• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제55권4호
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• pp.166-171
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• 2006

In this paper, we have studied for analysis of the partial discharge(PD) signal in underground transmission line. The PD signal has estimated as detected signal accumulation of a PRPDA method by using Labview, and analyzed with fuzzy algorithm. In our algorithm, we developed system configuration that detected accumulating PD signal using by Labview and programmed fuzzy algorithm can be analyzed the PD signal using with Matlab. With practical PD logic implementation of theoretical detected system and hardware implementation, the device for Hipotronics Company's 50kV setup has generated and then has applied with $15k{\sim}17kV$ with 1:1 time probe. It's also used the LDPE 0.27mmt (scratch error 0.05mmt) to sample for making PD. In conclusion, Our new class of PD detected algorithm has also compared with previous PRPDA or Fuzzy algorithm. which has diagnose more conveniently by adding numerical values.

• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제51권5호
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• pp.199-204
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• 2002

In order to recognize the deterioration of insulation system by partial discharge (PD), the characteristics of PD patterns which are occurring at the interface between epoxy and rubber materials in extra high voltage cable joints, have been investigated. The artificial defects such as voids, metal particles, insulation fiber and water impregnated insulation fiber are planted between the interfaces. A high frequency partial discharge detection system was used for measuring PD signals. An analysis of the PD patterns is focused on the shape of PD pattern, phase, width and time-dependence for each artificial defect. The PD Patterns in each defect show the different behaviors and it is suggested that the precise discrimination of PD patterns could be used for the diagnosis of deterioration in the insulation systems.

• 대한치과기공학회지
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• 제15권1호
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• pp.5-25
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• 1993

Effects of hydrogenation on microstructure and mechanical properties of pure Ti and Ti-0.15Pd alloy have been studied by means of optical microscopy, differential scanning calorimeter(DSC), Xray diffraction and micro vicker's hardness test. Grain size of pure Ti and Ti-0.15Pd alloy decresed largely by hydrogenation finer than that of pure Ti and the grain size refinement was evedent in Ti-0.15Pd alloy than that in pure Ti. Ti-.015Pd alloy carried out solution treatment at 950$^{\circ}C$, the transformation of $\alpha$' martensite was occured. The amount of Hydrogen absorption in Ti-.015Pd alloy was higher than that in pure Ti. Decomposition of hydride in pure titanium and Ti-0.15Pd alloy increased largely by hydrogenation, and micro vicker's hardness of Ti-.015Pd alloy was largely than that of pure Ti by 30% after hydrogenation. The micro vicker's hardness of Ti-0.15Pd alloy after solution treatment and dehydrogenation were higher at $\beta$ phase ranger(950$^{\circ}C$) than that phase range(750$^{\circ}C$).

• 한국결정학회지
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• 제12권1호
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• pp.10-13
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• 2001

Compound PdCl₂(PhCN)₂(1) reacted with tert-butylamine(t-BuNH₂) to give trans-[PdCl₂(t-BuNH₂)₂] (2) Compound 2 was characterized by spectroscopy (¹H-NMR, /sup 13/C{¹H}-NMR, and IR) and X-ray diffraction. Crystallographic data for f2: monoclinic space group p2₁/c, a=6.298(1)Å, b=20.740(2)Å, c=10.731(1)Å, β=92.58(1)°, Z=4, R(wR₂)=0.0207(0.0543).

• Bulletin of the Korean Chemical Society
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• 제35권7호
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• pp.1979-1984
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• 2014

We have developed an efficient method to generate highly active Pd and PdO nanoparticles (NPs) dispersed on graphene and graphene oxide (GO) by an impregnation method combined with thermal treatments in $H_2$ and $O_2$ gas flows, respectively. The Pd NPs supported on graphene (Pd/G) and the PdO NPs supported on GO (PdO/GO) demonstrated excellent carbon-carbon cross-coupling reactions under a solvent-free, environmentally-friendly condition. The morphological and chemical structures of PdO/GO and Pd/G were fully characterized using X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and transmission electron microscopy (TEM). We found that the remarkable reactivity of the Pd/G and PdO/GO catalysts toward the cross-coupling reaction is attributed to the high degree of dispersion of the Pd and PdO NPs while the oxidative states of Pd and the oxygen functionalities of graphene oxide are not critical for their catalytic performance.

• 한국수소및신에너지학회논문집
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• 제27권3호
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• pp.283-289
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• 2016

In this study, electrochemical characterizations of PdCu/C catalysts that are synthesized by modified polyol method are investigated. Most of all, amount of ethylene glycol (EG) that is used as main component for catalyst synthesis is mainly modulated to optimize synthetic condition of the PdCu/C catalyst, For evaluations about catalytic activity and performance of direct formic acid fuel cell (DFAFC), half cell and full cell tests are implemented. As a result, when amount of EG is 4M, catalytic activities of the PdCu/C catalyst such as peak current of formic acid oxidation and active surface area are best, while maximum power density of DFAFC using the optimized PdCu/C catalyst is better than that using commercial Pd/C (30 wt%) by 6%. Based on that, PdCu/C catalyst synthesized by modified polyol method plays a critical role in improving (i) catalytic activity for formic acid oxidation and (ii) DFAFC performance by employing as anodic catalyst.

• 한국재료학회지
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• 제4권3호
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• pp.295-300
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• 1994

이 논문은 $SnO_2$에 소량의 Pd를 첨가하여 이것을 $Al_2O_3$기판위에 진공증착시켜 가스소자를 제작한 후, 소자의 감지특성에 영향을 미치는 열처리 온도, 소자의 온도, Pd의 첨가량의 변화 효과를 조사한 것이다. 소자의 열처리 온도가 $550^{\circ}C$일때와 소자의 동작온도가 $350^{\circ}C$일때 ethanol gas에 접촉시 소자 저항이 가장 낮았다. Pd 1 wt%를 첨가한 경우 에탄올 가스에 대한 소자의 감지특성이 가장 양호하였으며, 저농도 영역에서 특히 우수하였다.

• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제54권7호
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• pp.332-338
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• 2005

PD(Partial Discharge) signal emitted from PD sources has their intrinsic features in the region of time and frequency STFT(Short Time Fourier Transform) shows time-frequency distribution at the same time. 2-Dimensional matrices(33$\times$77) from STFT for PD pulse signals are a good feature vectors and can be decreased in dimension by wavelet 2D data compression technique. Decreased feature vectors(13$\times$24) were used as inputs of Back-propagation ANN(Artificial Neural Network) for discrimination of Multi-PD sources(air discharge sources(3), surface discharge(1)). They are a good feature vectors for discriminating Multi-PD sources in the air.

• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제52권10호
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• pp.431-435
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• 2003

It is very difficult and dangerous to measure PD(Partial Discharges) from high voltage equipments in outdoor situation. But that is very important thing for preventing them from more serious accident by defects made by insulating degradation. This paper provides useful method to detect PD signals easily without any dangerous situation. Electric field sensor by the principle of capacitor can detect PD signals without direct connection between sensor and high voltage equipment and has very wide frequency range suitable for noise rejection. Electric field sensor and related circuit for processing PD signal show good performance as a PD sensor when it is applied to simulated high power equipment generating PD pulses.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2001년도 하계학술대회 논문집 C
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• pp.1673-1675
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• 2001

In this paper, Partial Discharge(PD) patterns are compared by means of Low Frequency PD(LFPD, based on the IEC 270) and recently proposed High Frequency PD(HFPD). For this purpose, three different types of artificial defects are provided such as corona in air, void in epoxy insulator and needle defect in XLPE cable insulation. PD were generated from each defect and then detected respectively by two different methods such as LFPD and HFPD. As a result, remarkable resemblance in PD pattern for differ detecting method have been observed from each defect. Accordingly, it could be deduced that the pattern recognition by LFPD could be regarded as the reference for the investigations by HFPD.