• Title/Summary/Keyword: Phase Composition

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Development of Drink from Composition with Medicinal Plants and Evaluation of Its Physiological Function (생약재를 이용한 음료의 개발 및 기능성 평가)

  • 박성혜;황호선;한종현
    • Journal of Nutrition and Health
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    • v.37 no.5
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    • pp.364-372
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    • 2004
  • The purpose of this study was to investigate the possibility of medicinal plants application as an edible functional food resource. We carried out to develop a traditional functional beverage by using hot-water extraction of 4 medicinal plants (Polygonatun sibiricum, Ophiopogonis radix, Lycii fructus, Schizandriae frutcus) and we examined the effects of drink on physiological response during exercise and recovery phase. The subjects were male baseball players, and exercise protocol was performed with 45 minutes treadmill running and 85% VO$_2$ max intensity. Brix, pH and titratable acidity of developed drink were 9.5%, 3.3 and 0.22%. The approximate nutritional composition of beverage was carbohydrate, 5.98%, total dietary fiber, 0.42%, crude protein, 0.70%, crude fat, 0.20% and crude ash, 0.20%. Developed. traditional functional beverage contained K (4.00 mg%), Na (3.68mg%), Ca (2.54mg%), Mg (1.60mg%) and Fe (0.29mg%). Developed beverage drinking group showed a lowest heart rate during exercise and recovery phase than the other two group (water group and ion beverage group). In the change of blood lactate concentration, developed beverage intake group showed a significant lowest values during exercise and recovery phase. And blood hematocrit values and osmolarity were lowest in the developed beverage intake group. In these results, exercise performance capacity was expected to improve most highly with the developed drink from composition with medicinal plants. Also developed beverage was effective in recovery of exercise-induced fatigue. Thus developed drink with medicinal plants can be used as a functional material improving decrease fatigue effects in beverage industry.

Ion Exchange Capacity and Phase Separation of Alkali Borosilicate Glass by Substituting $Al_2O_3$ (산화알루미늄의 치환에 따른 붕규산 유리의 분상 미 이온교환성에 관한 연구)

  • 김병호;유영문
    • Journal of the Korean Ceramic Society
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    • v.21 no.1
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    • pp.41-50
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    • 1984
  • The ion-exchange porous glasses were prepared by heat treating and subsequently acid treating the (95-y) $SiO_2$.$yB_2O_3$.$5Na_2O+xAl_2O_3$ glasses with y=55, 45, 35, 25. mole% and x=0, 2, 5, 9 mole% It was then investigated how the cation exchange capacity was affected by the phase separation in these glasses. For that matter such quantities as alkali extraction amount pore volume and specific surface area of the glasses were measured. The phase separation in these glasses was in general suppressed by the addition of $Al_2O_3$ maximally around the composition of 5 mole% $Al_2O_3$ This may be because the micro-phase separation prevailed in the glass of that composition over the macro-phase separation increasing thereby the specific surface area as well as the residual amount Al of after acid-treatment and accordingly the cation exchange capacity. The maximum values of the cation exchange capacity was observed to be about 150meq/100g for the glasses of (40-50) $SiO_2$ (55~45)$yB_2O_3$. $5Na_2O+5Al_2O_3$.

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Microstructural Behavior of Alumina Aggregate Compacts Prepared by Transient Liquid Phase Sintering

  • Lee, Seung-Jae;Kim, Hai-Doo;Lee, Deuk-Yong;Kim, Dae-Joon
    • The Korean Journal of Ceramics
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    • v.6 no.1
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    • pp.78-82
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    • 2000
  • Although alumina aggregates have been used as refractory aggregates due to the improved mechanical properties of refractories as a result of the low contraction of alumina aggregates, the aggregates have a difficulty in fabrication due to its low sinterability. Two types of alumina aggregates and a fused alumina aggregate containing transient liquid forming additives are prepared to investigate the sintering characteristics of aggregates. $Al_2O_3$rich composition in the $Al_2O_3$-MgO-$SiO_2$(-$TiO_2$) system is chosen for the transient liquid phase sintering and the final recrystallized bonding phase between grains inside the fused alumina aggregates is found to be a needle-like mullite phase. The flexural strength of alumina bars, reaction-bonded using the paste having a composition of $Al_2O_3$-MgO-$SiO_2$-$TiO_2$, is about 78 MPa, which is one half value of that of pure alumina.

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Separation of Glabridin from Licorice by RP-HPLC (RP-HPLC를 이용한 감초에서 Glabridin의 분리)

  • 정용안;이광진;권문주;노경호
    • KSBB Journal
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    • v.18 no.5
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    • pp.408-411
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    • 2003
  • By reversed-phase high-performance liquid chromatography, the extraction and separation of glabridin by from licoricce root was performed in this work. The column efficiencies and resolutions of glabridin were investigated with mobile phase composition on the reversed-phase chromatographic system. The glabridin collected from licorice root was identified by LC/MS. The mobile phase used to extract glabridin were composed of ethanol, methanol, acetone, and ethyl acetate. For one-hour ultrasonic extraction with solvent of ethyl acetate, the favorable content of glabridin was obtained as 1.26g/kg. The glabridin was well separated in the mobile phase composition of 50/50 vol. % (acetonitrile/water).

Characteristics of Housing Needs of Apartment Purchasers in Decision-making Steps (아파트 구매자의 구매의사결정 단계별 주요구 특성)

  • Ha, Jeung-Soon;Yoon, Jae-Woong
    • Journal of Families and Better Life
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    • v.24 no.6 s.84
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    • pp.33-45
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    • 2006
  • The purpose of this study was to find the characteristics of the housing needs of apartment purchasers in derision-making steps. The survey was took place from June to July, 2003 in the Daegu area. The data were collected from 1,187 married women using questionnaires and reponses were analyzed by SPSS Window Program. The results were as follows : 1. In the phase when housing problems are recognized the motives for moving were related to the floor space of the housing unit and the residential environment. 2. In the phase of acquiring information on apartments, the basis of the informations was mostly collected through conversations at model houses, from relatives, experts and real estate agents. 3. In the phase of considering alternative plans for apartment purchases, the factors considered were convenient interior space composition and educational environment for children. 4. In the phase of apartment purchase, the important factors was input from relatives and experts. 5. In the phase of post-purchase evaluation most discontent was related to privacy issues, interior space composition, and educational environment for children.

A simplified phase diagram in the ternary system $Y_2O_3-Ta(Nb)_2O_5-ZrO_2$ ($Y_2O_3-Ta(Nb)_2O_5-ZrO_2$ 삼성분계 상태도)

  • 이득용;김대준;장주웅;이명현
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.3
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    • pp.377-383
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    • 1997
  • Yttria-stabilized TZP alloyed with pentavalent oxides $(Ta_2O_5,\;Nb_2O_5)$ were fabricated by the conventional sintering method at $1500^{\circ}C$ in air to construct the simplified ternary phase diagram. The phase stability of tetragonal -$ZrO_2$ from the quasi-binary system $ZrO_2-YTa(Nb)O_4$, which do not transform to monoclinic-$ZrO_2$ even for a wide range of grain size and annealing temperature, was investigated to determine composition region of the non-transformable $t-ZrO_2$ solid solution$(NT_{ss})$. Phase stability of $NT_{ss}$ was probably due to the enhanced stability of $_YTa(Nb)O4$ having the tetragonal fergusonite structure. It was experimentally found that mixtures having $NT_{ss}$ alloyed with $T_{ss}$ by weight%% showed both excellent phase stability of $t-ZrO_2$ and fracture toughness even though the calculated composition of the mixture /was located outside $NT_{ss}$ composition region.

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Phase Diagrams and Stable Structures of Stranski-Krastanov Structure Mode for III-V Ternary Quantum Dots

  • Nakaima, Kazuno;Ujihara, Toru;Miyashita, Satoru;Sazaki, Gen
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1999.06a
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    • pp.81-114
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    • 1999
  • The strain, surface and inerfacial energies of III-V ternary systems were calculated for three kinds of structure modes: the Frank-van der Merwe (FM) mode, the Stranski-Krastanov (SK) mode an the Volmer-Wever (VW) mode. The free energy for each mode was estimated as functions of the thickness and composition or lattice misfit. Through comparison of the free energy of each mode, it was found that the thickness-composition phase diagrams of III-V ternary systems can be determined only by considering the balance of the free energy and three kinds of structure modes appear in the phase diagrams. The SK mode appears only when the lattice misfit is large and/or the lattice layer is thick. The most stable structure of the SK mode is a cluster with four lattice layers or minimum thickness on a wetting layer of increasing lattice layers. The VW mode appears when the lattice misfit is large and the lattice layer is thin and only in the InPSb/InP and GaPSb/GaP systems which have the largest lattice misfit of III-V ternary systems. The stable region of the SK mode in the GaPSb/GaP and InPSb/InP phase diagrams is largest of all because the composition dependence of the strain energy of these systems is stronger than that of the other systems. The critical number of lattice layers below which tow-dimensional (2D) layers precede the three-dimensional (3D) nucleation in the SK mode at x=1.0 depnds on the lattice misfit.

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Estimation of the chemical compositions and corresponding microstructures of AgInCd absorber under irradiation condition

  • Chen, Hongsheng;Long, Chongsheng;Xiao, Hongxing;Wei, Tianguo;Le, Guan
    • Nuclear Engineering and Technology
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    • v.52 no.2
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    • pp.344-351
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    • 2020
  • AgInCd alloy is widely used as neutron absorber in nuclear reactors. However, the AgInCd control rods may fail during service due to the irradiation swelling. In the present study, a calculational method is proposed to calculate the composition change of the AgInCd absorber. Calculated results show that neutron fluence has significant impact on the chemical compositions. Ag and In contents gradually decrease while Cd and Sn conversely increases from the center to the rim of AgInCd absorber due to the depression of neutron flux. The composition change at the surface is higher almost two times than that at the center. Based on the calculated compositions, six simulated AgInCdSn alloys were prepared and examined. With the increase of Cd and Sn, the simulated AgInCdSn alloys transform from a single fcc phase into the mixed fcc and hcp phases, and finally into the single hcp phase. The atomic volume of the hcp phase is obviously larger than the fcc phase. The fcc-hcp transformation results in considerable volume swelling of the AgInCd absorber. Moreover, the lattice parameters of the fcc and hcp phases gradually increase with Cd and Sn contents, which also can induce small volume swelling.

Orientation Measurement and Related Mechanical Properties of Directionally Solidified NiAl/$Ni_3Al$ Two-Phase Alloys (일방향응고된 NiAl/$Ni_3Al$ 2상합금의 방향성 측정 및 기계적 특성 평가)

  • Lee, Hye-Jung;Park, No-Jin;Choi, Hwan;Lee, Je-Hyun;Oh, Myung-Hoon
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.2
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    • pp.96-103
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    • 2010
  • $Ni_3Al$ is known as a good high temperature structural material because of high yield strength at ambient temperature. However, it is too brittle to use as a structural material because of their weak grain boundary. In this work, orientation measurement and related mechanical properties of directionally solidified NiAl/$Ni_3Al$ two-phase alloys with various compositions (Ni-23~27 at.%Al) were investigated for developing multi-phase DS-processed alloys with the growth rates of 10, 50 and 100 ${\mu}m/s$ in a modified Bridgeman type furnace. It was found that the multi-phase microstructures such as the $\gamma$ dendrite +${\gamma}'$ matrix duplex microstructure was formed in the hypoeutectic composition of 23 at.%Al, $\beta$ dendrite +${\gamma}'$ matrix duplex microstructure in the hypereutectic composition of 26 and 27 at.%Al. And ${\gamma}'$ single phase was formed in the composition of 24.5 and 25 at.%Al. The hypoeutectic alloy including $\gamma$ dendrites with ${\gamma}'$ matrix showed a large elongation of over 70% at room temperature. However, the room-temperature tensile elongation decreased with increasing Al contents because the volume fraction of brittle $\beta$ dendrites in the ductile ${\gamma}'$ matrix increased.

HPLC Separation of Isoquinoline Alkaloids for Quality Control of Corydalis species

  • Kim, Eun-Kyung;Jeong, Eun-Kyung;Han, Sang-Beom;Jung, Jee-H.;Hong, Jong-Ki
    • Bulletin of the Korean Chemical Society
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    • v.32 no.10
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    • pp.3597-3602
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    • 2011
  • A simple and rapid analytical method was developed for the determination of eight isoquinoline alkaloids in Corydalis species. Eight isoquinoline alkaloids, including 2 aporphine alkaloids (isocorydine and glaucine) and 6 protoberberine alkaloids (coptisine, palmatine, berberine, canadine, corydaline, and tetrahydrocoptisine) were used as chemical markers which have a various biological activity and determined for quality control of Corydalis (C.) species (C. ternata, C. yanhusuo, and C. decumbens). To evaluate the quality of these herbal medicines, LC chromatographic separation of alkaloids were preferentially investigated on reversed-phase C18 column with pH variation and composition of mobile phase. In addition, the separation of these alkaloids in herbal extracts was found to be significantly affected on mobile phase composition using gradient elution. Especially for C. yanhusuo extract, berberine was seriously interfered with other alkaloid extracted from sample matrix when mobile phase composition was not optimized. As results, these compounds were successfully separated within 28 min using 10 mM ammonium acetate containing 0.2% triethylamine (adjusted at pH 5.0) as a mobile phase with gradient elution. On the basis of optimized HPLC conditions, 23 different Corydalis species samples were analyzed for the determination of alkaloid levels. In addition, principal component analysis (PCA) combined with the chromatographic data could be successfully classified the different geographic origin samples.