• The Korean Journal of Ceramics
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• v.6 no.3
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• pp.236-239
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• 2000

Both the X-ray diffraction data of the normal direction in the sample orientation and the pole figure data of three reflections, (111), (200) and (220), were used to do the Rietveld refinement for the copper sheet prepared by a cold rolling process. The agreement between calculated and observed patterns was not satisfactory, which was attributed to the preferred orientation effect of the copper sheet. The Rietveld refinement for the copper sheet could be done successfully by applying the pole density of each reflection obtained from the corresponding inverse pole figure to the X-ray diffraction data of the normal direction. The R-weighted pattern, $R_{wp}$ was 12.99% and the goodness-of-fit indicator, S, was 3.68.

• The Korean Journal of Ceramics
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• v.6 no.3
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• pp.240-244
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• 2000

The three-dimensional orientation distribution function of a conical shaped tungsten liner prepared by the thermo-mechanical forming process was analyzed by 1.525$\AA$ neutrons to carry out the Rietveld refinement. The pole figure data of three reflections, (110)(220) and (211) were measured. The orientation distribution functions for the normal and radial directions were calculated by the WIMV method. The inverse pole figures of the normal and radial directions were obtained from their orientation distribution functions. The Rietveld refinement was performed with the RIETAN program that was slightly modified for the description of preferred orientation effect. We could successfully do the Rietveld refinement of the strongly textured tungsten liner by applying the pole density of each reflection obtained from the inverse pole figure to the calculated diffraction pattern. The correction method of preferred orientation effect based on the inverse pole figures showed a good improvement over the semi-empirical texture correction based on the direct usage of simple empirical functions.

• The Korean Journal of Ceramics
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• v.6 no.4
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• pp.354-358
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• 2000

The SnO$_2$film was deposited on a corning glass 1737 substrate by plasma enhanced chemical vapor deposition using a gas mixture of SnCl$_4$, $O_2$, and Ar. The film thickness was measured using $\alpha$-step and was about 9400$\AA$. The conventional X-ray diffractometry and pole figure attachment were used to refine the crystal structure of SnO$_2$ thin film. Six pole figures, (200), (211), (310), (301), (321), and (411), were measured with CoK$_\alpha$ radiation in reflection geometry. The X-ray diffraction data were measured at room temperature using CuK$_\alpha$ radiation with graphite monochromator. The agreement between calculated and observed patterns for the normal direction of SnO$_2$ thin film was not satisfactory due to the severely preferred orientation effect. The Rietveld refinement of heavily textured SnO$_2$ thin film was successfully achieved by adopting the pole density distribution of each reflection obtained from the inverse pole figure as a correction factor for the preferred orientation effect. The R-weighted pattern, R$_wp$, was 15.30%.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.03a
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• pp.117-120
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• 1997

Microstructure and pole figure through thickness in cold rolled sheet steel were investigated. The calculated plastic strain ratio in surface is greatly different with that in center layer and measured value in tensile test.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.14 no.6
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• pp.499-504
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• 2001

We evaluated the degree of texture through depth of the superconductor core of Bi-Sr-Ca-Cu-O(BSCCO) superconductor tape. The degree of texture was characterized by pole figure analysis indicating that the degree of texture varied significantly with depth of the superconductor core. It was observed that the degree of texture was higher near the interface than inside the superconductor core. Specifically, as getting near to the center from the sheath/core interface, the orientation of BSCCO became dispersed from normal direction(ND) which, in turn, resulted in the degradation of <001>-fiber texture. In addition, the <001> texture was non-uniform an, better texture was developed along rolling direction(RD), compared to transverse direction(TD). Microstructural investigation showed that grain alignment was locally degraded by the existence of second phases. I was observed that larger grain size and better texturing were developed near the relatively straight interface compared to those inside the superconducting core. Based on our study, the region near the interface is thought to carry significant current compared to that inside the core.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.114-117
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• 2007

In the present study, the effects of initial texture on the twinning formation of AZ31 Mg rolled sheet was investigated. Uniaxial compression tests were performed on samples cut along the normal direction and rolling direction of rolled AZ31 Mg alloy sheet at various temperatures (RT, 200, 250, 300, 350, $400^{\circ}C$) with the 0.01/s strain rate. Pole figure of rolling planes showed that basal planes of most gain were located parallel to the rolling direction. After compression test, microstructures and stress-strain curves results indicated that active deformation twining occurred only at the specimen cut along the rolling direction. The slip-twin transition with the increase of temperature was also investigated.

• The Korean Journal of Ceramics
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• v.4 no.1
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• pp.33-36
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• 1998

Epitaxially grown $Bi_4Ti_3O_{12}$ thin films on the MgO(100) substrates was prepared by dipping-pyrolysis process using metal naphthenates as starting materials. The films annealed at various temperatures were charactrized by X-ray diffraction $\theta$-2$\theta$ scans and pole-figure analysis ($\beta$ scanning). Highly c-axia oriented Bi4Ti3O12 films were crystallized by heat-treatment at 700$^{\circ}$ and 75$0^{\circ}C$ from precursor films pyrolyzed at 50$0^{\circ}C$. The X-ray pole-figure analysis indicated that the $Bi_4Ti_3O_{12}$ thin films have an epitaxial relationship with the MgO(100) substrates.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.10a
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• pp.287-290
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• 2005

The shearing and punching processes are analyzed with the finite element method using an isotropic material model. The experimental result in the punching process shows that final radiuses of sheet metal according to the rolling direction and transverse direction are different because of the material anisotropy. The material anisotropy is induced by complicated large deformation in the polycrystalline aggregate. The contact region between the punch and sheet metal experiences severe deformation such as shear, compression and tension in the punching process. In this paper, the analysis of punching process for Al 1100 is performed with the ABAQUS Standard. The analysis of texture development and evolution is carried out based on the deformation history in the punching process. The deformation histories are extracted by UMAT in the ABAQUS Standard. The torture development is investigated with the pole figure and yield surface during the punching process.

• Transactions of Materials Processing
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• v.29 no.1
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• pp.27-36
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• 2020

The Goss texture component of {110}<001> is well known as one of the best texture components to improve the magnetic properties of electrical steel sheets. The small amount of the Goss texture component is obtained at the surface of the steel sheet by shear deformation due to friction between the steel sheet and the roll during conventional symmetric rolling. This study aims to identify a method to obtain high intensity of the Goss texture component not only at the surface but in the whole layer of the steel sheet by shear deformation of asymmetric rolling. Low carbon steel sheets, which have different initial texture, were asymmetrically rolled by about 50%, 70%, and 80%. The pole figures of the top, center, and bottom layers of the initial and asymmetrically rolled low carbon steel sheets were measured by an X-ray diffractometer. Based on the measured pole figures of these samples, the intensities of the main texture components were analyzed for the initial and asymmetrically rolled low carbon steel sheets. As a result, the initial low carbon steel sheet with the γ-fiber component showed a higher intensity of the Goss texture component in the whole layer than the steel sheet with other texture components after asymmetric rolling.

• Proceedings of the Korean Nuclear Society Conference
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• 1998.05b
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• pp.93-98
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• 1998

CANDU 압력관의 집합조직을 원주 방향 집합조직에서 반경 방향 집합조직으로 변화시켜 $K_{IH}$ 를 평가하였다. 집합조직은 평면 변형에 의한 25% 확관 방법으로 번화시켰고 (0002) direct pole figure와 basal pole component (기저면 성분, Kearns number)로 분석하였다. 반경 방향집합조직의 압력관의 $K_{IH}$ 는 2$50^{\circ}C$에서 17MPa√m 이상으로 나타났으며, 이것은 상용 압력관의 $K_{IH}$ =8-10 MPa√m보다 70% 이상 높은 값이다. 반경 방향 집합조직의 압력관에서 나타나는 $K_{IH}$ 거동을 균열 진전면에서의 기저면 성분과 연계하여 분석하였으며, 평면 면형에 따른 집합조직의 변화는 슬립과 쌍정 기구의 작용으로 설명하였다. 본 연구의 결과는 CANDU 압책관의 delayed hydride cracking (DHC) 저항성 관점에서 반경 방향으로 집합조직을 제어하면 매우 효율적이라는 것을 보여 준다.