• Title/Summary/Keyword: Porosity Technique

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Interpretation of Limestone Provenance, Materials and Making Characteristics for Lime-Soil Mixture on Tomb Barrier of the Yesan Mokri Site in Joseon Dynasty (조선시대 예산 목리유적 회격묘의 재질 및 제작특성과 석회의 산지 해석)

  • Lee, Chan Hee;Cho, Ji Hyun;Kim, Jiyoung
    • Journal of Conservation Science
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    • v.32 no.4
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    • pp.471-490
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    • 2016
  • This study investigated provenance of raw materials and making technique of lime-based materials used in the tomb barriers of the Yesan Mokri tombs from Joseon dynasty on the basis of analysis to material characteristics and physical properties. In the barrier materials, dry density and porosity are the highest value ($1.82g/cm^3$) and the lowest value (25.20%) in the south wall of No. 1 tomb, respectively. Dry density and porosity are inversely proportional in all barrier materials, but unconfined compressive strength, which is the highest value of $182.36kg/cm^2$ in the No. 2 tomb, does not show an interrelation with porosity and density. Mineral components in the lime-soil mixtures of the tomb barrier are mainly quartz, feldspar, mica and calcite about 200 to $600{\mu}m$ size with yellowish brown matrix. Hydrotalcite and portlandite are detected in the lime mixture, and kaolinite in the soils. The lime materials of the tomb barrier occurred in large quantities weight loss and variable endothermic peaks caused by decarbonization reaction of $CaCO_3$ in the range from 600 to $800^{\circ}C$ in thermal analysis. Making temperature of lime for the tomb barrier is presumed approximately about $800^{\circ}C$ based on the occurrences, compositions and thermal analysis. The tomb barriers are revealed to very wide composition ranges of major elements and loss-on-ignition (22.5 to 33.6 wt.%) owing to mixture of the three materials (lime, sand and clay). It is interpreted that low quality construction technique was applied as the limes are very heterogeneous mixture with aggregates, and curing of the lime was poorly processed in the tomb barriers. Possible limestone sources are distributed in many areas around the Mokri site where limestone conformation and quarries for commercial production are found within Yesan and Hongseong areas. Therefore, we estimated that raw materials were possibly supplied from the local mines near the Mokri site.

Development of Biomimetic Scaffold for Tissue Engineering (조직공학을 위한 생체모사용 스캐폴드 개발)

  • Park, Su-A;Lee, Jun-Hee;Kim, Wan-Doo
    • Elastomers and Composites
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    • v.44 no.2
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    • pp.106-111
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    • 2009
  • Tissue engineering is a research field for artificial substitutes to improve or replace biological functions. Scaffolds play a important role in tissue engineering. Scaffold porosity and pore size provide adequate space, nutrient transportation and cell penetration throughout the scaffold structure. Scaffold structure is directly related to fabrication methods. This review will introduce the current technique of 3D scaffold fabrication for tissue engineering. The conventional technique for scaffold fabrication includes salt leaching, gas foaming, fiber bonding, phase seperation, melt moulding, and freeze drying. These conventional scaffold fabrication has the limitations of cell penetration and interconnectivity. In this paper, we will present the solid freeform fabrication (SFF) such as stereolithography (SLA), selective laser sintering (SLS), and fused deposition modeling (FDM), and 3D printing (3DP).

Vacuum Carburizing System for Powdered Metal Parts & Components

  • Kowakewski, Janusz;Kucharski, Karol
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1018-1021
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    • 2006
  • Powdered metal parts and components may be carburized successfully in a vacuum furnace by combining carburizing technology $VacCarb^{TM}$ with a hi-tech control system. This approach is different from traditional carburizing methods, because vacuum carburizing is a non-equilibrium process. It is not possible to set the carbon potential as in a traditional carburizing atmosphere and control its composition in order to obtain a desired carburized case. This paper presents test results that demonstrate that vacuum carburizing system $VacCarb^{TM}$ carburized P.M. materials faster than traditional steel with acceptable results. In the experiments conducted, PM samples with the lowest density and open porosity showed a dramatic increase in the surface carbon content up to 2.5%C and a 3 times deeper case. Currently the boost-diffusion technique is applied to control the surface carbon content and distribution in the case. In the first boost step, the flow of the carburizing gas has to be sufficient to saturate the austenite, while avoiding soot deposition and formation of massive carbides. To accomplish this goal, the proper gas flow rate has to be calculated. In the case of P.M. parts, more carbon can be absorbed by the part's surface because of the additional internal surface area created by pores present in the carburized case. This amount will depend on the density of the part, the densification grade of the surface layer and the stage of the surface. "as machined" or "as sintered". It is believed that enhanced gas diffusion after initial evacuation of the P.M. parts leads to faster carburization from within the pores, especially when pores are open . surface "as sintered" and interconnected . low density. A serious problem with vacuum carburizing is delivery of the carbon in a uniform manner to the work pieces. This led to the development of the different methods of carburizing gas circulation such as the pulse/pump method or the pulse/pause technique applied in SECO/WARWICK's $VacCarb^{TM}$ Technology. In both cases, each pressure change may deliver fresh carburizing atmosphere into the pores and leads to faster carburization from within the pores. Since today's control of vacuum carburizing is based largely on empirical results, presented experiments may lead to better understanding and improved control of the process.

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A Study on Application of Warm-Mix Quiet Pavement Using Fine-Size Aggregate (소입경 골재를 이용한 중온 저소음 아스팔트 포장의 적용 연구)

  • Jo, Shinhaeng;Baek, Yujin;Kim, Nakseok
    • Journal of the Society of Disaster Information
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    • v.9 no.1
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    • pp.56-64
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    • 2013
  • The study examines the quiet pavement using fine-size aggregates and warm-mix technique to reduce traffic noise. In order to evaluate the quality of pavement, mix design and laboratory tests were carried out. Test results showed that using 10mm aggregates can reduce the cantabro loss compared with 13mm aggregates due to increase contact area between aggregates. Mixing and compaction temperatures of warm mix quiet pavement should be determined by gyratory compactor test because it is used high viscosity asphalt binder. Using warm-mix additive could reduce compaction temperature by about $15^{\circ}C$. Noise measurement and permeability tests were conducted at the test road for evaluation of the field performance. All of quiet pavements meet the standard of permeability and have sufficient porosity. Noise reduction of the quiet pavement using fine-size aggregates is more effective than that using 13mm aggregates. In particular, the effect of noise reduction was noticeable at low speeds.

Automated quality characterization of 3D printed bone scaffolds

  • Tseng, Tzu-Liang Bill;Chilukuri, Aditya;Park, Sang C.;Kwon, Yongjin James
    • Journal of Computational Design and Engineering
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    • v.1 no.3
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    • pp.194-201
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    • 2014
  • Optimization of design is an important step in obtaining tissue engineering scaffolds with appropriate shapes and inner micro-structures. Different shapes and sizes of scaffolds are modeled using UGS NX 6.0 software with variable pore sizes. The quality issue we are concerned is the scaffold porosity, which is mainly caused by the fabrication inaccuracies. Bone scaffolds are usually characterized using a scanning electron microscope, but this study presents a new automated inspection and classification technique. Due to many numbers and size variations for the pores, the manual inspection of the fabricated scaffolds tends to be error-prone and costly. Manual inspection also raises the chance of contamination. Thus, non-contact, precise inspection is preferred. In this study, the critical dimensions are automatically measured by the vision camera. The measured data are analyzed to classify the quality characteristics. The automated inspection and classification techniques developed in this study are expected to improve the quality of the fabricated scaffolds and reduce the overall cost of manufacturing.

An Ultrasonic Pattern Recognition Approach to Welding Defect Classification (용접 결함 분류를 위한 초음파 형상 인식 기법)

  • Song, Sung-Jin
    • Journal of the Korean Society for Nondestructive Testing
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    • v.15 no.2
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    • pp.395-406
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    • 1995
  • Classification of flaws in weldments from their ultrasonic scattering signals is very important in quantitative nondestructive evaluation. This problem is ideally suited to a modern ultrasonic pattern recognition technique. Here brief discussion on systematic approach to this methodology is presented including ultrasonic feature extraction, feature selection and classification. A stronger emphasis is placed on probabilistic neural networks as efficient classifiers for many practical classification problems. In an example probabilistic neural networks are applied to classify flaws in weldments into 3 classes such as cracks, porosity and slag inclusions. Probabilistic nets are shown to be able to exhibit high performance of other classifiers without any training time overhead. In addition, forward selection scheme for sensitive features is addressed to enhance network performance.

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Laboratory tests for studying the performance of grouted micro-fine cement

  • Aflaki, Esmael;Moodi, Faramarz
    • Computers and Concrete
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    • v.20 no.2
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    • pp.145-154
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    • 2017
  • In geological engineering, grouting with Portland cement is a common technique for ground improvement, during which micro-fine cement is applied as a slurry, such that it intrudes into soil voids and decreases soil porosity. To determine the utility and behavior of cements with different Blaine values (index of cement particle fineness) for stabilization of fine sand, non-destructive and destructive tests were employed, such as laser-ray determination of grain size distribution, and sedimentation, permeability, and compressive strength tests. The results of the experimental study demonstrated a suitable mix design for the upper and lower regions of the cement-grading curve that are important for grouting and stabilization. Increasing the fineness of the cement decreased the permeability and increased the compressive strength of grouted sand samples considerably after two weeks. Moreover, relative to finer (higher Blaine value) or coarser (lower Blaine value) cements, cement with a Blaine value of $5,100cm^2/g$ was optimal for void reduction in a grouted soil mass. Overall, study results indicate that cement with an optimum Blaine value can be used to satisfy the designed geotechnical criteria.

Carbon rich fly ash and their nanostructures

  • Salah, Numan;Habib, Sami S.;Khan, Zishan H.;Alshahrie, Ahmed;Memic, Adnan;Al-ghamdi, Attieh A.
    • Carbon letters
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    • v.19
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    • pp.23-31
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    • 2016
  • Carbon rich fly ash was recently reported to have compositions that are ideal for use as a precursor and catalyst for carbon nanotube growth. This fly ash powder is mostly composed of pure carbon, predominantly present as sp2. In this work, the effect of sonication time on the morphology and structural properties of carbon rich fly ash particles is reported. The obtained results show that ultrasound treatment is an effective tool for producing ultrafine particles/fragments with higher porosity, which might be suitable for the adsorption of gasses. Moreover, carbon nanoparticles (CNPs) of this fly ash were produced in parallel using the ball milling technique, and were evaluated as reinforcements for epoxy based composites. These CNPs have almost spherical shapes with particle sizes of around 30 nm. They were found to have strong C=O carbonyl group bonds, which might be generated during the ball milling process. The tensile testing results of a fly ash CNP reinforced epoxy composite showed significant improvements in the mechanical properties, mainly in the stiffness of the polymer. The stiffness value was increased by around 23% of that of neat epoxy. These CNPs with chemically active groups might also be useful for other applications.

Comparative Reliability of Nondestructive Testing for Weld: Water Wall Tube in Thermal Power Plant Boiler Case Study (용접부 비파괴 검사의 신뢰성 비교: 화력 발전소의 보일러 수냉벽 배관 사례연구)

  • Choi, Chang Deok;Lim, Ik Sung
    • Journal of Applied Reliability
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    • v.18 no.3
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    • pp.240-249
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    • 2018
  • Purpose: The purpose of this research is to find which technique, between the PAUT (Phased array ultrasonic test) that has been used widely in practice and RT (Radiographic test) that was used widely in the past, has the higher reliability as a non-destructive testing of welding points in water wall tubes. Methods: To evaluated the reliability of non-destructive testing, eleven test pieces that were fabricated intentionally, which have the most frequently occurred defect types in water wall tubes and then both the PAUT and RT were performed on those eleven test pieces to compare their reliability. Results: The differences of type of defect, length are occurred due to the characteristics of nondestructive testing. The RT could not detect the lack of fusion defect type in specimen #4 and #8 while PAUT could not detect the lateral crack and 1 mm size small porosity in specimen #11. Conclusion: It is concluded that applying both the RT and PAUT result the best reliability rather than applying only one test method, if it is possible, in nondestructive testing of weld water wall tube in thermal power plant boiler case.

Analysis of Microsegregation in Fe-Cr-Ni Weld Metal (Fe-Cr-Ni강 용접금속부의 미세편석에 관한 해석)

  • 박준민;박종민;안상곤;이창희;윤의박
    • Journal of Welding and Joining
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    • v.16 no.5
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    • pp.56-66
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    • 1998
  • During solidification or welding of alloys, the solute redistribution brings out microsegregation. The microsegregation causes the formation of non-equilibrium second phases, shrinkage and porosity degrading mechanical/chemical properties Therefore, it has been required to predict microsegregation quantitatively. To predict the degree of microsegregation, more exact and appropriate computer simulation technique has been actively used during last two decades. To predict the degree of microsegregation in weld metal, an advanced two dimensional model was suggested. In the new model, both primary and secondary arm regions were defined for the analysis region. The growth in the primary arm regina was assumed to be a planar for effective calculation. Especially, for the growth of a secondary arm, a simple and effective mathematical function was established to show the growing pattern, the solute diffusion in the solid phase was calculated by finite difference method (FDM). The solid-liquid interface movement was considered to be in local equilibrium state. The experiments for welding of 310S stainless steel were carried out in order to examined the reasonability and feasibility of this model. The concentration profiles of the solute predicted by this model were compared with those obtained from experimental works.

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