• Proceedings of the Korea Concrete Institute Conference
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• 2008.11a
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• pp.685-688
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• 2008

Concrete is strong on the compressive property, but weak on the tensile and flexural properties. To improve these problems, the reinforcing bar is used in concrete. But porous concrete with steel fiber has a weak point when exposed to air, because porous concrete has the vast continuous void on its inside and steel fiber is easily rusted by air. For these reasons, this study investigated the void ratio, compressive strength, bending strength and bending toughness as steel fiber mixing ratio and target void ratio. From test results, actual void ratio and strength properties increased as the mixing ratio of steel fiber increase. In case the mixing ratio of steel fiber over the fixed ratio, strength is decreased. And from the toughness evaluation, compared to the porous concrete which isn't mixed with steel fiber, the deflection variation efficiency is remarkably improved. Consequently we can confirm the possibility of porous concrete with steel fiber for the secondary product and pavement material to improve strength and bending resistance efficiency.

• Maxillofacial Plastic and Reconstructive Surgery
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• v.35 no.1
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• pp.13-17
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• 2013

Purpose: This study evaluated the capability of bone formation of silk fibroin particles coated with hydroxyapatites (HA/SF), as bone graft material when put into the calvarial defect of rats. Methods: Twenty Sprague Dawley rats were used for this study and round shaped defects were formed in the center of parietal bones (diameter: 8.0 mm). The defect was filled with (1) HA/SF (experimental group), or (2) left as a vacant space (control group). The animals were sacrificed at 4 or 8 weeks, postoperatively. The specimens were decalcified and stained with Masson's trichrome for histomorphometric analysis. Results: The average of new bone formation was $33.18{\pm}3.10%$ in the experimental group and $20.49{\pm}5.79%$ in the control group at 4 weeks postoperatively. That was $42.52{\pm}7.74%$ in the experimental group and $25.50{\pm}7.31%$ in the control group at 8 weeks postoperatively. The difference between the groups was significantly higher at both 4 weeks and 8 weeks postoperatively (P<0.05). Conclusion: The rat calvarial defect was successfully repaired by HA/SF graft. The HA/SF graft showed more new bone formation compared with the unfilled control.

• KSBB Journal
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• v.27 no.3
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• pp.151-156
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• 2012

Lactic acid is an important product arising from the anaerobic fermentation by lactic acid bacteria (LAB). It is used in the pharmaceutical, cosmetic, chemical, and food industries as well as for biodegradable polymer and green solvent production. The poly lactic acid (PLA) is an important material for bio-plastic manufacturing process. For PLA production by new LAB, we screened LAB isolates from shellfish. A total of 28 LAB were isolated from various shellfishes. They were all Gram positive, oxidase and catalase negative. Based on API 50CHL kit, 7 strains among the 28 isolates were identified as Lactobacillus plantarum, 6 strains as Lactobacillus delbrueckii, 5 strains as Leuconostoc mesenteroides, 3 strains as Lactobacillus brevis, 2 strains as Lactococcus lactis, 1 strain as Lactobacillus salivarius, 1 strain as Lactobacillus paracasei, 1 strain as Lactobacillus pentosus, 1 strain as Lactobacillus fermentum and 1 strain as Pediococcus pentosaceu. Also, we examined the amount of total lactic acid produced by these new strains by HPLC analysis with Chiralpak MA column. One strain E-3 from Mytilus edulis was indentified as Lactobacillus plantarum and found to produce 20.0 g/L of D-form lactic acid from 20 g/L of dextrose. Further studies are underway to increase the D-lactic acid production by E-3.

• Advances in Traditional Medicine
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• v.7 no.1
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• pp.51-64
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• 2007

Mucus is an aqueous gel complex with a constitution of about 95% water, high molecular weight glycoprotein (mucin), lipid, salts etc. Mucus appears to represent a significant barrier to the absorption of some compounds. Natural mucoadhesive agent was isolated and purified from the aqueous extract of the seeds of prosopis pallida (PP). Formulated tablet with the isolated material by wet granulation method. Some natural edible substances are in consideration for candidates as mucoadhesive agents to claim more effective controlled drug delivery as an alternative to the currently used synthetic mucoadhesive polymers. Subjected the materials obtained from natural source i.e. PP and standard synthetic substance, sodium carboxymethyl cellulose for evaluation of mucoadhesive property by various in vitro and in vivo methods. Through standard dissolution test and a model developed with rabbit, evaluated in vitro controlled release and bioadhesive property of theophylline formulation. Mucoadhesive agent obtained from PP showed good mucoadhesive potential in the demonstrated in vitro and in viνo models. The results suggest that the mucoadhesive agent showed controlled release properties by their application, substantially. In order to assess the gastrointestinal transit time in vivo, a radio opaque X-ray study performed in healthy rabbit testing the same controlled release formulation with and without bioadhesive polymer. Plasma levels of theophylline determined by the HPLC method and those allowed correlations to the in vitro mucoadhesive study results. Better correlation found between the results in different models. PP may acts as a better natural mucoadhesive agent in the extended drug delivery system.

• The Journal of Korean Academy of Prosthodontics
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• v.41 no.1
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• pp.61-70
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• 2003

The purpose of this study was to investigate the contact angles and wettability of conventional dental stones and improved dental stones and newly developed dental stones on several impression materials. Materials included in this study were several dental stones and newly developed dental stone ; 2 type III stones (Snow Rock, New Diastone), 6 type IV stones(Crystal Rock, Vel Mix, Fuji Rock, Tuff Rock, Resin Rock and newly developed dental stone) and 1 type V stone (Die Keen). Contact angles on the impression materials were measured with contact angle measuring device. Ten specimens for each material, total 180 specimens were made on void entrapment model. The two impression materials (Handae, GC) were used to produce 9 groups of die stone casts form void entrapment model. Voids in the stone casts were counted under a stereoscopic microscope. The grad for the reproduction ability of each materials on the void entrapment model was calculated from the casts by one examiner. From the experiment, the following results were obtained : 1. The newly developed stones showed smallest contact angle. Type III dental stone had larger contact angles than type IV and V stones. Contact angle was much affected by the impression materials. 2. Resin containing die materials such as Tuff Rock and Resin Rock had smallest void number than any other groups. 3. In comparing reproduction parameters, Tuff Rock and Resin Rock presented superior results, while Vel Mix showed lowest reproduction ability.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.33 no.4
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• pp.1337-1347
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• 2013

The parametric analysis on ultimate behavior of buried cylindrical GFRP(Glass Fiber Reinforced Polymer) septic tank was presented. Two kinds of F.E. analysis model(soil-spring model and 3D full model) was constructed. The ultimate behavior of septic tank was investigated according to the size of stiffened steel ring and properties of underground soil. Ramberg-Osgood model and Druker-Prager model were used for material nonlinear characteristics of GFRP septic tank and soil, respectively. The diameter and thickness of stiffened steel ring inside septic tank, elastic modulus and internal friction angle of soil were selected for parametric variables. The ultimate behavior of septic tank, load-displacement, axial and hoop strain, were calculated and investigated.

• Steel and Composite Structures
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• v.35 no.1
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• pp.77-92
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• 2020

The present paper outlined a procedure for geometrically nonlinear dynamic analysis of functionally graded graphene platelets-reinforced (GPLR-FG) nanocomposite cylinder subjected to mechanical shock loading. The governing equation of motion for large deformation problems is derived using meshless local Petrov-Galerkin (MLPG) method based on total lagrangian approach. In the MLPG method, the radial point interpolation technique is employed to construct the shape functions. A micromechanical model based on the Halpin-Tsai model and rule of mixture is used for formulation the nonlinear functionally graded distribution of GPLs in polymer matrix of composites. Energy dissipation in analyses of the structure responding to dynamic loads is considered using the Rayleigh damping. The Newmark-Newton/Raphson method which is an incremental-iterative approach is implemented to solve the nonlinear dynamic equations. The results of the proposed method for homogenous material are compared with the finite element ones. A very good agreement is achieved between the MLPG and FEM with very fine meshing. In addition, the results have demonstrated that the MLPG method is more effective method compared with the FEM for very large deformation problems due to avoiding mesh distortion issues. Finally, the effect of GPLs distribution on strength, stiffness and dynamic characteristics of the cylinder are discussed in details. The obtained results show that the distribution of GPLs changed the mechanical properties, so a classification of different types and volume fraction exponent is established. Indeed by comparing the obtained results, the best compromise of nanocomposite cylinder is determined in terms of mechanical and dynamic properties for different load patterns. All these applications have shown that the present MLPG method is very effective for geometrically nonlinear analyses of GPLR-FG nanocomposite cylinder because of vanishing mesh distortion issue in large deformation problems. In addition, since in proposed method the distributed nodes are used for discretization the problem domain (rather than the meshing), modeling the functionally graded media yields to more accurate results.

• Journal of the Korean Chemical Society
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• v.54 no.6
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• pp.761-765
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• 2010

Poly (N,N-dimethylacrylamide) is very useful in various fields due to its remarkable properties, such as water solubility and biocompatibility. This study used N,N-dimethylacrylamide with the cross-linker EGDMA (ethylene glycol dimethacrylate), HEMA (2-hydroxyethyl methacrylate), MMA (methyl methacrylate), NVP (N-vinyl-2-pyrrolidone) and the initiator AIBN (azobisisobutyronitrile) for copolymerization. Measurement of the physical properties of the copolymerized polymer showed that the water content was 36 - 42%, refractive index was 1.433 - 1.426 and visible ray transmittance 90 - 91% while the oxygen permeability showed a distribution between 13.1 and $21.29{\times}10^{-11}(cm^2/sec)$ ($mlO_2/mL{\times}mmHg$). The measurement showed that the increased amount of oxygen permeability of the copolymer measured using the polarographic method range between 11.0% and 80.5%. Based on the results of this study, the produced copolymer is suitable for use as a material to high oxygen permeability hydrogel lenses.

• Proceedings of the International Microelectronics And Packaging Society Conference
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• 2000.04a
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• pp.43-55
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• 2000

In traditional electronic packages the die and the substrate are interconnected with fine wire. Wire bonding technology is limited to bond pads around the peripheral of the die. As the demand for I/O increases, there will be limitations with wire bonding technology. Flip chip technology eliminates the need for wire bonding by redistributing the bond pads over the entire surface of the die. Instead of wires, the die is attached to the substrate utilizing a direct solder connection. Although several steps and processes are eliminated when utilizing flip chip technology, there are several new problems that must be overcome. The main issue is the mismatch in the coefficient of thermal expansion (CTE) of the silicon die and the substrate. This mismatch will cause premature solder Joint failure. This issue can be compensated for by the use of an underfill material between the die and the substrate. Underfill helps to extend the working life of the device by providing environmental protection and structural integrity. Flux residues may interfere with the flow of underfill encapsulants causing gross solder voids and premature failure of the solder connection. Furthermore, flux residues may chemically react with the underfill polymer causing a change in its mechanical and thermal properties. As flip chip packages decrease in size, cleaning becomes more challenging. While package size continues to decrease, the total number of 1/0 continue to increase. As the I/O increases, the array density of the package increases and as the array density increases, the pitch decreases. If the pitch is decreasing, the standoff is also decreasing. This paper will present the keys to successful flip chip cleaning processes. Process parameters such as time, temperature, solvency, and impingement energy required for successful cleaning will be addressed. Flip chip packages will be cleaned and subjected to JEDEC level 3 testing, followed by accelerated stress testing. The devices will then be analyzed using acoustic microscopy and the results and conclusions reported.

• Proceedings of the International Microelectronics And Packaging Society Conference
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• 2000.04a
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• pp.9-15
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• 2000

Flip chip assembly on organic substrates using ACAs have received much attentions due to many advantages such as easier processing, good electrical performance, lower cost, and low temperature processing compatible with organic substrates. ACAs are generally composed of epoxy polymer resin and small amount of conductive fillers (less than 10 wt. %). As a result, ACAs have almost the same CTE values as an epoxy material itself which are higher than conventional underfill materials which contains lots of fillers. Therefore, it is necessary to lower the CTE value of ACAs to obtain more reliable flip chip assembly on organic substrates using ACAs. To modify the ACA composite materials with some amount of conductive fillers, non-conductive fillers were incorporated into ACAs. In this paper, we investigated the effect of fillers on the thermo-mechanical properties of modified ACA composite materials and the reliability of flip chip assembly on organic substrates using modified ACA composite materials. For the characterization of modified ACAs composites with different content of non-conducting fillers, dynamic scanning calorimeter (DSC), and thermo-gravimetric analyzer (TGA), dynamic mechanical analyzer (DMA), and thermo-mechanical analyzer (TMA) were utilized. As the non-conducting filler content increased, CTE values decreased and storage modulus at room temperature increased. In addition, the increase in tile content of filler brought about the increase of Tg$^{DSC}$ and Tg$^{TMA}$. However, the TGA behaviors stayed almost the same. Contact resistance changes were measured during reliability tests such as thermal cycling, high humidity and temperature, and high temperature at dry condition. It was observed that reliability results were significant affected by CTEs of ACA materials especially at the thermal cycling test. Results showed that flip chip assembly using modified ACA composites with lower CTEs and higher modulus by loading non-conducting fillers exhibited better contact resistance behavior than conventional ACAs without non-conducting fillers.ers.