• Title/Summary/Keyword: Phase response curve

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Determination of Fluorescent Whitening Agents in Paper Materials by Ion-Pair Reversed-Phase High-Performance Liquid Chromatography

  • Kim, Jeong Soo;Kim, Do Hwan;Kim, Keon
    • Bulletin of the Korean Chemical Society
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    • v.33 no.12
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    • pp.3971-3976
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    • 2012
  • A simple method was developed for the analysis of seven stilbene-type fluorescent whitening agents (FWAs) in paper materials by ion-pair reversed-phase high-performance liquid chromatography with fluorescence detection. These stilbene-type FWAs included two disulfonate, two tetrasulfonate, and three hexasulfonate compounds. After optimization of chromatographic conditions, the FWAs were satisfactorily separated using a reversed-phase column (RP-18) with the following isocratic mobile phase: methanol-water (60:40) containing 17.5 mM TBABr and 10 mM citrate buffer (pH = 7.0). The calibration plot was linear in the range from 5 to 500 ng/mL for two disulfo-FWAs and from 1 to 500 ng/mL for the other five FWAs. Precision levels of the calibration curve as indicated by RSD of response factors were 1.2 and 8.1%. Limits of quantitation (LOQ) ranged from 1.2 to 11 ng/mL.

Design of Generalized Controller by Improved Model Reduction (개선된 모델 축소 방법에 의한 범용적 제어기 설계)

  • Cho, Joon-Ho;Hwang, Hyung-Su
    • Journal of the Institute of Electronics Engineers of Korea SC
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    • v.44 no.5
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    • pp.1-10
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    • 2007
  • In this paper, we proposed development of improved model reduction and design of common controller using reduction model. The Algorithm of improved model reduction considered the transient response and the steady-state response in response curve. The generalized controller is designed not only to ensure specified phase margin and iso-damping property also optimized smith-predictor controller about real model using reduction model. Simulation examples are given to show the better performance of the proposed method than convention methods.

Nonlinear response of complex fluids under LAOS(large amplitude oscillatory shear) flow

  • Ahn, Kyung-Hyun;Kyu Hyun;Nam, Jung-Gun;Manfred Wilhelm;Lee, Seung-Jong
    • Korea-Australia Rheology Journal
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    • v.15 no.2
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    • pp.97-105
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    • 2003
  • In the previous paper (Hyun et al.,2002), we have investigated the shape of storage modulus (G') and loss modulus (G") of complex fluids under large amplitude oscillatory shear (LAOS) flow. As the strain amplitude increases, owever, the stress curve becomes distorted and some important information may be smothered during data processing. Thus we need to investigate the stress data more precisely and systematically. In this work, we have obtained the stress data using high performance ADC (analog digital converting) card, and investigated the nonlinear response of complex fluids, 4wt% xanthan gum (XG), 2 wt% PVA/ 1 wt% Borax, and 1 wt% hyaluronic acid (HA) solutions, using Fourier transformation (FT) rheology. Comparing the strain signals in time domain with FT parameters in frequency domain, we could illustrate the sensitivity and importance of FT rheology. Diverse and unique stress patterns were observed depending on the material system as well as flow environment. It was found that they are not the outcome of experimental deficiency like wall slip but characteristics of the material system. When nonlinear response of complex fluids is analyzed, the intensity and phase angle of higher harmonic contributions should be considered together, and the shape of the stress signal was found to be strongly dependent upon phase angle.ngle.

FFC Design for PI Flow Control System Designed by CDM

  • Oh, Kyu-Kwon;Yu, Kee-Ho
    • 제어로봇시스템학회:학술대회논문집
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    • 2001.10a
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    • pp.151.3-151
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    • 2001
  • A design of PI controller to be used to control the first-order lag plus dead time process, such as a flow process, by the coefficient diagram method (CDM) is investigated. The factor of the dead time of process is first approximated to be the first-order by the Pade approximation. The response of the flow control system designed by CDM satisfy both transient and steady state specifications. However, the transient response generally still has long rise time. In order to improve the speed of the system response, a feedforward controller (FFC) is added into the PI control system. The structure of the FFC is a phase lead structure with two designed parameters and one derivative time obtained from the reaction curve of the flow process ...

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A Sudy on the Undamped Forced Vibration of Nonlinear Two-Degree-of-Freedom Systems (비선형 2자유도계의 비감쇠 강제진동 연구)

  • 박철희;박선재;윤영석
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.12 no.2
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    • pp.193-199
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    • 1988
  • The forced vibrations of nondissipative nonlinear two-degree-of-freedom system, subjected to periodic forcing functions, are investigated by use of the method of slowly changing phase and amplitude. The first order differential equations are derived for nonrationally solutions and the coupled nonlinear algebraic equations for stationary solutions. Through investigating the response curves of the system, which are obtained numerically by using Newton-Raphson method, it is found that the resonances can occur at more than the number of degree-of-freedom of the system depending on the relation between the nonlinear spring parameters, which has no counterpart in linear systems.

Finite Element Modeling and Nonlinear Analysis for Seismic Assessment of Off-Diagonal Steel Braced RC Frame

  • Ramin, Keyvan;Fereidoonfar, Mitra
    • International Journal of Concrete Structures and Materials
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    • v.9 no.1
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    • pp.89-118
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    • 2015
  • The geometric nonlinearity of off-diagonal bracing system (ODBS) could be a complementary system to covering and extending the nonlinearity of reinforced concrete material. Finite element modeling is performed for flexural frame, x-braced frame and the ODBS braced frame system at the initial phase. Then the different models are investigated along various analyses. According to the experimental results of flexural and x-braced frame, the verification is done. Analytical assessments are performed in according to three dimensional finite element modeling. Nonlinear static analysis is considered to obtain performance level and seismic behaviour, and then the response modification factors calculated from each model's pushover curve. In the next phase, the evaluation of cracks observed in the finite element models, especially for RC members of all three systems is performed. The finite element assessment is performed on engendered cracks in ODBS braced frame for various time steps. The nonlinear dynamic time history analysis accomplished in different stories models for three records of Elcentro, Naghan and Tabas earthquake accelerograms. Dynamic analysis is performed after scaling accelerogram on each type of flexural frame, x-braced frame and ODBS braced frame one by one. The base-point on RC frame is considered to investigate proportional displacement under each record. Hysteresis curves are assessed along continuing this study. The equivalent viscous damping for ODBS system is estimated in according to references. Results in each section show the ODBS system has an acceptable seismic behaviour and their conclusions have been converged when the ODBS system is utilized in reinforced concrete frame.

Analysis on the Characteristics of National Assessment of Educational Achievement (NAEA) Items for Science Subject: With a Focus on Optics (국가수준 학업성취도 평가의 과학 문항 특성 분석 : 광학 내용을 중심으로)

  • Lee, Bongwoo;Lee, Inho
    • Journal of The Korean Association For Science Education
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    • v.35 no.3
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    • pp.465-475
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    • 2015
  • The purpose of this study is to analyze the results of physics (optics) in nationwide standardized assessment and to investigate middle-school students' characteristics of achievement by using an option response rate distribution curve. For this purpose, we analyzed the 10 optics problems from the National Assessment of Educational Achievement (NAEA) items for middle school science subject conducted in 2010-2013. The results of this study are as follows; First, students showed a little higher achievement in optics than classical mechanics and electromagnetism. Second, students achieved significantly worse in 'formation of image' in 'light' part and 'variation of phase in propagation of wave' in 'wave' part. Third, students showed a context-dependent problem solving strategy and result. Additionally, we suggested some implications about the readjustment of some optics concepts level of national science curriculum, the need for teaching and learning strategies for basic level students, and the need for teaching and learning strategies focused on the realistic context.

IRF performance prediction by analyzing of amplitude and phase errors for the wideband Chirp signal (광대역 첩 신호의 진폭 및 위상오차 분석을 통한 IRF 성능 분석)

  • Kim, Dong-Sik;Kim, Jong-Pil;Lee, Jong-Hwan
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.44 no.2
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    • pp.131-138
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    • 2016
  • In this paper, we studied the IRF performances of the chirp signal used in the SAR system. The most important factors that degrade IRF performances are amplitude and phase errors. Each factor can be represented to linear, quadratic, random and ripple terms. That can be extracted by a quadratic polynomial curve fitting of chirp waveform. We analyzed the IRF performances by the error terms and supposed the minimum value of RF non-linearity to meet the specification of the PSLR and ISLR.

In Situ Mechanical Response of Bovine Humeral Head Articular Cartilage in a Physiological Loading Environment (생리학적인 하중 조건에서 소 상완골 연골의 기계적 특성)

  • Park, Seong-Hun
    • Journal of the Korean Society for Precision Engineering
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    • v.25 no.1
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    • pp.145-150
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    • 2008
  • One of the unresolved questions in articular cartilage biomechanics is the magnitude of the dynamic modulus and tissue compressive strains under physiological loading conditions. The objective of this study was to characterize the dynamic modulus and compressive strain magnitudes of bovine articular cartilage at physiological compressive stress level and loading frequency. Four bovine calf shoulder joints (ages 2-4 months) were loaded in Instron testing system under load control, with a load amplitude up to 800 N and loading frequency of 1 Hz, resulting in peak engineering stress amplitude of ${\sim}5.8\;MPa$. The corresponding peak deformation of the articular layer reached ${\sim}27%$ of its thickness. The effective dynamic modulus determined from the slope of stress versus strain curve was ${\sim}23\;MPa$, and the phase angle difference between the applied stress and measured strain which is equivalent to the area of the hystresis loop in the stress-strain response was ${\sim}8.3^{\circ}$. These results are representative of the functional properties of articular cartilage in a physiological loading environment. This study provides novel experimental findings on the physiological strain magnitudes and dynamic modulus achieved in intact articular layers under cyclical loading conditions.

Sensing Characteristics of Uncoated Double Cladding Long-period Fiber Grating Based on Mode Transition and Dual-peak Resonance

  • Zhou, Yuan;Gu, Zheng Tian;Ling, Qiang
    • Current Optics and Photonics
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    • v.5 no.3
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    • pp.243-249
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    • 2021
  • In this paper, the sensing characteristics of a double cladding fiber (DCF) long-period fiber grating (LPFG) to the surrounding refractive index (SRI) are studied. The outer cladding of the DCF plays the role of the overlay, thus, the mode transition (MT) phenomenon of DCF can be induced by etching the outer cladding radius instead of coating overlays. The response characteristics of the effective refractive index (ERI) of the cladding mode to the outer cladding radius are analyzed. It is found that in the MT range, the change rate of ERIs of cladding modes is relatively larger than that for other ranges. Further, based on the features of the mode transition region (MTR), the phase-matching curve of the 11th cladding mode is investigated, and the response of the DCF-LPFG to the SRI is characterized by the change of wavelength intervals between the dual peaks under different outer cladding radii. The numerical simulation results show that the SRI sensitivity is greatly improved, which is available to 3484.0 nm/RIU with the fitting degree 0.998 in the SRI range of 1.33-1.37. The proposed DCF-LPFG can provide new theoretical support for designing the DCF-LPFG refractive index sensor with excellent performances of sensitivity, linearity and structure.