• 제목/요약/키워드: Phase Stability

검색결과 1,974건 처리시간 0.032초

Y-TZP의 燒結性 및 相 安定性에 대한 CuO添加의 影響 (Influence of CuO Dopants on the Sintering Ability and Phase Stability of Yttria-Stabilized Tetragonal Zirconia Polycrystals)

  • 피재환;김윤해
    • 한국해양공학회지
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    • 제13권2호통권32호
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    • pp.35-40
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    • 1999
  • Effects of CuO addition on the sintering ability and the phase stability of Y-TZP. (Yttria doped Tetragonal Zirconia Polycrystals) were studied. The CuO dopants were found to be quite effective in reducing the sintering temperature to obtain full density and refining the grain size. The maximum allowable concentration of the dopants was limited to 0.3%mol% for CuO to maintain fully tetragonal phase. With the addition of these dopants, the flexual strength decreased by 20% in comparison with the undoped specimen but the fracture toughness increased by 15%.

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Phase stability and Morphology of high-k gate stack of $Si/SiO_2/HfO_2$ and $Si/SiO_2/ZrO_2$

  • Lee, Seung-Hwan;Bobade, Santosh M.;Yoo, W.J.
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2007년도 추계학술대회 논문집
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    • pp.118-119
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    • 2007
  • Phase stability and morphological investigation on the $Si/SiO_2/HfO_2$ and $Si/SiO_2/ZrO_2$ stack are presented. Thermal stability of $HfO_2$ and $ZrO_2$ determines the quality of interface and subsequently the performance of device. The stacks have been fabricated and annealed at $1000^{\circ}C$ for various time. In evolution of crystalline phase and morphology (electrical and geometrical) of high-k materials, annealing time and process are observed to be crucial factors. The crystallization of some phase has been observed in the case of $Si/SiO_2/HfO_2$. The chemical environment around Zr and Hf in respective samples is observed to be different.

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GeSbTe계 이중층의 상변화 특성에 미치는 열처리 온도 효과 (Effect of Annealing Temperature on Phase-change Characteristics of GeSbTe-based Bilayers)

  • 윤회진;방기수;이승윤
    • 한국전기전자재료학회논문지
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    • 제30권2호
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    • pp.86-90
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    • 2017
  • This work reports the phase-change behavior and thermal stability of doped GeSbTe/GeSbTe bilayers. We prepared the bilayers using RF sputtering, and annealed them at annealing temperature ranging from $100^{\circ}C$ to $400^{\circ}C$. The sheet resistance of the bilayer decreased and saturated with increasing annealing temperature, and the saturated value was close to that of pure GeSbTe film. The surface of the bilayer roughened at $400^{\circ}C$, which corresponds to the surface roughening of doped GeSbTe film. Mixed phases of face-centered cubic and hexagonal close-packed crystalline structures were identified in the bilayers annealed at elevated temperature. These results indicate that the phase-change behavior of the bilayer depends on the concurrent phase-transitions of the two GeSbTe-based films. The dopants in the doped GeSbTe film were diffused out at annealing temperatures of $300^{\circ}C$ or higher, which implies that the thermal stability of the bilayer should be considered for its application in phase-change electronic devices.

Phase Inversion Emulsification and Enhancement of Physical Properties for Cationic Emulsified Asphalt

  • Lee, Eun-Kyoung
    • Elastomers and Composites
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    • 제50권4호
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    • pp.265-273
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    • 2015
  • In this work, the emulsified asphalt with high phase stability and storage stability was prepared by using phase inversion emulsification and the surfactant mixed with cationic and nonionic surfactants. It was found that the asphalt together with Span 20, nonionic surfactant and DDA (Dimethyl Dodecyl Amine), cationic surfactant showed the most stable phase. The phase stability of the emulsified asphalt, therefore, was investigated through the particle size with mixed surfactant content, rheology behavior and Zeta potential value; the particle size decreased with the increase of the mixed surfactant content but the viscosity increased. The shear thinning behaviors and the Zeta potential value with 50 mV~60 mV were shown, which was found to be considered stable. In addition, SBR latex(Styrene-butadiene-rubber) and water dispersed Epoxy (EPD) were used to enhance the physical properties of the emulsified asphalt. The swelling and adhesion features of the emulsified asphalt were also studied with $CaCO_3$, Silica, and Montmorillonite (MMT). It was shown that the addition of SBR latex and MMT can be another way to improve the physical properties of the emulsified asphalt in that the lowest swelling feature was found.

상변위에 의한 동기전동기의 과도안정도 개선 (Improvement of Synchronous Motor Transient Stability by Phase Slipping)

  • 한송엽
    • 전기의세계
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    • 제21권2호
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    • pp.20-24
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    • 1972
  • The transient stability of the synchronous motor is generally improved by damper winding or flywheel. However the synchronous motor at full load will be pulled out from normal operation state when the period of power failure exceeds approximately ten cycle per second. This paper studies the method of improving the stability of synchronous motor by equipping the phase slipping switch between the motor and power source. This paper shows the motor does not pull out, which results from the decrease of power angle to about 30 electrical degrees by means of the switch even when the relatively long period of power failure brings the power angle to some 150 electrical degrees.

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$Pb(Zn_{0.6}Mg_{0.4})_{1/3}Nb_{2/3}O_3$ [PZMN] 계에서 A-자리 치환에 따른 상안정화 및 유전 특성 변화 (Variation of Dielectric Properties and Phase Stabilities with Substitution of A-Site in $Pb(Zn_{0.6}Mg_{0.4})_{1/3}Nb_{2/3}O_3$[PZMN] System)

  • 김봉철;김정주;김남경;조상희
    • 한국세라믹학회지
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    • 제33권10호
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    • pp.1131-1137
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    • 1996
  • The dielectric properties and phase stabilities of Pb(Zn0.6Mg0.4)1/3Nb2/3O3 [PZMN]system were investigated into substitution of A-site with Ba, Sr and Ca ions. The A-site substitutions led to the complexity of components of perovskite phase and then DPT coefficient increased. The A-site substitutions of Ba or Sr ion perovskite single phase could be easily formed by columbite process due to increase of perovskite phase stability. The variation of lattice parameters in specimen obeyed Vegard's law and curie temperature and dielectric constant of specimen decreased linearly. But Ca substitution led to perovskite phae instability. The lattice parameter dielectric constant and curie temperature of specimens drasticaly decreased with formation of pyrochlore phase.

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역도 인상동작 불안정성 수준에 따른 발바닥 체성감각요인 분석 (Factor Analysis of the Somatosensory for Foot according to the Instability Level of Snatch Lifting)

  • Moon, Young Jin
    • 한국운동역학회지
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    • 제30권1호
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    • pp.7-16
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    • 2020
  • Objective: It is to find factors related to stability through analysis of plantar pressure factors according to the level of instability when performing Snatch. Method: Foot pressure analysis was performed while 10 weightlifters performed 80% of the highest level of Snatch, and motion was classified and analyzed in 3 grades according to the level of instability. Results: First, in Bad Motion, the movement distance of the pressure center in the direction of ML and AP was larger significantly in Phase 2. Second, in Phase 2, the number of zero-crossing in the AP direction was larger statistically significantly in Good Motion. Third, in the bad motion in Phase 3, the number of zero-crossing in the ML direction showed a significantly larger value. Fourth, in Phase 4, it was found that the more stable the lock out motion, the greater the activity of foot controlling in the left and right directions. Fifth, Phase 3, the greater the Maximum/Mean foot pressure value, the more stable the pulling action. Sixth, in Phase 2, the foot pressure was concentrated with a wide distribution in the midfoot and rearfoot. Seventh, the triggering number of the forefoot region was small in the last pull phase. Eighth, the number of triggers in the toe area was significantly higher during Good Motion in Phase 4. Conclusion: Summarizing the factors of instability in Snatch, there was no significant difference in Phase 1 for each condition. In order to enhance the stability in Phase 2, the sensory control ability in the AP direction is required, and focusing the foot pressing motion with a wide distribution in the middle and rear parts increases the instability. In Phase 3, it was found that the more unstable, the more sensory control activity was performed in the ML direction, the stronger the forefoot pressing action should be performed for a stable Snatch. In Phase 4, It is important that the feet sensory control activity in ML directions and the control ability of the toes in order to have stable Lock out motion.

Solid-liquid phase equilibria on the GdBa2Cu3O7-δ stability phase diagram in low oxygen pressures (1 - 100 mTorr)

  • Lee, J.W.;Lee, J.H.;Moon, S.H.;Yoo, S.I.
    • 한국초전도ㆍ저온공학회논문지
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    • 제14권4호
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    • pp.28-31
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    • 2012
  • We report the solid-liquid phase equilibria on the $GdBa_2Cu_3O_{7-{\delta}}$ (GdBCO) stability phase diagram in low oxygen pressures ($PO_2$) ranging from 1 to 100 mTorr. On the basis of the GdBCO stability phase diagram experimentally determined in low oxygen pressures, the isothermal sections of three different phase fields on log $PO_2$ vs. 1/T diagram were schematically constructed within the $Gd_2O_3-Ba_2CuO_y-Cu_2O$ ternary system, and the solid-liquid phase equilibria in each phase field were described. The invariant points on the phase boundaries include the following three reactions; a pseudobinary peritectic reaction of $GdBCO{\leftrightarrow}Gd_2O_3$ + liquid ($L_1$), a ternary peritectic reaction of $GdBCO{\leftrightarrow}Gd_2O_3+GdBa_6Cu_3O_y$ + liquid ($L_2$), and a monotectic reaction of $L_1{\leftrightarrow}GdBa_6Cu_3O_y+L_2$. A conspicuous feature of the solid-liquid phase equilibria in low $PO_2$ regime (1 - 100 mTorr) is that the GdBCO phase is decomposed into $Gd_2O_3+L_1$ or $Gd_2O_3+GdBa_6Cu_3O_y+L_2$ rather than $Gd_2BaCuO_5+L$ well-known in high $PO_2$ like air.

골반안정화 운동프로그램이 엉치엉덩관절 통증을 동반한 만성요통환자의 통증과 엉덩관절에 미치는 영향 (The Effect of Pelvic Stability Exercise Program on Pain and Hip Joint of Patients with Chronic Low Back Pain involving Sacroiliac Joint Pain)

  • 강정일;최현
    • 디지털융복합연구
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    • 제11권4호
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    • pp.331-338
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    • 2013
  • 본 연구는 엉치엉덩관절 통증을 동반한 만성 요통환자 52명을 대상으로 6주 간 골반운동프로그램 및 전통적 물리치료를 병행한 실험군 27명과 전통적 물리치료만을 중재한 대조군 25명을 무작위 임상 표본 추출 하였다. 두 군 모두 통증의 정도를 알아보는 오스웨스트리-요통장애지수검사와 보행 시 엉덩관절의 각도분석을 한 후, 집단별 실험 전과 실험 후의 오스웨스트리-요통장애지수검사와 보행 시 엉덩관절의 각도분석을 비교하여 골반안정화 운동프로그램이 엉치엉덩관절 통증을 동반한 만성요통환자의 통증과 엉덩관절에 미치는 영향을 알아보고자 하였다. 요통의 변화는 집단 내와 집단 간에서 모두 유의하게 감소되었음을 알 수 있었고, 엉덩관절 각도비교에서는 실험군내 좌측 엉덩관절에서 중간디딤기, 말기디딤기, 유각전기, 초기흔들기와 우측 엉덩관절의 중간디딤기, 말기디딤기, 유각전기, 초기흔들기에서 차이가 있었다. 대조군 내 좌측 엉덩관절에서는 중간디딤기, 말기디딤기, 초기흔들기와 우측 엉덩관절의 체중전달기, 중간디딤기, 말기흔들기, 유각전기에서 유의한 차이가 있었다. 따라서 골반안정화 운동프로그램이 통증을 포함한 요통기능장애수준에 효과적이고 보행 시 입각기와 유각기 동안 엉덩관절의 굽힘과 폄이 리듬 있게 이동하여 보행이 대칭적으로 자연스럽게 이동되는데 도움이 되는 것으로 나타났다.

폐비닐로 개질된 아스팔트의 저장안정성에 관한 연구 (A Study on the Storage Stability of Waste Vinyl-Modified Asphalt)

  • 김강산;홍영근
    • Elastomers and Composites
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    • 제43권3호
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    • pp.191-198
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    • 2008
  • 아스팔트 개질재로 쓰이고 있는 폴리에틸렌은 아스팔트와의 비중차와 비상용성으로 인하여 상분리가 일어난다고 알려지고 있다. 본 연구에서는 상분리를 억제하기 위하여 폴리에틸렌을 가교시킬 수 있는 것으로 알려지고 있는 과산화물을 사용하여 상분리 억제를 시도하였다. 폴리에틸렌 수지로는 폐비닐을 사용하였으며, 과산화물로는 디큐밀퍼옥사이드와 로로일퍼옥사이드를 사용하였다. 현미경상으로는 과산화물이 첨가되어 상분리가 억제되었다. 그러나 유변물성을 측정한 결과는 아스팔트와 폴리에틸렌은(비록 폴리에틸렌이 가교된다 하더라도) 분자단위에서는 서로 섞일 수 없음을 보여주고 있다. 기계적 시험(인장강도, 마샬안정도, 동적안정도)에서는 매우 우수한 물성을 보여주어 소성변형에 대한 저항성이 크게 향상된 것으로 나타났고, 이는 기존의 슈퍼팔트보다 우수한 것으로 나타났다.