• Title/Summary/Keyword: Porosity improvement

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Corrosion Behavior of TiN Ion Plated Steel Plate(II)-Effects of Ni and Ni/Ti interlayers- (TiN 이온 플레이팅한 강판의 내식성에 관한 연구 (II)-Ni 및 Ni-Ti 하지코팅의 영향-)

  • 한전건;연윤모;홍준희
    • Journal of the Korean institute of surface engineering
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    • v.25 no.2
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    • pp.82-89
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    • 1992
  • The effect of interlayer coating of Ni and Ti on corrosion behavior was studied in TiN ion plated steel plate. Interlayer coating was carried out in a single and bi-layer to a various thickness combination prior to final TiN coating of $2\mu\textrm{m}$. Corrosion behavior was evaluated by anodic polarization test in 1N H2SO4 as well as salt spray test. Porosity of each coating was also tested by using SO2 test. Corrosion resistance was improved with increasing the thickness of Ni interlayer coating and Ni-Ti interlayer coating markedly enhanced the corrosion resistance. Ni/Ti interlayer coating of $2\mu\textrm{m}$/2$\mu\textrm{m}$ prior to $2\mu\textrm{m}$ TiN coating decreased the corrosion current density of active range by an order of 4 and that of passive range by an order of 1. This improvement was associated with the retardation of corrosive agent penetration with increasing coating thickness and inherent corrosion resistance of Ni and Ti interlayers, Ni/Ti interlayers coating were also very effective in improvement of corrosion resistance under salt atmosphere.

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Evaluation of Injection capabilities of a biopolymer-based grout material

  • Lee, Minhyeong;Im, Jooyoung;Chang, Ilhan;Cho, Gye-Chun
    • Geomechanics and Engineering
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    • v.25 no.1
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    • pp.31-40
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    • 2021
  • Injection grouting is one of the most common ground improvement practice to increase the strength and reduce the hydraulic conductivity of soils. Owing to the environmental concerns of conventional grout materials, such as cement-based or silicate-based materials, bio-inspired biogeotechnical approaches are considered to be new sustainable and environmentally friendly ground improvement methods. Biopolymers, which are excretory products from living organisms, have been shown to significantly reduce the hydraulic conductivity via pore-clogging and increase the strength of soils. To study the practical application of biopolymers for seepage and ground water control, in this study, we explored the injection capabilities of biopolymer-based grout materials in both linear aperture and particulate media (i.e., sand and glassbeads) considering different injection pressures, biopolymer concentrations, and flow channel geometries. The hydraulic conductivity control of a biopolymer-based grout material was evaluated after injection into sandy soil under confined boundary conditions. The results showed that the performance of xanthan gum injection was mainly affected by the injection pressure and pore geometry (e.g., porosity) inside the soil. Additionally, with an increase in the xanthan gum concentration, the injection efficiency diminished while the hydraulic conductivity reduction efficiency enhanced significantly. The results of this study provide the potential capabilities of injection grouting to be performed with biopolymer-based materials for field application.

HVOF Spray Coating of Co-alloy(T800) for the Improvement of durability of High Speed Spindle (초고속 회전체의 내구성향상을 위한 Co-alloy(T800)의 초고속 용사코팅)

  • Cho, Tong-Yul;Yoon, Jae-Hong;Kim, Kil-Su;Youn, Suk-Jo;Back, Nam-Ki;Park, Byung-Chul;Chun, Hui-Gon
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.15 no.6
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    • pp.32-37
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    • 2006
  • Micron size Co-alloy(T800) powder was coated on Inconel 718 by HVOF thermal spraying for the studies of the improvement of durability of high speed spindle by using Taguchi program for the parameters of spray distance, flow rates of hydrogen and oxygen and powder feed rate. The optimal coating process was determined by the studies of coating properties such as micro-structure, porosity, surface roughness and micro hardness. Friction and wear behaviors of coatings were investigated by sliding wear test at room temperature and $1000^{\circ}F(538^{\circ}C)$. At both room temperature and $538^{\circ}C$ the sliding wear debris and friction coefficients of the coating were drastically reduced compared with the surface of non-coated parent material. This shows that Co-alloy powder coating is highly recommendable for the durability improvement surface coating of high speed air-bearing spindle. At high temperature wear traces and friction coefficients of both coating and non-coating were drastically reduced compared with those of room temperature since the brittle oxides were formed easily on the surface, and the brittle oxide phases were attrited by the reciprocating sliding wear according to the complicated mixed wear mechanisms These oxide particles, partially melts and the melts play role as lubricant and reduce the wear and friction coefficient. This also shows that Co-alloy powder coating is highly recommendable far the durability improvement surface coating on the surface vulnerable to frictional heat such as high speed spindles.

Enhancement of Interfacial Adhesion of Epoxy/Red Mud Nanocomposites Produced by Acidic Surface Treatment on Red Mud (Red Mud의 산처리에 의한 에폭시/Red Mud 나노복합재료의 계면 결합력 향상)

  • Park, Soo-Jin;Seo, Dong-Il;Lee, Jae-Rock;Kim, Dae-Su
    • Polymer(Korea)
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    • v.25 no.4
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    • pp.587-593
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    • 2001
  • In this work, red mud (RM) was chemically modified by 0.1, 1, and 5 M H3PO4 solution to prepare epoxy/RM nanocomposites. The effect of chemical treatment on pH, acid-base values, specific surface area, and porosity of RM surface was analyzed. To estimate the mechanical interfacial properties of epoxy/RM nanocomposites, the critical stress intensity factor (K$_{IC}$) was measured. From the experimental results, it was clearly revealed that the porosity, specific surface area, and acid values of RM surface were developed as the increase of the treatment concentration due to the increase of acidic functional group, including hydroxyl group on RM surface. The mechanical interfacial properties of epoxy/treated-RM nanocomposites were higher than those of epoxy/RM as-received due to an improvement of interfacial bonding between basic matrix and RM surface.

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A Study on Improvement of Fracture Toughness of $\beta-SiC-ZrB_2$Composites ($\beta-SiC-ZrB_2$ 복합체의 파괴인성 증진연구)

  • Shin Yong-Deok;Ju, Jin-Young;Yoon, Se-Won;Hwang, Chul;Song, Joon-Tae
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.291-294
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    • 1999
  • The effect of AI$_2$O$_3$+Y$_2$O$_3$additives on fracture toughness of $\beta$-SiC-ZrB$_2$composites by hot-pressed sintering were Investigated. The $\beta$-SiC-ZrB$_2$ ceramic composites were hot-presse sintered and annealed by adding 1, 2, 3wt% AI$_2$O$_3$+Y$_2$O$_3$(6:4wt%) powder as a liquid forming additives at 195$0^{\circ}C$ for 4h. In this microstructures, no reactions were observed between $\beta$-SiC and ZrB$_2$, and the relative density Is over 90.79% of the theoretical density and the porosity decreased with increasing AI$_2$O$_3$+Y$_2$O$_3$ contents. Owing to crack deflection and crack bridging of fracture toughness mechanism, the fracture toughness showed the highest of 5.5328MPa . m$^{1}$2/ for composites added with 2wt% AI$_2$O$_3$+Y$_2$O$_3$ additives at room temperature. But the standard deviation of fracture toughness of specimens decreased with increasing AI$_2$O$_3$+Y$_2$O$_3$ contents and showed the highest of 0.8624 for composite tilth 1wt%, AI$_2$O$_3$+Y$_2$O$_3$additives.

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Threshold Subsoil Bulk Density for Optimal Soil Physical Quality in Upland: Inferred Through Parameter Interactions and Crop Growth Inhibition

  • Cho, Hee-Rae;Han, Kyung-Hwa;Zhang, Yong-Seon;Jung, Kang-Ho;Sonn, Yeon-Kyu;Kim, Myeong-Sook;Choi, Seyeong
    • Korean Journal of Soil Science and Fertilizer
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    • v.49 no.5
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    • pp.548-554
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    • 2016
  • Optimal range of soil physical quality to enhance crop productivity or to improve environmental health is still in dispute for the upland soil. We hypothesized that the optimal range might be established by comparing soil physical parameters and their interactions inhibiting crop growth. The parameter identifying optimal range covered favorable conditions of aeration, permeability and root extension. To establish soil physical standard two experiments were conducted as follows; 1) investigating interactions of bulk density and aeration porosity in the laboratory test and 2) determining effects of soil compaction and deep & conventional tillage on physical properties and crop growth in the field test. The crops were Perilla frutescens, Zea mays L., Solanum tuberosum L. and Secale cereael. The saturated hydraulic conductivity, bulk density from the root depth, root growth and stem length were obtained. Higher bulk density showed lower aeration porosity and hydraulic conductivity, and finer texture had lower threshold bulk density at 10% aeration bulk density. Reduced crop growth by subsoil compaction was higher in silt clay loam compared to other textures. Loam soil had better physical improvement in deep rotary tillage plot. Combined with results of the present studies, the soil physical quality was possibly assessed by bulk density index. Threshold subsoil bulk density as the upper value were $1.55Mg\;m^{-3}$ in sandy loam, $1.50Mg\;m^{-3}$ in loam and $1.45Mg\;m^{-3}$ in silty clay loam for optimal soil physical quality in upland.

Friction Behavior of High Velocity Oxygen Fuel (HVOF) Thermal Spray Coating Layer of Nano WC-Co Powder

  • Cho, T.Y.;Yoon, J.H.;Kim, K.S.;Fang, W.;Joo, Y.K.;Song, K.O.;Youn, S.J.;Hwang, S.Y.;Chun, H.G.
    • Journal of the Korean institute of surface engineering
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    • v.40 no.4
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    • pp.170-174
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    • 2007
  • High Velocity Oxygen Fuel (HVOF) thermal spray coating of nano size WC-Co powder (nWC-Co) has been studied as one of the most promising candidate for the possible replacement of the traditional hard plating in some area which causes environmental and health problems. nWC-Co powder was coated on Inconel 718 substrates by HVOF technique. The optimal coating process obtained from the best surface properties such as hardness and porosity is the process of oxygen flow rate (FR) 38 FMR, hydrogen FR 57 FMR and feed rate 35 g/min at spray distance 6 inch for both surface temperature $25^{\circ}C\;and\;500^{\circ}C$. In coating process a small portion of hard WC decomposes to less hard $W_2C$, W and C at the temperature higher than its decomposition temperature $1,250^{\circ}C$ resulting in hardness decrease and porosity increase. Friction coefficient increases with increasing coating surface temperature from 0.55-0.64 at $25^{\circ}C$ to 0.65-0.76 at $500^{\circ}C$ due to the increase of adhesion between coating and counter sliding surface. Hardness of nWC-Co is higher or comparable to those of other hard coatings, such as $Al_2O_3,\;Cr,\;Cr_2O_3$ and HVOF Tribaloy 400 (T400). This shows that nWC-Co is recommendable for durability improvement coating on machine components such as high speed spindle.

Exploration of shockwaves on polymeric membrane physical properties and performance

  • Lakshmi, D. Shanthana;Saxena, Mayank;Ekambaram, Shivakarthik;Sivaraman, Bhalamurugan
    • Membrane and Water Treatment
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    • v.12 no.1
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    • pp.43-49
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    • 2021
  • The Commercial polymeric membranes like Polysulfone (PSF), Polyvinylidene difluoride (PVDF) and Polyacrylonitrile (PAN) which are an integral part of water purification investigation were chosen for the shockwave (SW) exposure experiment. These membranes were prepared by blending polymer (wt. %) / DMF (solvent) followed by phase-inversion casting technique. Shockwaves are generated by using Reddy Tube lab module (Table-top Shocktube) with range of pressure (1.5, 2.5 and 5 bar). Understanding the changes in membrane before and after shock wave treatment by parameters, i.e., pure water flux (PWF), rejection (%), porosity, surface roughness (AFM), morphology (SEM) and contact angle which can significantly affect the membrane's performance. Flux values PSf membranes shows increase, 465 (pristine) to 524 (1.5wt%) LMH at 50 Psi pressure and similar enhancement was observed at 100Psi (625 to 696 LMH). Porosity also shows improvement from 73.6% to 76.84% for 15wt% PSf membranes. It was observed that membranes made of polymers such as PAN and PSF (of high w/w %) exhibits some resistance against shockwaves impact and are stable compared to other membranes. Shockwave pressure of up to 1.5 bar was sufficient enough to change properties which are crucial for performance. Membranes exposed to a maximum pressure of 5 bar completely scratched the surface and with minimum pressure of 1.5bar is optimum enough to improve the water flux and other parameters. Initial results proved that SW may be suitable alternative route to minimize/control membrane fouling and improve efficiency.

Improvement in Mechanical Properties of AZ91D Mg-Alloy through Thixomolding Process (틱소몰딩 공정을 이용한 AZ91D Mg합금의 기계적 성질 증대)

  • Shin, Dong-Soo;Chung, Sung-Chong
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.21 no.4
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    • pp.593-600
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    • 2012
  • Thixomolding of Mg-alloy is a semi-solid injection molding process utilizing thixotropic phenomenon. Using this process, higher strength, thinner wall section and tighter tolerance without porosity are obtained. It has been applied for production of near-net-shape magnesium component. To design optimal thixomolding process of Mg-alloy part, molding conditions such as slurry temperature, mold temperature and injection time should be determined properly. Selection of these parameters has been dependent upon engineers' experience and intuitiveness. In this paper, to improve mechanical properties of the thixomolded product, optimal selection of process variables such as injection velocity, barrel temperature and die temperature in the process has been studied through microstructural analysis and Taguchi method. Performance of the process is verified through experiments.

Pre Calendering Effect after Primary Coating in Double Coating System(1)

  • Kim, Byeong-Soo;Bousfield Douglas W.
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2006.04a
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    • pp.124-131
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    • 2006
  • It is well known that smoother surface in substrate for coating or converting can obtain better results. Generally paper substrate is taking machine calendar process in papermaking system to give more uniformity and to get better coating runnability. This paper was prepared to find better idea for obtaining smoother surface after precalendering precoated paper as a substrate of double coating system. It was shown precalendering had effect on roughness improvement for precoating layer but was difficult to say it was effected to supercalendering results for double coating. The porosity and ink evaluation with precalendered double coated paper is needed to identify more essential clue for precalendering effect.

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