• 제목/요약/키워드: Pore structure analysis

검색결과 295건 처리시간 0.029초

종이의 Pore 특성 측정 기법의 비교 (Comparison of pore analysis techniques of the paper)

  • 남기영;정순기;원종명
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2007년도 추계학술발표논문집
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    • pp.179-186
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    • 2007
  • The best way to understand paper properties is to study paper structure. Paper is composed solid materials (pulp and other additives) and air three-dimensionally, it's important to understand pore structure of the paper. There are several method to analysis pore structure of the paper. Mercury intrusion technique is frequently used for the characterization of the porous paper, giving access to parameters such as pore size and pore distribution. But some researchers indicated mercury intrusion distorts the structure due to application of high pressure. So this paper suggest new analysis technique to pore structure of the paper. New pore analysis technique with SEM does not require high pressure, gives good resolution and measures pore structure.

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종이의 기공 특성 측정 기법의 비교 (Comparison of Characterization Techniques of the Pore in Paper Sheet)

  • 원종명;남기영;정순기
    • 펄프종이기술
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    • 제39권4호
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    • pp.1-6
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    • 2007
  • Paper is a composite consisted of various solid materials including pulp, filler and other additives. The pore is also one of components consisting the paper structure. Thus the characterization of pore structure of paper is very helpful in the understanding the structural properties of paper. Mercury intrusion technique is frequently used for the characterization of the porous paper, giving access to parameters such as pore size and pore distribution. But some researchers pointed out the problem that the distortion of the pore structure can be occurred by the application of high pressure during mercury intrusion. Thus in this study, we tried to evaluate the potential of SEM and image analysis method as means for analyzing pore structure of the paper. The new pore analysis technique with SEM and image analysis does not require the application of high pressure, and gave better relation between the measured pore characteristics and the bulk of sheet than mercury intrusion method.

Realistic pore structure of Portland cement paste: experimental study and numerical simulation

  • Ma, Hongyan;Li, Zongjin
    • Computers and Concrete
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    • 제11권4호
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    • pp.317-336
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    • 2013
  • In this study, the pore structure of Portland cement paste is experimentally characterized by MIP (mercury intrusion porosimetry) and nitrogen adsorption, and simulated by a newly developed status-oriented computer model. Cement pastes with w/c=0.3, 0.4 and 0.5 at ages from 1 day to 120 days are comprehensively investigated. It is found that MIP cannot generate valid pore size distribution curves for cement paste. Nevertheless, nitrogen adsorption can give much more realistic pore size distribution curves of small capillary pores, and these curves follow the same distribution mode. While, large capillary pores can be effectively characterized by the newly developed computer model, and the validity of this model has been proved by BSE imaging plus image analysis. Based on the experimental findings and numerical simulation, a hypothesis is proposed to explain the formation mechanism of the capillary pore system, and the realistic representation of the pore structure of hydrated cement paste is established.

셰일 저류층 내 공극 구조 연구를 위한 표면 밀링 (Surface Milling for the Study of Pore Structure in Shale Reservoirs)

  • 박선영;최지영;이현석
    • 광물과 암석
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    • 제33권4호
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    • pp.419-426
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    • 2020
  • 비전통 저류층에서 에너지 자원의 회수율을 높이기 위해서는 저류층 내의 미세 공극 형태와 연결도 등을 포함하는 공극 구조 연구가 필수적이다. 본 연구에서는 셰일 저류층 내 나노스케일의 공극 구조 연구에 적합한 조건과 방법을 찾기 위해 집속 이온 빔 시스템(Focused Ion Beam, FIB)과 이온 밀링 시스템(Ion Milling System, IMS)을 이용하여 분석을 진행하였다. 셰일 저류층 내 공극 구조 연구를 위해 리아드 분지에서 획득된 A-068 시추공의 시료를 사용하였다. 각 시료마다 특성이 다르기 때문에 시료 전처리 방법과 조건을 달리하여 최적의 조건을 찾았고 FE-SEM을 이용하여 공극 이미지를 획득하였다. 연구 결과 국소 부위의 공극구조를 관찰하기 위해서는 FIB를 사용하여 시표 표면을 밀링 후 바로 공극 이미지를 얻는 것이 효율적이고 반면에 넓은 면적을 단시간에 밀링하여 여러 공극 구조를 관찰하기 위해서는 IMS를 이용해야 한다는 것을 확인했다. 특히 탄산염 광물 함량이 높고 강도가 큰 암석에 대해서는 FIB보다는 IMS를 활용하여 밀링을 수행해야 공극 구조 관찰이 가능하다는 사실이 밝혀졌다. 본 연구를 통해 셰일 저류층 내 공극 구조 관찰을 위한 방법이 정립되었으며 향후 이를 이용한 셰일 가스 저류층 시료 분석을 통해 공극의 크기나 형태가 셰일가스 회수 증진에 미치는 영향을 밝힐 수 있을 것이다.

고온 가열 시멘트 페이스트의 3D 영상화 및 세공구조 변화 분석에 관한 연구 (A Study on the 3D Imaging of High Temperature Heating Cement Paste and the Analysis of Variation of the Pore Structure)

  • 김민혁;이건철
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2020년도 가을 학술논문 발표대회
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    • pp.147-148
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    • 2020
  • In case of high temperature damage such as fire, the durability of concrete is reduced due to the collapse of internal pore tissue. Therefore, in this paper, we are going to analyze the pore structure of cement paste hardening agent using MIP analysis and build up 3D data produced using X-ray CT tomography. The test specimen is made of cement paste from W/C 0.4. As the temperature of heating increased, the amount of air gap and the diameter of air gap in cement paste increased. It is judged that the air gap structure inside cement collapsed due to the evaporation of the hydrate, gel count, capillary water, etc. inside the cement due to the high temperature.

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모직물의 수분율 변화와 구조에 따른 기공도 및 수분전달 특성변화 (Change of Porosity and Water Vapour Transport Properties of Wool Fabrics by the Change of Moisture Regain and Fabric Structure)

  • 김동옥;나미희;김은애
    • 한국의류학회지
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    • 제23권6호
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    • pp.820-828
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    • 1999
  • The purpose of this study was to investigate the changes of pore area and water vapour transport by the changes of moisture regain and fabric structure of wool fabrics, As specimens 4 worsted wool fabrics were used. The pore area were measured by image analysis method and dinamic vapour transport and water reisitance was determined by clothing-environment-body modelling system. The pore area was changed by the moisture regain of wool fabrics. The change of pore area was influenced by the yarn twist thread count and cover factor and the weave type. The water vapour transport was changed by the moisture regain. The change of water vapour transport was influenced by the change of pore aree which was determined by image analysis.

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화상분석법을 이용한 하이브리드 콘크리트의 공극구조 특성 및 투수성 평가 (Estimation of Pore Structure Characteristic and Permeability of Hybrid Concrete by Image Analysis Method)

  • 장봉진;전범준;홍영호;배종오;임홍범
    • 한국도로학회논문집
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    • 제17권1호
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    • pp.59-67
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    • 2015
  • PURPOSES : In this study, an image analysis method is used to evaluate the pore structure characteristics and permeability of hybrid concrete. METHODS : The binder weight of hybrid concrete is set to $400kg/m^3$, $370kg/m^3$, and $350kg/m^3$, and for each value of binder weight, the pore structure and permeability of concrete mixture is evaluated. The permeability of hybrid concrete is evaluated using a rapid chloride penetration test(RCPT). RESULTS : The concrete pore structure characteristics of hybrid concrete reveals that as the binder weight is reduced, the entrained air is reduced and the entrapped air is increased. The permeability of the hybrid concrete for all values was measured to be below 1000 C, which indicates a "Very Low" level of permeability relative to the evaluation standard of KS F 2711. Additionally, as the binder weight is decreased, there is a significant increase in the permeability of chloride ions. CONCLUSIONS : In this study, the pore structure characteristics of hybrid concrete at different binder weights shows that as the binder weight is reduced, the entrained air is reduced and the entrapped air is increased. Consequently, chloride ion penetration resistance of the hybrid concrete is diminished. As a result, it is expected that this will reduce the concrete's durability.

Review of Soil Structure Quantification from Soil Images

  • Chun, Hyen-Chung;Gimenez, Daniel;Yoon, Sung-Won;Park, Chan-Won;Moon, Yong-Hee;Sonn, Yeon-Kyu;Hyun, Byung-Keun
    • 한국토양비료학회지
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    • 제44권3호
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    • pp.517-526
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    • 2011
  • Soil structure plays an important role in ecological system, since it controls transport and storage of air, gas, nutrients and solutions. The study of soil structure requires an understanding of the interrelations and interactions between the diverse soil components at various levels of organization. Investigations of the spatial distribution of pore/particle arrangements and the geometry of soil pore space can provide important information regarding ecological or crop system. Because of conveniences in image analyses and accuracy, these investigations have been thrived for a long time. Image analyses from soil sections through impregnated blocks of undisturbed soil (2 dimensional image analyses) or from 3 dimensional scanned soils by computer tomography allow quantitative assessment of the pore space. Image analysis techniques can be used to classify pore types and quantify pore structure without inaccurate or hard labor in laboratory. In this paper, the last 50 years of the soil image analyses have been presented and measurements on various soil scales were introduced, as well. In addition to history of image analyses, a couple of examples for soil image analyses were displayed. The discussion was made on the applications of image analyses and techniques to quantify pore/soil structure.

알칼리 자극제 혼입 고로슬래그 미분말의 공극구조 및 미소수화열 분석 (Pore Structure and Heat of Microhydration Analysis of Blast Furnace Slag Containing Alkaline Activator)

  • 박지웅;박희곤;김우재;이건철
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2017년도 추계 학술논문 발표대회
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    • pp.20-21
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    • 2017
  • In this study, fundamental properties by pore structure and heat of microhydration test were determined. As a result of pore structure analysis, BS(AA) specimen showed showed the maximum peak value of significantly lower incremental intrusion than the maximum peak value of incremental intrusion at smaller pore size than that of BS. As a result of heat of microhydration test, the maximum heating value was in the order of OPC > BS > BS(AA), and initial drying shrinkage and compressive strength of BS(AA) were expected to be improved.

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콘크리트의 공극 특성에 관한 실험적 연구 (An Experimental Study on the Concrete Pore Structure Property)

  • 이문환;정미경;오세출;서치호
    • 한국구조물진단유지관리공학회 논문집
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    • 제3권4호
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    • pp.179-189
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    • 1999
  • This study attempts to propose an evaluation considering the property of concrete pore which affects the deterioration of neutralization and the rebar resistance of concrete. Understanding pore property of concrete in using extent, for practical using of concrete manufacturing condition. basic quality property and durability estimation etc, the results of the experiment are as follows. 1) The result of analysis pore property of every specimen with the method of area ratio, in limitation of $10^{-6}{\sim}10^{-5}m$, the pore distribution ratio was maximum. It was high value as W/C was increased and the unit cement content was decreased. 2) In case of using admixture. the volume of pores was some increased as variation of mixing content. In high W/C range, it was very increased compared with plain concrete. 3) Concerned with compressive strength and volume of pores in hardened concrete, it is possible compressive strength estimation using the property of concrete pores. 4) Direct measurement of concrete pore property is difficult. the valuation of the dynamic modulus of elasticity using ultrasonic wave velocity was available. 5) Quantitatively evaluation of concrete structure durability by past result of pore distribution estimation, and it can be estimative scale of property study on the concrete materials.

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