• 제목/요약/키워드: Polishing and coating

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Technology of selective absorber coatings on solar collectors using black chromium+3 sulfate acid on substrates (흑색 황산3가크롬을 이용한 태양열 흡열판 선택흡수막 도금기술)

  • Ohm, Tae-In;Yeo, Woon-Tack;Kim, Dong-Chan
    • Journal of the Korean Solar Energy Society
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    • v.33 no.3
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    • pp.27-35
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    • 2013
  • One of the most important factors that have a large influence on performance of the solar water heater system is performance of the solar collector, more detailedly, coating technology on the surface of the solar collector, which can provide high solar absorptance and low emittance. The core of the coating technology is to coat solar selective surfaces. In this study, various performance experiments are carried out using $Cr_2(SO_4)_3{\cdot}15H_2O$ coating technology. Here, IGBT(Insulated Gate Bipolar Transistor) of 5000A-15V was used as the surface processing rectifier which can stably output power and also can control voltage and current. The plating solution mainly contains black chrome$^{+3}$ concentration, H-y Conductivity, N-u Complex, NF Additive and NC-2 Wetter. Before applying the black chrome coating on the copper plate, optimal conditions are provided by using various preprocessing methods such as removal of fat, activation, electrolytic polishing, nickel strike, copper sulfate plating and bright neckel plating, and then the automatic continuous coating experiment are performed according to plating time and cathode current density. In the experiment, after the removal of fat, chemical polishing, nickel strike and activation processes as the preprocessing methods, the black chrome coating was performed in a plate solution temperature of $28^{\circ}C$ and a cathode current density of $18A/cm^2$ for 90 seconds. The thickness of chrome and nickel on the coated plate is $0.389{\mu}m$, $159{\mu}m$ respectively. As a result of the coating experiment, it showed the most excellent performance having a high solar absorptance of 98% and a low emittance of $5{\pm}1%$ when the black chrome surface had a thickness of $0.398{\mu}m$.

Growth of Graphene on Electro-polished Copper Foil by Thermal CVD

  • Jin, Xiaozhan;Kim, Sung-Jin;Seo, Eun-Kyoung;Boo, Doo-Wan;Lee, Jung-Ah;Hwang, Chan-Yong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.410-410
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    • 2012
  • The continuous monolayer graphene was synthesized on electro-polished copper foil. Electro-polishing sticks off the coating layer of copper foil, which prevents the continuous graphene growth. The quality of continuous graphene is dependent on roughness of copper foil. Copper foil roughness could be controlled by changing polishing condition. The effects of working voltage (4-6 V) and time (30-70 sec) for electro-polishing were systematically examined. The change of surface roughness was checked with AFM.

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Technical Overview on the Electron Backscattered Diffraction Sample Preparation

  • Kim, Dong-Ik;Kim, Byung-Kyu;Kim, Ju-Heon
    • Applied Microscopy
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    • v.45 no.4
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    • pp.218-224
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    • 2015
  • A technical overview on the various sample preparation methods for electron backscattered diffraction (EBSD) analysis is carried out. The mechanical polishing with colloidal silica finish, electro-chemical polishing, dual layer coating and ion beam milling are introduced for the common sample preparation methods for EBSD observation and some issues that are frequently neglected by the common EBSD users but should be considered to get a reliable EBSD data are discussed. This overview would be especially helpful to the people who know what EBSD technique is but do not get a reliable EBSD data because of difficulties in sample preparation.

Development of Superfinishing Machine to Polish the Inner Surfaces of Aircraft Hydraulic Oil Reservoirs (항공기 유압유 저장조 내면연마를 위한 슈퍼피니싱 장치 개발에 관한 연구)

  • Choi, Su Hyun;Kong, Kwang Ju;Cho, Young Tae
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.8
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    • pp.110-116
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    • 2020
  • Aircraft hydraulic oil reservoirs made with aluminum 7075 have an anodized coating to enable airtightness and corrosion resistance. To maintain a stable oil pressure, the internal surface roughness of the reservoir should be less than approximately 0.2 ㎛. To this end, precision polishing must be performed. However, ensuring the processing quality is challenging, as most polishing operations are performed manually, owing to which, the inner surface roughness is not uniform, and the product quality is irregular. Therefore, we developed a special superfinishing machine to realize the efficient inner polishing of an aircraft hydraulic oil reservoir, by using an abrasive film to improve the process throughput and uniformity. In the experiment involving the superfinishing of an anodized aluminum 7075 cylinder specimen by using the proposed machine, a higher surface roughness than that achieved in the repetitive manual polishing process could be realized.

Study for Improvement of Laser Induced Damage of 1064 nm AR Coatings in Nanosecond Pulse

  • Jiao, Hongfei;Cheng, Xinbing;Lu, Jiangtao;Bao, Ganghua;Zhang, Jinlong;Ma, Bin;Liu, Huasong;Wang, Zhanshan
    • Journal of the Optical Society of Korea
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    • v.17 no.1
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    • pp.1-4
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    • 2013
  • For the conventionally polished fused silica substrate, an around 100 nm depth redeposition polishing layer was formed on the top of surface. Polishing compounds, densely embedded in the redeposition polishing layer were the dominant factor that limited the laser induced damage threshold (LIDT) of transmission elements in nanosecond laser systems. Chemical etching, super-precise polishing and ion beam etching were employed in different ways to eliminate these absorbers from the substrate. After that, Antireflection (AR) coatings were deposited on these substrates in the same batch and then tested by 1064 nm nano-pulse laser. It was found that among these techniques only the ion beam etching method, which can effectively remove the polishing compound and did not induce extra absorbers during the disposal process, can successfully improve the LIDT of AR coatings.

Diamond Conditioner Wear Characterization for a Copper CMP Process

  • Boruckia, L.;Zhuang, Y.;Kikuma, R.;Rikita, N.;Yamashita, T.;Nagasawa, K.;Lee, H.;Sun, T.;Rosales-Yeomans, D.;Philipossian, A.;Stout, T
    • Transactions on Electrical and Electronic Materials
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    • v.8 no.1
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    • pp.15-20
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    • 2007
  • Conditioner wear, copper polish rates, pad temperature and coefficient of friction (COF) are measured for two novel Mitsubishi Materials Corporation designs during an extended wear and polishing test. Both designs are coated with a $Teflon^{TM}$ film to reduce substrate wear and chemical attack. Using optical interferometry, changes in the coating that result in gradual changes in diamond exposure are measured. Theories of the COF, conditioning, and polishing are applied to explain the observed performance differences between the designs.

Acid Pickling/polishing of AZ31 Magnesium Alloy

  • Fazal, Basit Raza;Moon, Sungmo
    • Journal of the Korean institute of surface engineering
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    • v.49 no.3
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    • pp.231-237
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    • 2016
  • This article reports a new chemical bath for preparing a mirror-like surface of AZ31 Mg alloy. In order to find an appropriate chemical polishing solution, four different acidic solutions of sulphuric acid, nitric acid, acetic acid and a specially designed mixture of nitric acid and acetic acid were investigated in view of the changes in surface appearance, roughness and dissolution rate of AZ31 Mg alloy. The surface scales on AZ31 Mg alloy were readily removed by all the acidic solutions, but a reflective surface was produced only by etching in the specially designed solution, and only after a specific etching time. The surface roughness increased with etching time in sulphuric acid, nitric acid, and acetic acid, but it lowered after a specific etching time in the specially designed mixture of nitric acid and acetic acid. Dissolution rate of the alloy in the specially designed mixture of nitric acid and acetic acid appeared to be more than twice than that in separate nitric acid or acetic acid. In this work, we recommend the mirror-like surface of AZ31 Mg alloy obtained by polishing for an optimum time in a mixture of nitric acid and acetic acid for following surface finishings, chemical conversion coating, electroplating, electrophoretic painting and anodizing treatment.

Evaluation of Scratch Characteristics of Diaphragm for Application of Hydrogen Compressor Parts

  • Sung-Jun Lee;Chang-Lae Kim
    • Tribology and Lubricants
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    • v.39 no.5
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    • pp.212-215
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    • 2023
  • Diaphragm compressors play a crucial role in safely compressing large volumes of high-purity hydrogen gas without contamination or leakage, thereby ensuring quality and reliability. Diaphragm compressors use a thin, flat, triple-layered diaphragm plate that is subjected to repetitive piston pressure for compression. They are usually made of metallic materials such as stainless steel or Inconel owing to their high-pressure resistance. However, since they are consumable components, they fail due to fatigue from repetitive pressure and vibration stress. This study aims to evaluate the scratch characteristics of diaphragms in operational environments by conducting tests on three different samples: Inconel 718, AISI 301, and Teflon-coated AISI 301. The Inconel 718 sample underwent a polishing process, the AISI 301 sample used raw material, and the Teflon coating was applied to the AISI 301 substrate at a thickness of 50 ㎛. To assess the scratch resistance, reciprocating motion friction tests were performed using a tribometer, utilizing 220 and 2000 grit sandpapers as the counter materials. The results of the friction tests suggested that the Teflon-coated sample exhibited the lowest initial friction coefficient and consistently maintained the lowest average friction coefficient (0.13 and 0.11 with 220 and 2000 grit, respectively) throughout the test. Moreover, the Teflon-coated diaphragm showed minimal wear patterns, indicating superior scratch resistance than the Inconel 718 and AISI 301 samples. These findings suggest that Teflon coatings may offer an effective solution for enhancing scratch resistance in diaphragms, thereby improving compressor performance in high-pressure hydrogen applications.

A Study on Restoration Technology of Unit Injector Spill Valve for Injection System of Commercial Diesel Engine (상용차 디젤의 연료분사장치 유닛 인젝터 핵심부품인 스필 밸브의 성능 복원 관한 연구)

  • Lee, Chunggeun;Lee, Jeongho;Lee, Daeyup
    • Transactions of the Korean Society of Automotive Engineers
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    • v.25 no.3
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    • pp.389-396
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    • 2017
  • Restorations of automotive parts have been done ever since the first vehicle was produced. Because the most expensive parts of a vehicle are in the engine system, there have been various restoration methods developed for engine parts. In the case of commercial diesel engines, the fuel injection device is a key and expensive component. It also has a significant effect on vehicle performance. In particular, reduced engine power and increased exhaust gas emissions may result from mechanical damage due to abrasion of the spill valve in the fuel injection system of a diesel engine. In this paper, restoration techniques for damaged parts are applied to restore the abrasion of a spill valve of fuel injection, also called as the "unit injector", of commercial diesel engines. In order to recover the damage, optimized polishing techniques using hard-metal and coating processes are applied. To evaluate restoration techniques for the spill valve, performance and durability tests are performed on a test bench.

A COMPARATIVE STUDY ON SURFACE ROUGHNESS OF GLASS IONOMER CEMENT BY SURFACE COATING AGENT (표면도포제에 따른 수복용 글라스 아이오노머 세멘트의 표면조도 비교)

  • Choi, Byung-Jai;Hwang, Dong-Hwan
    • Journal of the korean academy of Pediatric Dentistry
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    • v.23 no.4
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    • pp.915-924
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    • 1996
  • The purpose of this paper is to investigate the surface roughness of glass ionomer cement during initial setting time followed by applying surface coating agent. No other finishing or polishing procedure is done and each surface coating agents (varnish, adhesive, gloss, sealant) are used after filling of glass ionomer cement. Surface roughness indices(Ra) are measured and surface contours are obtained electronically by Surfcorder SEF-30D(Kosaka laboratory Ltd., Japan). The results are as follows: 1. During initial setting time, surface roughness increases slightly regardless of surface coating agents. But it is statistically insignificant. (p>0.05) 2. Among surface coating agents used, Ra indices of group using varnish are high significantly compared to other groups regardless of elapsed time.(p<0.05) Among the groups which has used other surface coating agents except for the varnish group, similar Ra index all over the experiment is obtained, when compared to control group (no agent). 3. If no surface treatment is performed, tri-cure glass ionomer cement (Vitremer) has higher Ra Index than light cure glass ionomer cement (Fuji II LC) (t<0.05). But there is no difference between two groups in Ra index if any kinds of agents are applied except for sealant. (t>0.05)

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