• Title/Summary/Keyword: Phase boundary

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Influence of geometry and loading conditions on the dynamics of martensitic fronts

  • Berezovski, Arkadi
    • Smart Structures and Systems
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    • v.4 no.2
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    • pp.123-135
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    • 2008
  • Damping capacity of SMA damping devices is simulated numerically under distinct geometry and loading conditions. Two-dimensional numerical simulations are performed on the basis of a phenomenological model of dynamics of martensite-austenite phase boundaries. Results of the simulations predict the time delay and the value of the stress transferred to other parts of a construction by a damper device.

Microstructural Analysis of Thermo-Mechanical Processed Ti-6Al-4Fe Alloy (Ti-6Al-4Fe 합금의 가공열처리 미세조직 분석)

  • Choe, Byung Hak;Choi, Won-Youl;Shim, Jong Heon;Park, Chan Hee;Kang, Joo-Hee;Kim, Seung Eon;Hyun, Yong Taek
    • Korean Journal of Materials Research
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    • v.25 no.8
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    • pp.410-416
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    • 2015
  • Microstructural analysis of a (${\alpha}+{\beta}$) Ti alloy was investigated to consider phase transformation in each step of the thermo-mechanical process using by SEM and TEM EDS. The TAF (Ti-6Al-4Fe) alloy was thermo-mechanically treated with solid solution at $880^{\circ}C$, rolling at $880^{\circ}C$ and annealing at $800^{\circ}C$. In the STQ state, the TAF microstructure was composed of a normal hcp ${\alpha}$ and metastable ${\beta}$ phase. In a rolled state, it was composed of fine B2 precipitates in an ${\alpha}$ phase, which had high Fe segregation and a coherent relationship with the ${\beta}$ matrix. Finally, in the annealing state, the fine B2 precipitates had disappeared in the ${\alpha}$ phase and had gone to the boundary of the ${\alpha}$ and ${\beta}$ phase. On the other hand, in a lower rolling temperature of $704^{\circ}C$, the B2 precipitates were more coarse in both the ${\alpha}$ and the boundary of ${\alpha}$ and ${\beta}$ phase. We concluded that microstructural change affects the mechanical properties of formability including rolling defects and cracks.

Crystal Defects and Grain Boundary Properties in ZnO-Zn2BiVO6-Co3O4-Cr2O3-CaCO3 Varistor (ZnO-Zn2BiVO6-Co3O4-Cr2O3-CaCO3 바리스터 내의 결정결함과 입계특성)

  • Hong, Youn-Woo;Ha, Man-Jin
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.32 no.4
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    • pp.276-280
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    • 2019
  • In this study, we investigated the crystal defects and grain boundary properties in a ZZCCC ($ZnO-Zn_2BiVO_6-Co_3O_4-Cr_2O_3-CaCO_3$) varistor, with the liquid-phase sintering aid $Zn_2BiVO_6$ developed by our laboratory. The ZZCCC varistor sintered at $1,200^{\circ}C$ exhibited excellent nonlinear current-voltage characteristics (${\alpha}=63$), with oxygen vacancy ($V_o^*$ ; 0.35 eV) as a main defect, and an apparent activation energy of 1.1 eV with an electrically single grain boundary. Therefore, among the various additives to improve the electrical properties of ZnO varistors, if $Zn_2BiVO_6$ is used as a liquid phase sintering aid, it will be ideal to use Co for the oxygen vacancy and Ca for the electrically single grain boundary. This will allow the good properties of ZnO varistors to be maintained up to high sintering temperatures.

Analysis of Phase Separation by Thermal Aging in Duplex Stainless Steels by Magnetic Methods

  • Kim, Sunki;Wonmok Jae;Kim, Yongsoo
    • Nuclear Engineering and Technology
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    • v.29 no.5
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    • pp.361-367
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    • 1997
  • The phase separation in ferrite phase of duplex stainless steel is the primary cause of thermal aging embrittlement of the LWR primary pressure boundary components. In this study the phase separation of simulated duplex stainless steel was detected by Mossbauer spectroscopy and magnetic property analysis by VSM(Vibrating Specimen Magnetometer). The simulated duplex stainless steels, Fe-Cr binary, Fe-Cr-Ni ternary, and Fe-Cr-Ni-Si quarternary allots, were aged at 370 and 40$0^{\circ}C$ up to 5,340 hours. It was observed from Mossbauer spectra analysis that internal magnetic field increases with aging time and from VSM that the specific saturation magnetization and Curie temperature increase with aging time. These result are indicative that phase separation into Fe-rich region and Cr-rich region is caused by thermal aging in the temperature range of 370~40$0^{\circ}C$ In cases of specimens containing Ni, the increase of specific saturation magnetization is much higher. This implies that Ni seems to promote Fe-Cr interdiffusion, which accelerates the phase separation into Fe-rich $\alpha$ phase and Cr-rich $\alpha$' phase.

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Phase Diagram of Spin Density Wave and $\pi$ Phase Shifted Superconductivity in the Fe Pnictide Superconductors (철 초전도체에서 스핀 밀도 파와 $\pi$ 위상 차 초전도성의 상전이 그림)

  • Lee, Na-Young;Choi, Han-Yong
    • Progress in Superconductivity
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    • v.11 no.2
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    • pp.112-117
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    • 2010
  • We examine phase transition of the spin density wave and $\pi$ phase shifted superconductivity in the Fe pnictide superconductors. The phase diagram is described in the plane of the temperature T and the doping x with the combination of Ginzburg-Landau expansion of the free energy near the multi-critical temperature $T_c$ and the self-consistent numerical iterations of the gap equations. The phase separation or coexistence is determined by computing the 4-th order terms of the free energy which is confirmed by the numerical calculations. We can show the phase coexistence when the spin density wave is incommensurate. And the first order phase transition is observed near the boundary between commensurate and incommensurate spin density wave.

The Effect of Initial α' on Low and High Cycle Fatigue Behavior of STS 304 Stainless Steel (STS 304 강의 저주기 및 고주기 피로에 있어 초기 마르텐사이트의 영향)

  • Lee, Hyun-Seung;Sin, Hyung-Ju;Kim, Song-Hee
    • Journal of Industrial Technology
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    • v.21 no.B
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    • pp.331-339
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    • 2001
  • Zero to tension fatigue tests and strain controlled fatigue tests were carried out to find how initial strain induced martensite, ${\alpha}^{\prime}$ affects low and high cycle fatigue behavior and fatigue crack growth mechanisms. Microscopic study and phase analysis were carried out with TEM, SEM, EDAX, Optical Microscope, Ferriscope, and X-ray diffractometry. The amount of Initial ${\alpha}^{\prime}$ was controlled from 0% to 33% by controlling the temperatures for cold working and heat treatment. Lower contents of initial ${\alpha}^{\prime}$ showed higher fatigue resistance in low cycle fatigue but lower fatigue resistance in high cycle fatigue because it is ascribed to the more transformation of ${\alpha}^{\prime}$ martensite during low cycle fatigue and higher ductility. In high cycle fatigue, fatigue life is attributed to the strength and phase transformation of austenite into ${\alpha}^{\prime}$ during fatigue was negligible. ${\gamma}$ boundary, ${\gamma}/twin$ boundary, and ${\gamma}/{\alpha}^{\prime}$ boundary were found to be the preferred site of fatigue crack initiation.

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Similarity analysis of a forced uniform flow impinging on a rotating disk in a vapor deposition process (증착공정에서의 회전원판 정체점유동에 대한 상사해석)

  • Song, Chang-Geol;Hwang, Jeong-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.21 no.3
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    • pp.371-379
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    • 1997
  • A theoretical study for a forced uniform flow impinging on a rotating disk, typically involved in Chemical Vapor Deposition(CVD) and Vapor-phase Axial Deposition(VAD) processes, has been carried out. A set of exact solutions for flow and temperature fields are developed by employing a similarity variable obtained from force balance on a control volume near the disk. The solutions depend on the rotating speed of the disk, .omega., and the forced flow speed toward the disk, a. For constant forced flow speed, the overall boundary layer thickness decreases when the rotating speed increases. Approximately 5%, 15%, and 30% decreases of the thickness are obtained for .omega./a = 2, 5, and 10, respectively, compared to the case of .omega./a = 0 (axisymmetric stagnation point flow). For constant rotating disk speed the boundary layer thickness immediately decreases as the forced flow speed increases, compared to the case of .omega./a .rarw. .inf. (induced flow near a rotating disk). Effects of .omega. and a on heat transfer coefficient are studied and explained with the boundary layer characteristics.

Numerical Simulation of the Aluminum Alloys Solidification in Complex Geometries

  • Monteiro Eliseu;Rouboa Abel
    • Journal of Mechanical Science and Technology
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    • v.19 no.9
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    • pp.1773-1780
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    • 2005
  • The process of mould design in the foundry industry has been based on the intuition and experience of foundry engineers and designers. To bring the industry to a more scientific basis the design process should be integrated with scientific analysis such as heat transfer. The production by foundry techniques is influenced by the geometry configuration, which affects the solidification conditions and subsequent cooling. Numerical simulation and/or experiments make possible the selection of adequate materials, reducing cycle times and minimizing production costs. The main propose of this work is to study the heat transfer phenomena in the mould considering the phase change of the cast-part. Due to complex geometry of the mould, a block unstructured grid and a generalized curvilinear formulation engaged with the finite volume method is described and applied. Two types of boundary conditions, diffusive and Newtonian, are used and compared. The developed numerical code is tested in real case and the main results are compared with experimental data. The results showed that the solidification time is about 6 seconds for diffusive boundary conditions and 14.8 seconds for Newtonian boundary conditions. The use of the block unstructured grid in combination with a generalized curvilinear formulation works well with the finite volume method and allows the development of more efficient algorithms with better capacity to describe the part contours through a lesser number of elements.

Effects of Periodic Blowing Through a Spanwise Slot on a Turbulent Boundary Layer (II) - Effects of Blowing Frequency - (슬릿을 통한 주기적 국소 가진이 난류경계층에 미치는 영향 (II) - 분사 주파수의 효과 -)

  • Kim, Kyoung-Youn;Sung, Hyung-Jin
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.28 no.1
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    • pp.41-51
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    • 2004
  • A direct numerical simulation is performed to analyze the effects of a localized time-periodic blowing on a turbulent boundary layer flow at R $e_{+}$=300. Main emphasis is placed on the blowing frequency effect on near-wall turbulent flow structures at downstream. Wall-normal velocity on a spanwise slot is varied periodically at different frequencies (0.004$\leq$ $f^{+}$$\leq$0.080). The amplitude of periodic blowing is $A^{+}$=0.5 in wall nit, which corresponds to the value of $v_{rms}$ at $y^{+}$=15 without blowing. The frequency responses are scrutinized by examining the phase or time-averaged turbulent statistics. The optimal frequency ( $f^{+}$=0.03) is observed, where maximum increase in Reynolds shear stress, streamwise vorticity fluctuations and energy redistribution occurs. The phase-averaged stretching and tilting term are investigated to analyze the increase of streamwise vorticity fluctuations which are closely related to turbulent coherent structures. It is found that the difference between PB and SB at a high blowing frequencies is negligible.e.e.

Electrochemical Characteristics of Welded Stainless Steels Containing Ti (Ti 함유된 스테인리스강 용접부의 전기화학적 특성)

  • Choe Han-Cheol
    • Journal of the Korean institute of surface engineering
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    • v.38 no.6
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    • pp.227-233
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    • 2005
  • Electrochemical characteristics of welded stainless steels containing Ti have been studied by using the electrochemical techniques in 0.5 M $H_2SO_4$+0.01 M KSCN solutions at $25^{\circ}C$. Stainless steels with 12 mm thick-ness containing $0.2{\~}0.9 wt\%$ Ti were fabricated with vacuum melting and following rolling process. The stainless steels were solutionized for 1hr at $1050^{\circ}C$ and welded by MIG method. Samples were individually prepared with welded zone, heat affected zone, and matrix for intergranular corrosion and pitting test. Optical microscope, XRD and SEM are used for analysing microstructure, surface and corrosion morphology of the stainless steels. The welded zone of the stainless steel with lower Ti content have shown dendrite structure mixed with $\gamma$ and $\delta$ phase. The Cr-carbides were precipitated at twin and grain boundary in heat affected zone of the steel and also the matrix had the typical solutionized structure. The result of electrochemical measurements showed that the corrosion potential of welded stainless steel were Increased with higher Ti content. On the other hand, reactivation($I_r$), passivation and active current($I_a$) density were decreased with higher Ti content. In the case of lower Ti content, the corrosion attack of welded stainless steel was remarkably occurred along intergranular boundary and ${\gamma}/{\delta}$ phase boundary in heat affected zone.