscale Al/alumina Powder by Wire Electric Explosion Process

  • Kim, Ji-Soon;Kim, H. T.;Illyin, A. P.;Kwon, Young-Soon
    • 한국분말재료학회지
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    • 제12권5호
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    • pp.351-356
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    • 2005
  • Nanoscale Al powder with thin layer of alumina was produced by Wire Electric Explosion (WEE) process. Spark-Plasma Sintering (SPS) was performed for the produced powder to confirm the effectiveness of SPS like so-called 'surface-cleaning effect' and so on. Crystallite size and alumina content of produced powder varied with the ratio of input energy to sublimation energy of Al wire ($e/e_s$): Increase in ($e/e_s$) resulted in the decrease of crystallite size and the increase of alumina content. Shrinkage curve during SPS process showed that the oxide surface layer could not be destroyed near the melting point of Al. It implied that there was not enough or no spark-plasma effect during SPS for Al/Alumina powder.

노후 분말소화기의 폭발사고 원인과 예방대책에 관한 분석 (Analysis of the Precautionary Measures and Causes on Explosion Accidents of a Old Dry Chemical Powder Extinguisher)

  • 이의평
    • 한국화재소방학회논문지
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    • 제26권3호
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    • pp.91-99
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    • 2012
  • 분말소화기를 조작하거나 해체하는 과정 중에 아주 드물게 사상자가 발생하는 경우가 있다. 부식된 분말소화기는 조작 중 또는 해체(폐기)과정 중에 폭발하면 로켓과 같이 위쪽으로 솟아오르면서 소화기 조작자나 해체과정 중인 사람의 머리나 가슴, 목 부위 등을 쳐서 사상사고를 발생하게 한다. 이 논문에서는 분말소화기파열사고사례를 알아본 후, 파열사고의 원인과 파열로 인한 반동력, 예방대책에 대해 알아보았다. 소화기 파열사고의 예방대책으로 훈련이나 교육에 부식된 소화기의 사용 자제, 부식된 소화기에 대한 위험성 교육 및 홍보, 기설치 가압식분말소화기에 파열위험성 표시, 내용연수 표시 의무화, 일정기간 경과 소화기에 대한 수압검사 제도의 도입 검토, 폐소화기 회수시스템 구축, 폐소화기의 재활용시스템 구축, 노후소화기관련 상담창구 운영 등을 제안하였다.

전기폭발(wire explosion)에 의한 나노분말 제조 (Synthesis of Nanosized Powders by Wire Explosion)

  • 조주현;임근희;이홍식
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2005년도 제36회 하계학술대회 논문집 C
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    • pp.2057-2059
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    • 2005
  • Silver nanosized powder have been synthesized using wire explosion technology. The discharge system of 10kw (10uF, 20kV, 0.5 shots/s) was set up for mass production of 300g/h. The high purity silver powder was collected and separated by cyclone and fabric filters.

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전기도금법과 전기선폭발법을 이용한 Al-Cu 합금 나노분말제조 (The Fabrication of Al-Cu Alloy Nano Powders by a New Method Combining Electrodeposition and Electrical Wire Explosion)

  • 박제신;서창열;장한권;이재천;김원백
    • 한국분말재료학회지
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    • 제13권3호
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    • pp.187-191
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    • 2006
  • Al-Cu alloy nano powders were produced by the electrical explosion of Cu-plated Al wires. The composition and phase of the alloy could be controlled by varying the thickness of Cu deposit on Al wire. When the Cu layer was thin, Al solid solution and $CuAl_2$ were the major phases. As the Cu layer becomes thicker, Al diminished while $Al_4Cu_9$ phase prevailed instead. The average particle size of Al-Cu nano powders became slightly smaller from 63 nm to 44 nm as Cu layer becomes thicker. The oxygen content of Al-Cu powder decreased linearly with Cu content. It is well demonstrated that the electrodeposition combined with wire explosion could be simple and economical means to prepare variety of alloy and intermetallic nano powders.

액중 전기선 폭발 공정을 이용한 Pt/alloy 하이브리드 나노입자의 제조 및 그 특성 (Synthesis of Pt/alloy Nanoparticles by Electrical Wire Explosion in Liquid Media and its Characteristics)

  • 구혜영;윤중열;양상선;이혜문
    • 한국입자에어로졸학회지
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    • 제8권2호
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    • pp.83-88
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    • 2012
  • The electrical wire explosion process in liquid media is promising for nano-sized metal and/or alloy particles. The hybrid Pt/Fe-Cr-Al and Pt/Ni-Cr-Fe nanoparticles for exhaust emission control system are synthesized by electrical wire explosion process in liquid media. The alloy powders have spherical shape and nanometer size. According to the wire component, while Pt/Fe-Cr-Al nanoparticles are shown the well dispersed Pt on the Fe-Cr-Al core particle, Pt/Ni-Cr-Fe nanoparticles are shown the partially separated Pt on the Ni-Cr-Fe core particle. Morphologies and component of two kinds of hybrid nano catalyst particles were characterized by transmission electron microscope and energy dispersive X-ray spectroscopy analysis.

도금선재의 전기선폭발을 이용한 Cu-Zn 합금 나노분말 제조 (Fabrication of Cu-Zn Alloy Nano Powders by Wire Explosion of Electrodeposited Wires)

  • 김원백;박제신;서창열;이재천;오용준;문정일
    • 한국분말재료학회지
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    • 제14권1호
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    • pp.38-43
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    • 2007
  • Cu-Zn alloy nano powders were fabricated by the electrical explosion of Zn-electroplated Cu wire along with commercial brass wire. The powders exploded from brass wire were composed mainly of ${\alpha},{\beta},\;and\;{\gamma}$ phases while those from electroplated wires contained additional Zn-rich phases as ${\varepsilon}$, and Zn. In case of Zn-elec-troplated Cu wire, the mixing time of the two components during explosion might not be long enough to solidify as the phases of lower Zn content. This along with the high vapor pressure of Zn appears to be the reason for the observed shift of explosion products towards the high-Zn phases in electroplated wire system.

전기선폭발법에 의한 Cu-Ni-P 합금 나노 분말 제조 (Cu-Ni-P Alloy Nano Powders Prepared by Electrical Wire Explosion)

  • 김원백;박제신;서창열;이재천;김정환;오용준
    • 한국분말재료학회지
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    • 제14권2호
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    • pp.108-115
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    • 2007
  • Cu-Ni-P alloy nano powders were fabricated by the electrical explosion of electroless Ni plated Cu wires. The effect of applied voltage on the explosion was examined by applying pulse voltage of 6 and 28 kV, The estimated overheating factor, K, were 1.3 for 6 kV and 2.2 for 28 kV. The powders produced with pulse voltage of 6 kV were composed of Cu-rich solid solution, Ni-rich solid solution, and $Ni_3P$ phase. While, those produced with 28 kV were complete Cu-Ni-P solid solution and small amount of $Ni_3P$ phase. The initial P content of 6.5 at.% was reduced to 2-3 at.% during explosion due to its high vapour pressure.

전기선 폭발법으로 제조된 Al-Cu 합금 나노분말을 이용한 다공성 나노 입자 제조 (Fabrication of Porous Nano Particles from Al-Cu Alloy Nano Powders Prepared by Electrical Wire Explosion)

  • 박제신;김원백;서창열;안종관;김병규
    • 한국분말재료학회지
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    • 제15권3호
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    • pp.234-238
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    • 2008
  • Al-Cu alloy nano powders have been produced by the electrical explosion of Cu-plated Al wire. The porous nano particles were prepared by leaching for Al-Cu alloy nano powders in 40wt% NaOH aqueous solution. The surface area of leached powder for 5 hours was 4 times larger than that of original alloy nano powder. It is demonstrated that porous nano particles could be obtained by selective leaching of alloy nano powder. It is expected that porous Cu nano powders can be applied for catalyst of SRM (steam reforming methanol).

전기선폭발법으로 제조된 텅스텐 분말의 산소 조성이 방전플라즈마소결 거동에 미치는 영향 (Effect of Oxygen Content in the Tungsten Powder Fabricated by Electrical Explosion of Wire Method on the Behavior of Spark-Plasma Sintering)

  • 김철희;이성;김병기;김지순
    • 한국분말재료학회지
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    • 제21권6호
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    • pp.447-453
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    • 2014
  • Effect of oxygen content in the ultrafine tungsten powder fabricated by electrical explosion of wire method on the behvior of spark plasma sintering was investigated. The initial oxygen content of 6.5 wt% of as-fabricated tungsten powder was reduced to 2.3 and 0.7 wt% for the powders which were reduction-treated at $400^{\circ}C$ for 2 hour and at $500^{\circ}C$ for 1h in hydrogen atmosphere, respectively. The reduction-treated tungsten powders were spark-plasma sintered at $1200-1600^{\circ}C$ for 100-3600 sec. with applied pressure of 50 MPa under vacuum of 0.133 Pa. Maximun sindered density of 97% relative density was obtained under the condition of $1600^{\circ}C$ for 1h from the tungsten powder with 0.7 wt% oxygen. Sintering activation energy of $95.85kJ/mol^{-1}$ was obtained, which is remarkably smaller than the reported ones of $380{\sim}460kJ/mol^{-1}$ for pressureless sintering of micron-scale tungsten powders.