• 제목/요약/키워드: Phase degree

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미소부 X-선 회절분석기를 이용한 미립조암광물의 상동정 및 배향도 측정 -$Al_{2}SiO_{5}$ 3상다형- (Phase identification and degree of orientation measurements far fine-grained rock forming minerals using micro-area X-ray diffractometer -$Al_{2}SiO_{5}$ Polymorphs-)

  • 박찬수;김형식
    • 암석학회지
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    • 제9권4호
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    • pp.205-210
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    • 2000
  • 암석중에 미립(직경 0.3mm내외)으로 존재하는 조암광물의 동정 및 결정학적인 배향도를 미소부 X선 회절분석기를 이용하여 측정하였다. 실험에 사용된 표품들은 $A1_{2}SiO_{5}$ 3상디형(규선석, 남정석, 홍주석)으로서 모든 표품들은 박편상의 것을 측정대상으로 하였다 측정에 이용된 X선 회절분석기는 3(${\omega}\;{\chi}\;{\phi}$)축 회전 측각기 및 위치민감형 검출기로 구성되어 있으며 X선원으로는 $CuK_{\alpha}$를 사용하였으며 직경 $50\;\mu\textrm{m}$의 시준기를 사용하였다. 광물 동정은 3(${\omega}\;{\chi}\;{\phi}$)축 회전 측정법에 의해 시행되었으며, 박편표면에 우세하게 나타나는 광물상의 격자면을 알아보기 위해 2(${\omega}\;{\phi}$)축 회전 측정을 실시하였고 2축 회전 측정법에 의해 우세하게 나타난 회절선에 대한 격자방향의 배향도와 극분포를 확인하기 위하여 X-선 극점도 측정을 시행하였다. 3축 회전 측정결과 측정대상 광물상에 대해 동정이 가능하였으며 2축 회전 측정과 X-선 극점도 측정결과 규선석(310), 남성석(200), 홍주석(122)극이 절단면, 즉 박편표면의 법선방향으로 잘 발달하고 있음을 확인할 수 있었다. 본 측정법은 편광현미경을 사용하여 식별이 용이하지 않은 미립조암광물의 동정과 배향도를 알아보는데 유용하게 사용될 수 있는 분석기법이다.

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Properties and pozzolanic reaction degree of tuff in cement-based composite

  • Yu, Lehua;Zhou, Shuangxi;Deng, Wenwu
    • Advances in concrete construction
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    • 제3권1호
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    • pp.71-90
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    • 2015
  • In order to investigate the feasibility and advantage of tuff used as pozzolan in cement-based composite, the representative specimens of tuff were collected, and their chemical compositions, proportion of vitreous phase, mineral species, and rock structure were measured by chemical composition analysis, petrographic analysis, and XRD. Pozzolanic activity strength index of tuff was tested by the ratio of the compression strength of the tuff/cement mortar to that of a control cement mortar. Pozzolanic reaction degree, and the contents of CH and bond water in the tuff/cement paste were determined by selective hydrochloric acid dissolution, and DSC-TG, respectively. The tuffs were demonstrated to be qualified supplementary binding material in cement-based composite according to relevant standards. The tuffs possessed abundant $SiO_2+Al_2O_3$ on chemical composition and plentiful content of amorphous phase on rock texture. The pozzolanic reaction degrees of the tuffs in the tuff/cement pastes were gradually increased with prolongation of curing time. The consistency of CH consumption and pozzolanic reaction degree was revealed. Variation of the pozzolanic reaction degree was enhanced with the bond water content and relationship between them appeared to satisfy an approximating linear law. The fitting linear regression equation can be applied to mutual conversion between pozzolanic reaction degree and bond water content.

배관 압력을 이용한 방향제어밸브 위상각 대역폭 주파수 측정에 관한 연구 (A Study on the Phase Bandwidth Frequency of a Directional Control Valve Based on the Hydraulic Line Pressure)

  • 김성동;이정은;신대영
    • 드라이브 ㆍ 컨트롤
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    • 제15권4호
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    • pp.1-10
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    • 2018
  • Spool displacement of a direction control valve is the standard signal to measure the bandwidth frequency of the direction control valve. When the spool displacement signal is not available, it is suggested in this study to use the metering hydraulic line as an alternative way to measure - 90 degree phase bandwidth frequency of the hydraulic direction control valve. Dynamics of the hydraulic line is composed of inertia, capacitance, and friction effects. The effect of oil inertia is dominant in common hydraulic line dynamics and the line dynamics is close to a derivative action in a range of high frequency; such as a range of bandwidth frequency of common directional control valves. Phase difference between spool displacement and line load pressure is nearly constant as a valve close to 90 degree. If phase difference is compensated from the phase between valve input and pressure, compensated phase may be almost same as the phase of spool displacement that is a standard signal to measure phase bandwidth frequency of the directional control valve. A series of experiments were conducted to examine the possibility of using line pressure in to measure phase bandwidth frequency of a directional control valve. Phase bandwidth frequency could be measured with relatively high precision based on metering hydraulic line technique and it reveals consistent results even when valve input, oil temperature, and supply pressure change.

비정방 선형 시스템의 강인 제어기 설계 및 그 응용 (Robust Controller Design of Non-Square Linear Systems and Its Applications)

  • 손영익;심형보;조남훈
    • 대한전기학회논문지:시스템및제어부문D
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    • 제52권4호
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    • pp.189-197
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    • 2003
  • The problem of designing a parallel feedforward compensator (PFC) is considered for a class of non-square linear systems such that the closed-loop system is strictly passive. If a given square system has (vector) relative degree one and is weakly minimum phase, the system can be rendered passive by a state feedback. However, when the system states are not always measurable and the given output is considered, passivation (i.e. rendering passive) of a non-minimum phase system or a system with high relative degree cannot be achieved by any other methodologies except by using a PFC. To passivate a non-square system we first determine a squaring gain matrix and design a PFC such that the composite system has relative degree one and is minimum phase. Then the system is rendered strictly passvie by a static output feedback law. Necessary and sufficient conditions for the existence of the PFC and the squaring gain matrix are given by the static output feedback formulation, which enables to utilize linear matrix inequality (LMI). As an application of the scheme, an alternative way of replacing the role of velocity measurements is provided for the PD-control law of a convey-crane system.

시트르산의 양과 소결온도에 따른 (La,Sr)$MnO_3/Gd_{0.2}Ce_{0.8}O_{1.9}$ 계면특성 (Characterization of (La,Sr))$MnO_3/Gd_{0.2}Ce_{0.8}O_{1.9}$ Interface with Citric Acid Contents and Sintering Temperature)

  • 윤일영;윤희성;김병호
    • 한국전기전자재료학회논문지
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    • 제11권1호
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    • pp.18-25
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    • 1998
  • G $d_{0.2}$C $e_{0.8}$ $O_{1.9}$(CGO) for electrolyte and L $a_{0.5}$S $r_{0.5}$Mn $O_3$(LSM50) for cathode in Solid Oxide Fuel Cells(SOFC) were synthesized by citrate process. Specimens were prepared with sintering temperatures at 110$0^{\circ}C$, 120$0^{\circ}C$ and 130$0^{\circ}C$, which were fabricated by slurry coating with citric acid contents. Interfacial resistance was measured between cathode and electrolyte using AC-impedance analyzer. With various citric acid content, the degree of agglomeration for the initial particles changed. Also sintering temperature changed the particle size and the degree of densification of cathode. Factors affecting the interfacial resistance were adherent degree of the electrolyte and cathode, distribution of TPB(three phase boundaries, TPB i.e., electrolyte/electrode/gas phase area) and porosity of cathode. By increasing the sintering temperature, particle size and densification of the cathode were increased. And then, TPB area which occurs catalytic reaction was reduced and so interfacial resistance was increased.sed.sed.d.

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스퍼터링 및 저압화학기상증착 비정질 실리곤 박막의 고상 결정화 특성 (Characterization of Solid Phase Crystallization in Sputtered and LFCVD Amorphous Silicon Thin Film)

  • 김형택
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1995년도 추계학술대회 논문집
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    • pp.89-93
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    • 1995
  • Effects of hydrogenation in amorphous silicon rile growths on Solid Phase Crystallization (SPC) was investigated using x-ray diffractometry, energy dispersive Spectroscopy, and Raman spectrum. Interdiffusion of barium(Ba) and aluminum(Al) compounds of corning substrate was observed in both of rf sputtering and LFCVD films under the low temperature(580$^{\circ}C$) annealing. Low degree of crystallinity resulted from the interdiffusion was obtained. Highly applicable degree of crystallinity was obtained through the mechanical damage induced surface activation on amorphous silicon films. X-ray diffraction intensity of (111) orientation was used to characterize the degree of crystallinity of SPC. Nucleation and growth rate in SPC could be controllable through the employed surface treatment. IIydrogenated LPCVD films showed the superior crystallinity to non-hydrogenated sputtering films. Insignificant effects of activation treatment in sputtered film was of activation treatment in sputtered film was observed on SPC.

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Fault Diagnosis of Power Converter for Switched Reluctance Motor based on Discrete Degree Analysis of Wavelet Packet Energy

  • Gan, Chun;Wu, Jianhua;Yang, Shiyou
    • Journal of international Conference on Electrical Machines and Systems
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    • 제2권3호
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    • pp.336-341
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    • 2013
  • Power converter plays a very important role in switched reluctance motor (SRM) systems, and it is also the easiest one to experience failures. Power converter faults will cause the motor to run in non equilibrium states, and a long time fault operation will lead to motor and other modules damaged, and make the system completely lose working stability. This paper uses an asymmetric bridge converter as the research object with three-phase SRM, employs the wavelet packet decomposition for the phase currents. It analyzes and studies the short circuit fault condition of IGBT, uses an energy discrete degree of the wavelet packet nodes as the fault characteristic, and conducts the corresponding experimental and simulation analysis to verify the effectiveness and practicality of the proposed method.

압축수의 임계유량에 관한 해석적 연구 (An Analytical Study for Critical Mass Flowrate of Compressed Water)

  • 김희동;김재형;한민교;박경암
    • 한국추진공학회지
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    • 제7권1호
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    • pp.57-65
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    • 2003
  • 본 연구에서는 압축수가 노즐을 통해 급격히 팽창될 때 기액이상류가 플래싱 증발하게 되는 이상류의 임계유동을 Isentropic-Homogeneous-Equilibrium model과 Leung model을 사용해 해석하였다. 그 결과 이상유동은 연속/불연속적 초크로 될 수 있으며, 정체점의 압력이 10Mpa일 경우에는 단상류 유동의 초크현상과 유사한 연속적인 초크현상이 정체점의 아냉각도가 10K이하일 경우에만 발생한다는 것을 알았다.

슈퍼듀플렉스강 용접금속의 입계부식에 미치는 σ 상의 영향 (Effect of σ-phase on Intergranular Corrosion of Super Duplex Stainless Steel Weld Metal)

  • 이재형;정병호;서기정;강창룡
    • 열처리공학회지
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    • 제26권6호
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    • pp.293-299
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    • 2013
  • A specimen of weld metal was prepared by GTA welding with weld wire of super duplex stainless steel. Aging treatment was conducted for the sample at the temperature range of 700 to $900^{\circ}C$ for 5 to 300 minutes. The effect of volume fraction of ${\sigma}$-phase to intergranular corrosion of weld metal has been investigated and the results were derived as follows. The volume fraction of ${\sigma}$ phase tends to increase with an increase of aging temperature and time and intergranular corrosion of weld metal was increased by an increase of ${\sigma}$ phase. Degree of sensitization representing intergranular corrosion was found to tend to increase with an increase of aging time at 700 to $800^{\circ}C$, while it decreased by an increase of aging time at $900^{\circ}C$.

Parasitoid Complex of the Gypsy Moth (Lymantria dispar) in the Increase-phase Populations in Korea

  • Lee, Jang-Hoon;Pemberton, Robert W.
    • Journal of Ecology and Environment
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    • 제32권2호
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    • pp.75-81
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    • 2009
  • The species composition of the parasitoid complex and the degree of parasitism by each species were analyzed for gypsy moth (Lymantria dispar) populations in the increasing phase. Total of 7,826 mid-late instar larvae and pupae were collected and reared from two collection sites in Gangwon Province, Korea. Two tachinid flies (Blepharipa schineri and Parasetigena silvestris), and the ichneumonid wasp (Coccygomimus disparis) were the most abundant parasitoids, in the order of decreasing importance. Other parasitoids occurring included Coteisa melanoscelus, Cotesia scheaferi, Glyptapanteles liparidis, Brachymeria lasus, and Exorista spp. The low incidence of the NPVirus is hypothesized to be an important factor in determining degree of parasitism rate by P. silvestris and B. schineri, and their relative dominance in the parasitoid complex.