• Title/Summary/Keyword: Peeling off

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Fabrication of Core-Shell Structure of Ni/Au Layer on PMMA Micro-Ball for Flexible Electronics

  • Hong, Sung-Jei;Jeong, Gyu-Wan;Han, Jeong-In
    • Current Photovoltaic Research
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    • v.4 no.4
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    • pp.140-144
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    • 2016
  • In this paper, core-shell structure of nickel/gold (Ni/Au) conductive layer on poly-methyl-methacrylate (PMMA) micro-ball was fabricated and its conduction property was investigated. Firstly, PMMA micro-ball was synthesized by using dispersion polymerization method. Size of the ball was $2.8{\mu}m$ within ${\pm}7%$ deviation, and appropriate elastic deformation of the PMMA micro-ball ranging from 31 to 39% was achieved under 3 kg pressure. Also, 200 nm thick Ni/Au conductive layer was fabricated on the PMMA micro-ball by uniformly depositing with electroless-plating. Adhesion of the conductive layer was optimized with help of surface pre-treatment, and the layer adhered without peeling-off despite of thermal expansion by collision with accelerated electrons. Composite paste containing core-shell structured particles well cured at low temperature of $130^{\circ}C$ while pressing the test chip onto the substrate to make electrical contact, and electrical resistance of the conductive layer showed stable behavior of about $6.0{\Omega}$. Thus, it was known that core-shell structured particle of the Ni/Au conductive layer on PMMA micro-ball was feasible to flexible electronics.

Corrosion Behavior and Oxide Film Formation of T91 Steel under Different Water Chemistry Operation Conditions

  • Zhang, D.Q.;Shi, C.;Li, J.;Gao, L.X.;Lee, K.Y.
    • Corrosion Science and Technology
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    • v.16 no.1
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    • pp.8-14
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    • 2017
  • The corrosion behavior of a ferritic/martensitic steel T91 exposed to an aqueous solution containing chloride and sulfate ions is investigated depending on the stimulated all-volatile treatment (AVT) and under oxygenated treatment (OT) conditions. The corrosion of T91 steel under OT condition is severe, while the corrosion under AVT condition is not. The co-existence of chloride and sulfate ions has antagonistic effect on the corrosion of T91 steel in both AVT and OT conditions. Unlike to corrosion resistance in the aqueous solution, OT pretreatment provides T91 steel lower oxidation-resistance than VAT pretreatment. From scanning electron microscopy/energy dispersive X-ray spectroscopy (SEM/EDS) and X-ray diffraction (XRD) analysis, the lower corrosion resistance in the aqueous solution by VAT conditions possibly is due to the formation of pits. In addition, the lower oxidation resistance of T91 steel pretreated by OT conditions is explained as follows: the cracks formed during the immersion under OT conditions accelerated peeling-off rate of the oxide film.

A fundamental Study on the Performance Improvement of Hwangto plaster (황토미장재 성능개선을 위한 실험적 연구)

  • Hwang, Hey-zoo;Lee, Jong-kuk;Kang, Nam-yi
    • KIEAE Journal
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    • v.5 no.3
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    • pp.49-56
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    • 2005
  • Recently the Volatile Organic Compound, HCHO, a harmful object spout from the construction materials is made an issue of social problem. Also the appearance of the building where the confidentiality is high was interior air pollution and it was brought about a huge problem. The government research facility and a relation industry sector conducts a many effort to improves like this actual condition. The Diverse ability building material which contains the natural material of the jade, the charcoal and the hwangto instead of the finish material which contains the harmful chemical material, is becoming development and utility. Hereupon the study have carried out research on hwangto plaster that was composed of hwangto and rice straw. The result of test that is deduced by basic proportion is properly appeared with suitable ratio of the hwangto and the sand to 4:6~5:5 by the compressive strength and crack control, workability. The result of test, that adds the rice straw to basic blending for a crack control, appeared with the fact that it is most suitable 3%to add the rice straw that has a length of 0.5cm~2cm. The result of test that plaster over the large size to compare a cement plaster with a hwangto plaster show a similar efficiency by workability. Also it controlled the crack and peeling off actual condition which is discovered from the hwangto plaster of existing perfectly.

A Study on the Characteristics of Cast Bonding Aluminium Alloy and Fe-17wt%Cr Steel with Vacuum Die Casting (진공다이캐스트법에 의한 Al합금과 Fe-17wt%Cr 강의 주조접합 특성연구)

  • Kim, Yong-Hyun;Kim, Eok-Soo;Kim, Heung-Sik;Lee, Kwang-Hak
    • Journal of Korea Foundry Society
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    • v.19 no.5
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    • pp.410-418
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    • 1999
  • To overcome the undesirable deformation, peeling off and geometrical restrictions which were mainly caused by differences in thermal expansion coefficients during the cladding of aluminum strip and stainless strip, new processing method based on vacuum die casting is designed and implemented in fabricating Fe-17wt%Cr steel (stainless steel). To increase cast-bonding ability, the surface of Fe-17wt%Cr steel is electrochemical etched to have optimum pit size (above 0.2 mm) and pit density (above 30%). The implementation of vacuum die casting by using surface treated stainless steel (Fe-17wt%Cr Steel) produces good trial products having acceptable cast-bonding ability. The enabling conditions for cast-bonding are pouring temperature $690^{\circ}C$, filling speed 30 m/sec and casting pressure $800\;kg/cm^2$. The microscopic observation of cast-bonded Al/Fe-17wt%Cr steel does not show any evidence of intermetallic compounds. The bonding strength of trial products is $150-400\;kg/cm^2$ and this is stronger than conventionally cladded metal having $30-70\;kg/cm^2$.

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Treatment of Morsicatio Buccarum by Oral Appliance: Case Report

  • Chang, Min;Kim, Jiyeon;Park, YounJung;Kwon, Jeong-Seung;Kim, Seong-Taek;Choi, Jong-Hoon;Ahn, Hyung-Joon
    • Journal of Oral Medicine and Pain
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    • v.46 no.3
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    • pp.84-87
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    • 2021
  • Morsicatio buccarum is a condition caused by chronic cheek biting. It means frictional hyperkeratosis by repetitive cheek biting, which may be associated with obsessive compulsion. Clinically it presents as rough, shaggy, whitish, often peeling surface. We report a 9-year-old female patient who complained oral ulceration on both buccal mucosa. The initial diagnosis was oral candidiasis because of whitish plaques which were peeled off. Topical antifungal agent was ineffective and the symptom did not disappear. By incisional biopsy, she was diagnosed with morsicatio buccarum. A soft oral appliance was placed in the patient's oral cavity. Although morsicatio buccarum improved significantly when the appliance was used, the oral lesion had a tendency to recur, when the patient stopped using the appliance. In case of recurrence, cognitive behavioral therapy for obsessive-compulsive disorder is needed for the fundamental treatment.

Real Time Analysis of Friction/Wear Characteristics of Metal Coatings with a Tribo-tester Installed in an SEM (SEM 내부에 설치된 트라이보 시험기를 통한 금속 코팅의 실시간 마찰/마모 특성 분석)

  • Kim, Hae-Jin;Kim, Dae-Eun;Kim, Chang-Lae
    • Tribology and Lubricants
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    • v.34 no.6
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    • pp.318-324
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    • 2018
  • This study aims to visualize the friction and wear behaviors of metal coatings in real time. The main mechanism of wear is identified by observing all the processes in which wear occurs. The friction coefficients of the moments are monitored to confirm the relationship between the friction and wear characteristics of the coating. Thin Ag coatings, which are several hundred nanometers in thickness, are prepared by depositing Ag atoms on silicon substrates through a sputtering method. A pin-on-disk-type tribo-tester is installed inside a scanning electron microscope (SEM) to evaluate the friction and wear characteristics of the Ag coating. A fine diamond pin is brought into contact with the Ag coating surface, and a load of 20 mN is applied. The contact pressure is calculated to be approximately 15 GPa. The moments of wear caused by the sliding motion are visualized, and the changes in the friction characteristics according to each step of wear generation are monitored. The Ag coating can be confirmed to exhibit a wear phenomenon by gradually peeling off the surface of the coating on observing the friction and wear characteristics of the coating in real time inside the SEM. This can be explained by a typical plowing-type wear mechanism.

Evaluation of Friction and Wear Characteristics of Carbon-based Solid Lubricant Films for Surface Application of Compressor Parts (압축기 부품소재 표면 적용을 위한 탄소 기반 고체 윤활막의 마찰 및 마모 특성 평가)

  • Lee, Sung-Jun;Kim, Chang-Lae
    • Tribology and Lubricants
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    • v.38 no.5
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    • pp.222-226
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    • 2022
  • Between diaphragms made of stainless steel (SUS), which is the main component of a hydrogen gas compressor, micro-slip occurs owing to repeated bending, resulting in scratches on the surface. The surface scratch of the compressor part is a problem with airtightness, which reduces the efficiency of the compressor; in severe cases, damage is a possibility. In this study, the changes in friction and wear characteristics due to the surface polishing of SUS and carbon-based solid lubricant films (graphene and CNT) were analyzed. Bare SUS, polished SUS, graphene film, and CNT film specimens were prepared. The surface roughness of the SUS was significantly reduced by surface polishing but increased by carbon-based solid lubricating films. In contrast, the friction coefficient maintained a similar value after surface polishing but was significantly reduced by the carbon-based solid lubricant films. In particular, the graphene film exhibited the lowest initial friction coefficient, while the CNT film exhibited the lowest overall average friction coefficient. Regarding the wear rate, polished SUS exhibited the lowest value, but the surface condition of the wear track showed that the carbon-based solid lubricating films were relatively less damaged. Although the wear rate measured was largely attributed to the solid lubricating film peeling off, the SUS surface under the film was considered protected.

Studies on the AFM analysis of Cu CMP processes for pattern pitch size and density after global planarization (패턴 피치크기 및 밀도에 따른 Cu CMP 공정의 AFM 분석에 관한 연구)

  • 김동일;채연식;윤관기;이일형;조장연;이진구
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.35D no.9
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    • pp.20-25
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    • 1998
  • Cu removal rates for various SiO$_2$ trench pitch sizes and densities and AFM images of surface profiles after global planarization using Cu CMP technology are investigated. In the experimental results, Cu removal rates are increasing as the pattern densities and pattern pitches are getting high and low, respectively, and then decreasing after local planarization. The rms roughness after global planarization are about 120$\AA$. AFM images with a 50% pattern density for 1${\mu}{\textrm}{m}$ and 2${\mu}{\textrm}{m}$ pitches show that thicknesses of 120~330$\AA$ Cu interconnects have been peeled off and oxide erosion of Cu/Sio$_2$ sidewall is observed. However, AFM images with a 50% pattern density for 10${\mu}{\textrm}{m}$ and 15${\mu}{\textrm}{m}$ pitches show that 260~340$\AA$ thick Cu interconnects have been trenched at the boundaries of Cu/Sio$_2$ sidewall.

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Study on the Radiation Dose about Skin Thickness of Rat (For Radiation Damage Tissue Engineering) (쥐의 피부두께에 따른 선량연구)

  • Jung, Hongmoon;Won, Doyeon;Kim, Hyeongyun;Jung, Jaeeun;Choi, hyeun-woo
    • Journal of the Korean Society of Radiology
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    • v.10 no.6
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    • pp.375-379
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    • 2016
  • A rat is the most common experimental animal used for the realization of the radiation injury model. The certain thickness of rat skin was prepared by peeling off a rat skin. Radiation level was measured by using this rat skin. Also, The schematic of the formula was made that can predict the radiation absorbed dose (RAD) as a function of the thickness of the rat skin. Consequently, we will provide the RAD information in the realization of in-vitro experimental model regarding the rat's skin thickness by applying the formulas. Moreover, the results from this study can be effectively used for the in-vitro experiment of the rat subcutaneous tissue which was exposed to radiation.

Influence of Sputtering Conditions on Structural and Electrochemical Properties of the Si Anode Film for Lithium Secondary Batteries (리튬 이차전지에서 Si 음극박막의 스퍼터링 증착조건에 따르는 구조적, 전기화학적 특성 연구)

  • Joo, Seung-Hyun;Lee, Seong-Rae;Cho, Won-Il;Cho, Byung-Won
    • Korean Journal of Materials Research
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    • v.19 no.2
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    • pp.73-78
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    • 2009
  • This study investigated the dependence of the various sputtering conditions (Ar pressure: $2{\sim}10\;mTorr$, Power: $50{\sim}150\;W$) and thickness ($50{\sim}1200\;nm$) of Si thin film on the electrochemical properties, microstructural properties and the capacity fading of a Si thin film anode. A Si layer and a Ti buffer layer were deposited on Copper foil by RF-magnetron sputtering. At 10 mTorr, the 50 W sample showed the best capacity of 3323 mAh/g, while the 100 W sample showed the best capacity retention of 91.7%, also at 10 mTorr. The initial capacities and capacity retention in the samples apart from the 50W sample at 10 mTorr were enhanced as the Ar pressure and power increased. This was considered to be related to the change of the microstructure and the surface morphology by various sputtering conditions. In addition, thinner Si film anodes showed better cycling performance. This phenomenon is caused by the structural stress and peeling off of the Si layer by the high volume change of Si during the charge/discharge process.