• Title/Summary/Keyword: Phase composition

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Phase Separation and Precipitation Characteristics in ZnS doped Borosilicate Glasses (ZnS 미립자 분산 붕규산엽계 유리에서의 분상 및 미립자 석출 특성)

  • 이승환;류봉기
    • Journal of the Korean Ceramic Society
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    • v.35 no.12
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    • pp.1337-1342
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    • 1998
  • To investigate an effect of phase separation on precipitation characteristics of ZnS microcrystals in ma-trix glass ZnS doped borosilicate glasses for nonlinear optical applications were prepared by melting and pre-cipitation process. ZnS dopant contributed to phase separation promotion which increased the phase separa-tion of the matrix glass within immiscibility region. It was also found that ZnS as phase separation promoter showed a similar contribution for some selected glass compositions in miscibility region. The precipitation of ZnS microcrystals occurred in thephase separable glass compoitions. The radius of ZnS microcrystals in-creased with increasing the heat treatment temperature and Na2O contents of matrix glass composition. The ZnS particle sizes estimated by effective mass approximation ranged from about 30 to 80${\AA}$ It was suf-ficiently small to show quantum confinement effect.

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The measurement & Analysis of Voltage Unbalance Factor at LV Customer of Three-Phase Four-Wire System (3상 4선식 저압 수용가의 전압 불평형율 측정분석)

  • Kim, Jong-Gyeum;Park, Young-Jin;Lee, Eun-Woong
    • Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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    • 2004.05a
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    • pp.43-47
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    • 2004
  • Most of LV customer has been composed the 3-phase four wire system distribution system which is supplying simultaneously at the 1-phase & 3-phase load. In this system, the composition of the power apparatus system is simple rather than conventional separation mode of the 1-phase & 3-phase, But due to uneven load unbalance or unclean power quality, various kinds such as do-rating or power losses become an issue. In this paper, we measured and analyzed voltage and current waveform in the field, compared with internationally allowable voltage unbalance limits.

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Synthesis of Superconductor $YBa_{2}Cu_{4}O_{8}$ by Pyrolysis of EDTA Complex

  • Jeong Cheol-Mo;Mun Seung-Ho;Kang Cheol-Hwa;Lee Cheol-Eui;Yom Sang-Seop;Kim Keon
    • Bulletin of the Korean Chemical Society
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    • v.13 no.6
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    • pp.663-665
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    • 1992
  • The superconducting $YBa_2Cu_4O_8$ was synthesized in oxygen condition at 1 atm. The starting material with 1 : 2 : 4 composition was obtained by pyrolysis of EDTA complex, which was converted to 1-2-3 phase during densification, followed by the 1-2-4 phase recovery at $810^{\circ}C$ . The phase presents were identified by XRD, TG, DTA and AC magnetic susceptibility. Our data indicated that considerable amounts of 1-2-4 phase formed but with the 1 : 2 : 3 phase or possibly 2-4-7 as visible. As the P($O_2$) increased with temperature, impurity peak, CuO ($2{\Theta}$ = 38.8), gradually decrease, and we conclude that the 1-2-4 phase is predominant bulk superconductor under the high oxygen pressure.

Recent developments of manganese-aluminium as rare-earth-free magnets

  • Sirisathitkul, Chitnarong
    • Advances in materials Research
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    • v.9 no.4
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    • pp.323-335
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    • 2020
  • This article reviews findings and progresses in the past decade on manganese-aluminium (MnAl) based magnets as the interest has been revived to fulfill their potential as commercial magnets. The challenges in developments of these rare-earth-free magnets are to acquire a high remanence and coercivity from the ferromagnetic τ-phase in MnAl alloys. To this end, the phase transformation to this τ-MnAl with L10 body centered tetragonal structure has been promoted by a variety of methods and a few percents of carbon (C) is often added to prevent the phase decomposition. Magnetization and coercivity are not only influenced by the phase composition but also the microstructure. The fabrication processes and factors affecting the phase and microstructure are therefore covered. Finally, the productions of bulk MnAl magnets are addressed.

High temperature deformation behavior of $\alpha\;and\;\beta$ phase of Ti-6Al-4V alloy with an equiaxed microstructure (등축정 Ti-6Al-4V 합금의 $\alpha,\;\beta$ 구성상의 고온변형거동 규명)

  • Lee, You-Hwan;Yeom, Jong-Taek;Park, Nho-Kwang;Lee, Chong-Soo;Kim, Jeoung-Han
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.05a
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    • pp.295-298
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    • 2005
  • High temperature deformation behavior of $\alpha\;and\;\beta$ phase of Ti-6Al-4V was investigated within the framework of a self-consistent approach at various temperature ranges. To examine the flow behavior of u-phase, Ti-7.0Al-1.5V alloy was used, whose chemical composition is close to that of the $\alpha$ phase in Ti-6Al-4V at hot working temperatures. The flow stress of $\beta$ phase was predicted by using self-consistent approach. The flow stress of $\alpha$ phase was higher than that of $\beta$ phase above $750^{\circ}C$, while the $\beta$ phase revealed higher flow stress than a phase at $650^{\circ}C$. It was found that the relative strength and strain rate ratio between $\alpha\;and\;\beta$ phase significantly varied with temperature. From this approach, the mode for grain matrix deformation was proposed as a mixed type of both iso-stress and iso-strain rate modes.

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Study on Metal Cupferrate Complex (Part II) Spectrophotometric Determination of Fe(III)-Cupferrate Composition (Metal Cupferrate Complex 에 關한 硏究 (第 2 報) Spectrophotometry 에 의한 Fe(III)-Cupferrate의 化學組成의 決定)

  • Si-Joong Kim;Doo-Soon Shin
    • Journal of the Korean Chemical Society
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    • v.7 no.4
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    • pp.280-282
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    • 1963
  • Fe (III)-cupferrate composition in chloroform phase was determined by molar ratio method, continuous variation method and slope ratio method spectrophotometrically at 325m$\mu$ and 385m$\mu$ wavelength. At both wavelength, compositions of the complex were Fe$Cupf_3$.

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Comparison and Analysis of P2P Botnet Detection Schemes

  • Cho, Kyungsan;Ye, Wujian
    • Journal of the Korea Society of Computer and Information
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    • v.22 no.3
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    • pp.69-79
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    • 2017
  • In this paper, we propose our four-phase life cycle of P2P botnet with corresponding detection methods and the future direction for more effective P2P botnet detection. Our proposals are based on the intensive analysis that compares existing P2P botnet detection schemes in different points of view such as life cycle of P2P botnet, machine learning methods for data mining based detection, composition of data sets, and performance matrix. Our proposed life cycle model composed of linear sequence stages suggests to utilize features in the vulnerable phase rather than the entire life cycle. In addition, we suggest the hybrid detection scheme with data mining based method and our proposed life cycle, and present the improved composition of experimental data sets through analysing the limitations of previous works.

Effect of droplet size on electro-optical switching properties of polymer dispersed liquid crystals (폴리머 분산 액정의 전기 광학적 스위칭 특성에 대한 액정방울 크기의 효과)

  • Kim, In-Tae;Yu, Yeon-Serk
    • Korean Journal of Optics and Photonics
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    • v.17 no.1
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    • pp.23-30
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    • 2006
  • Effects of liquid-crystal droplets size on electro-optical properties of the polymer dispersed liquid crystals are investigated experimentally The liquid crystal droplets size was varied by controlling the Laser power for phase separation and LC/oligomer composition ratio. Electro-optical switching voltage is dependent on the LC/oligomer composition ratio and liquid crystal droplet size. The experimental results showed droplet size will be small and saturation voltage is increased but rise time will be short at high power illumination laser light for phase separation.

Dielectric Properties of $(Ba,Sr,Ca)TiO_{3}$ Ceramics with Additon of Dopant (불순물 첨가에 따른 $(Ba,Sr,Ca)TiO_{3}$ 세라믹의 유전특성)

  • Lee, Sung-Gap;Lee, Young-Hie;Lim, Sung-Soo;Park, In-Gil
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.42-45
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    • 2001
  • $(Ba_{0.6}Sr_{0.4}Ca_{x})TiO_{3}+yZrO_{2}$ wt% (x=0.10, 0.15, 0.20, y=0.5~3.0) specimens were fabricated by the mixed-oxide method and then the structural and dielectric properties as a function of the composition ratio and $ZrO_2$ contents were studied. All BSCT specimens showed dense and homogeneous structure without the presence of the seconds phase. The Curie temperature and the dielectric constant at room temperature decreased with increasing the Ca/Ba composition ratio and $ZrO_2$ content. The BSCT(50/40/10) specimens showed the excellent tunability property. And the tunability were increased with increasing the contents of $ZrO_2$.

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A Pseudo-Random Carrier PWM Technique by Fixed Frequency Carrier Composition (고정 주파수의 캐리어 합성에 의한 준 랜덤 주파수 캐리어 PWM기법)

  • Kim, Jong-Nam;Jung, Young-Gook;Lim, Young-Cheol;Park, Sung-.Jun;Kim, Kwang-Heon
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.54 no.11
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    • pp.547-552
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    • 2005
  • This paper describes a pseudo-random carrier PW technique for the power converters. The proposed method generates a new pseudo-random carrier by randomly composing a carrier with fixed frequency and a carrier with opposition phase. To confirm the validity of the proposed method, a single-phase multi-level inverter was implemented and tested. The experimental results show that the output voltage and current harmonics spectra of an inverter have broadening effect of harmonics, as only simple composition of fixed frequency carries.