• Korean Journal of Materials Research
• /
• v.25 no.8
• /
• pp.386-390
• /
• 2015

Fe-base superalloy powders with $Y_2O_3$ dispersion were prepared by high energy ball milling, followed by spark plasma sintering for consolidation. High-purity elemental powders with different Fe powder sizes of 24 and 50 mm were used for the preparation of $Fe-20Cr-4.5Al-0.5Ti-O.5Y_2O_3$ powder mixtures (wt%). The milling process of the powders was carried out in a horizontal rotary ball mill using a stainless steel vial and balls. The milling times of 1 to 5 h by constant operation (350 rpm, ball-to-powder ratio of 30:1 in weight) or cycle operation (1300 rpm for 4 min and 900 rpm for 1 min, 15:1) were applied. Microstructural observation revealed that the crystalline size of Fe decreased with an increase in milling time by cyclic operation and was about 15 nm after 3 h, forming a FeCr alloy phase. The cyclic operation had an advantage over constant milling in that a smaller-agglomerated structure was obtained. The milled powders were sintered at $1100^{\circ}C$ for 30 min in vacuum. With an increase in milling time, the sintered specimen showed a more homogeneous microstructure. In addition, a homogenous distribution of Y-compound particles in the grain boundary was confirmed by EDX analysis.

• Journal of the Korean Recycled Construction Resources Institute
• /
• v.3 no.2
• /
• pp.115-121
• /
• 2015

The objective of this study is to present the design approach of low $CO_2$ concrete structures for reduction of $CO_2$ emissions. The design approach was implemented considering the system boundary for each processing presented in the ISO 13315-2. As for life-cycle inventory(LCI) for $CO_2$ assessment of concrete structures, data provided from domestic LCI DB was used. Based on the process presented in this study, case studies on the life-cycle $CO_2$ assessment of shear wall concrete structure was conducted. As substitution level of GGBS is 25%, the amount of $CO_2$ emissions and $CO_2$ uptake by concrete carbonation was decreased in the material, demolition and crushing, and transport phase. The amount of $CO_2$ emissions of column and total member was decreased by 26% and 22% respectively, compared to that of OPC.

• Journal of the Korean Electrochemical Society
• /
• v.14 no.1
• /
• pp.50-55
• /
• 2011

To enhance the performance of a MEA (membrane electrode assembly) in a polymer electrolyte membrane fuel cell (PEMFC), optimum contents of Nafion ionomer as electrolyte in the 20 and 40 wt% Pt/C used in electrodes were examined. Variety characterization techniques were applied to examine optimum Nafion contents: cell performance test, electrochemical impedance spectroscopy (EIS), and cyclic voltammetry (CV). According to Pt wt% supported on carbon support, it has been observed that polarization, ohmic, and mass transfer resistances were changed so that the cell performance was significantly dependent on the content of Nafion ionomer. Optimum Nafion ionomer contents in the 20 wt% Pt/C and 40 wt% Pt/C were showed 35 wt% and 20 wt%, respectively. This is due to different surface area of the Pt/C catalyst, and formation of triple phase boundary seems to be affected by the Nafion contents.

• The Korean Journal of Ceramics
• /
• v.5 no.2
• /
• pp.171-177
• /
• 1999

In the $(Pb_{1-x}M_x)[(Mn_{1/3}Sb_{2/3})_{0.05}Zr_yTi_{0.95-y}]O_3$ system, where M=Ca and Sr, the piezoelectric properties were evaluated to examine the possibility of application to piezoelectric transformer. A Rosen-type piezoelectric transformer was formed, then the electrical properties of voltage step-up ratio, frequency characteristics etc. were analysed. The morphotropic phase boundary was determined to be y=0.475 in $Pb[(Mn_{1/3}Sb_{2/3})_{0.05}Zr_yTi_{0.95-y}]O_3$ system and the piezoelectric properties of this composition was kp=0.59, Qm=1600 and $\varepsilon_r$=1150. Moreover, when 1-2 mol% of Sr are substituted, enhanced piezoelectric properties of kp=0.61, Qm=1600 and $\varepsilon_r$=1400 were shown. The temperature rising (ΔT) of a piezoelectric transformer with $Pb[Mn_{1/3}Sb_{2/3})_{0.05}Zr_{0.475}Ti_{0.475})]O_3 $ composition was $10^{\circ}C$, and the voltage step-up ratio was 500 when the output voltage was 4000V, whereas the ΔT was below $3^{\circ}C$ and the resonant frequency variation ($\Delta f_r$) as a function of load resistance was below 5% when the output voltage was 2000 V. These characteristics are superior to the properties of materials, which were substituted by Ca or without substitution.

• Journal of the Korean Ceramic Society
• /
• v.28 no.8
• /
• pp.625-625
• /
• 1991

The specimens for the corrosion test were made by hot-pressing of SiC power with 2 wt% Nl2O3 and 10wt% Al2O3 additions at 2000℃ and 2050℃. The specimens were corroded in 37 mole% NaCl and 63 mole% Na2SO4 salt mixture at 1000℃ up to 60 min. SiO2 layer was formed on SiC and then this oxide layer was dissolved by Na2O ion in the salt mixture. The rate of corrosion of the specimen containing 10 wt% Al2O3 was slower than that of the specimen containing 2 wt% Al2O3. This is due to the presence of continuous grain boundary phase in the specimen containing 10 wt% Al2O3. The oxidation of SiC produced gas bubbles at the SiC-SiO2 interface. The rate of corrosion follows a linear rate law up to 50 min. and then was accelerated. This acceleration is due to the disruption oxide layer by the gas evolution at SiC-SiO2 interface. Pitting corrosion has found at open pores and grain boundaries.

• Journal of the Korean Ceramic Society
• /
• v.45 no.4
• /
• pp.220-225
• /
• 2008

Lead-free ferroelectric ceramics are widely researched today for industrial applications as sensors, actuators and transducers. Since $Pb(Zr_aTi_{1-a})O_3$-(PZT) has high Curie temperature($T_C$), high piezoelectric properties near its morphotropic phase boundary(MPB) composition and small temperature dependence electrical behavior, it has been used to commercial materials for wide temperature range and different application fields. According to the tolerance factor concept, since the $Bi^{3+}$ cation with 12-fold coordinate has a smaller ionic radius than 12-fold coordinate $Pb^{2+}$, most bismuth based perovskites possess a smaller tolerance factor. Therefore, MPBs with a higher $T_C$ may be expected in $Bi(Me^{3+})O_3PbTiO_3$ solid solutions. As in lead based perovskite systems, it is clear that we need to explore more materials in simple or complex bismuth based MPB systems. The objective of this study is to investigate the $Bi(Ni_{1_a}X_a)O_3-PbTiO_3(X=Ti^{4+},\;Nb^{5+})$ perovskite solid-solution. For improving the electronic conduction problem, the magnesium and manganese modified system was also studied.

• Journal of the Microelectronics and Packaging Society
• /
• v.6 no.4
• /
• pp.23-33
• /
• 1999

A finite element method was employed fort thermal and stress analyses of an IGBT module of 3-phase full bridge. The effect of material parameters such as substrate material, substrate area, solder thickness on the temperature and stress distributions of the module packages has been investigated. Thermal analysis results have also been compared by setting of boundary conditions such as equivalent heat transfer coefficient or constant temperature at a base metal surface of the package. The increase of ceramic substrate area up to 3 times does little contribution to the reduction(8.9%) of thermal resistance, while contributed a lot to the reduction(60%) of thermal stress. Thicker solder resulted in higher thermal resistance but did slightly reduced thermal stresses. It is revealed by the stress analysis that maximum stress was induced at the region of copper pads which are bonded with ceramic substrate.

• The Transactions of the Korea Information Processing Society
• /
• v.4 no.7
• /
• pp.1694-1705
• /
• 1997

In the future mobile computing environment, it will be generalized that a mobile host with portable Laptop of Palmtop accesses to database through wireless communication channel. For solving the problems which are caused from low bandwidth of wireless communication, mobile hosts cache the datum used frequently on them. Thus the mobile hosts must always retain the cache consistency for the correctness of the cached datum. the cache consistency is mainly affected from the unrestricted host mobility and the disconnection of the communication between mobile hosts and mobile support station. In this situation, the strategy to retain efficiently cache consistency is required. In this paper, we propose a strategy using updatable message for retaining the cache consistency, in the mobile computing environment, with replicated database supporting 2 phase commit protocol. This strategy makes use of a updatable message to resolve the cache consistency problem, since mobile host crosses the boundary of cell. In using of this updatable, it find out and cache only the update data of missing invalidation message. As a result, the proposed strategy utilizes network bandwidth efficiently because it is not need to delete all the cached datum with any datum change.

• Journal of Korean Society of Coastal and Ocean Engineers
• /
• v.23 no.3
• /
• pp.205-214
• /
• 2011

Finite element grid refinements with different intensities having 14 K, 52 K and 211 K on the Yellow Sea (YS) have been constructed to make precise tidal simulations. In the meanwhile 57 K grid was made to the extended North Western Pacific (NWP) sea. Numerical simulation were done based on 32 parallel processors by using pADCIRC v 49.21 model. In the YS tidal simulation on YS-G52K and YS-G211K grid structure, KorBathy30s and ETOPO1 bathymetry data are used and 4 major tidal constituents are prescribed from FES2004. Computed results are in good agreement within 0.138 meter in RMS error for amplification and 14.80 degree of phase compared to observed tidal records. Similar error bounds are acquired in the extended NWP tidal simulation on NWP-G57K grid with 8 tidal constituent prescription on the open boundary.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.31 no.7
• /
• pp.41-52
• /
• 2003

In this paper, three-dimensional thermo-mechanical properties of carbon-phenolic 8-hamess satin weave composites were predicted considering geometric parameters of microstructures. The effective properties were calculated by a series of numerical experiments based on unit cell analysis. The microstructural details were modeled through macro-elements, and the periodic boundary conditions were derived for corresponding un it cell types. The Monte Carlo method was employed to consider the random phase shift between the layers, and the results were investigated on the effect of the geometric parameters of shift, number of layers and waviness ratios. Experimental tests were also performed and the results were compared.