• 제목/요약/키워드: Particle Size Measurement

검색결과 444건 처리시간 0.026초

MICRSTRUCTURAL INVESTIGATION OF CALCINED AND SULFATED LIMESTONE FOR THE UTILIZAION IN THE AFBC ENVIRONMENT

  • Kim, Hyung-Taek;Kim, Dong-Hyung;Kim, Hong-Tae;Hyukbo Kwon
    • 한국표면공학회지
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    • 제26권5호
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    • pp.255-262
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    • 1993
  • Major parameters determining the extent of Ca utilization were investigated for their calcination/sulfation behavior of limestone in the AFBC(Atmospheric Fluidized Bed Combustion) environments. Three different particle sizes of Fredonia limestone were investigated in the lab-scale tubular reactor. The results of the calcination codnversion of limestone imply that thesd decomposition rate of CaCO3 into CaO is dependent on the amount of heat which limestone absorbed. Hg porosimeter measurement of calcined limestone illustrated that surface area and pore volume are increased with decreasing particle size. Raw Fredonia limestone and sequentially as well as simultaneously calcined/sulfated limestones were also examined using SEM. The SEM Studied showed that the surface of the calcined limestone particles is more diffusive nature than that of the parent calcite. However, the sulfur distribution pattern of simultaneously-treated particles and that of the se-quentially-treated one shows no difference.

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고점성 유체 내부에서의 다상유동장 가시화 및 PIV 측정 (Flow Visualization and PIV Measurement of Multiphase Flow in Highty Viscous Liquid)

  • 김현동;류승규;김경천
    • 한국가시화정보학회:학술대회논문집
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    • 한국가시화정보학회 2006년도 추계학술대회 논문집
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    • pp.48-54
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    • 2006
  • A visualization study of flow characteristics in a mixer using multi-nozzle bubbling was performed. The mixer is filled with liquid glycerin (dynamic viscosity = $1000mPa{\cdot}$ s at $25^{\circ}C$) and convective mixing is induced by air bubbles generated from 9 orifices installed on the bottom of the mixer. To visualize the flow field, PIV (Particle Image Velocimetry) system consisting of 532nm Nd:YAG laser, $2k\times2k$ CCD camera and synchronizer is adopted. The bubbles generated with uniform size and frequency form bubble stream, and bubble streams rise vertically without interaction between bubble streams. Mixing efficiency is affected by the height of bubbler and the effective height of bubbler is 20mm from the bottom of the mixer.

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화학적 기계 연마(CMP)에 의한 단결정 실리콘 층의 평탄 경면화에 관한 연구 (Planarization & Polishing of single crystal Si layer by Chemical Mechanical Polishing)

  • 이재춘;홍진균;유학도
    • 한국진공학회지
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    • 제10권3호
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    • pp.361-367
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    • 2001
  • CMP(Chemical Mechanical Polishing)는 반도체 소자 제조공정 중 다층 배선구조의 평탄 경면화에 널리 이용되고 있다. 차세대 웨이퍼로 각광받는 SOI(Silicon On Insulator) 웨이퍼 제조공정 중 웨이퍼 표면 미소 거칠기를 개선하기 위해서 본 논문에서는 여러 가지 가공변수(슬러리와 연마패드)에 따른 CMP 연마능률과 표면 미소 거칠기 변화에 대해 연구하였다. 결과적으로 연마능률은 슬러리의 입자 크기가 증가할수록 이에 따라 증가하였으며, 미소 거칠기는 슬러리의 연마입자보다는 연마패드에 영향이 더욱 지배적이다. AFM(Atomic Force Microscope)에 의한 평가에서 표면 미소 거칠기가 27 $\AA$ Rms에서 0.64 $\AA$ Rms로 개선됨을 확인할 수 있었다.

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Dispersive Activity and Physical Properties of Exopolysaccharide (Cystan) produced by Cystobacter sp. MSL-9

  • 이강모;김세경;이문원;최선영;이운택;윤현식
    • 한국생물공학회:학술대회논문집
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    • 한국생물공학회 2003년도 생물공학의 동향(XII)
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    • pp.719-723
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    • 2003
  • Cystan의 분산활성은 점토광물에 대한 침강속도가 완연히 느려짐을 확인하여 분산제로서의 성능이 우수함을 볼 수 있었으며, 넓은 범위의 중성 pH에서는 고르게 분산활성을 유지하는 것으로 밝혀졌다. 이는 rheological test에서도 알 수 있었는데, 여러 pH와 온도에서의 Cystan 용액의 점도측정결과 넓은 영역에서 pH 및 온도 변화에 따른 큰 차이가 없었다. Cystobacter sp. MSL-9에 의해 생산되는 Cystan은 분산활성과 안정성이 높으며 기존 화학분산제보다 환경친화적이어서 그 산업적 가치가 클 것으로 기대된다.

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정수처리시 Fe(III) 응집제를 사용한 응집동력학에 대한 온도의 영향 (Effects of Temperature on Flocculation Kinetics Using Fe(III) Coagulant in Water Treatment)

  • 강임석
    • 한국환경과학회지
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    • 제4권2호
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    • pp.181-194
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    • 1995
  • 여러가지 다양한 상수처리 실험조건에서 응집제로 Ferric Nitrate를 사용하여 수증의 카오린 점토입자를 응결하는 과정중의 응집동력학을 조사하기 위하여 본 영구는 수행되었다. 응집동력학을 측정하기 위한 방법으로서 AIA 시스템으로 부터 없어진 입자크기분포와 Rlowing suspension에서의 PDA에 의한 탁도증가 정도의 측정이 사용되었다. 결론으로서, 저온에서의 응집은 그 효율이 상당히 저하 되는것으로 발견 되었으며 저온에서의 응집을 향상시키기 위아여 수중의 pH보다는 pOH를 일정하게 유지하는 것이 부분적으로 응집효율향상에 도움이 되는 것으로 나타났다.

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폴리올 프로세스를 통한 연료전지용 백금 촉매 제조 (Investigation of carbon supported pt nano catalyst preparation by the polyol process for fuel cell applications)

  • 오형석;김한성
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2007년도 춘계학술대회
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    • pp.200-203
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    • 2007
  • Parametric investigation of the polyol process for the preparation of carbon supported Pt nano particles as catalysts for fuel cells was carried out. It was found that the concentration of glycolate anion, which is a function of pH, plays an important role in controlling Pt particle size and loading on carbon. It was observed that Pt loading decreased with increasing alkalinity of the solution. As evidenced by zeta potential measurement, this was mainly due to poor adsorption or repulsive forces between the metal colloids and the supports. In order to modify the conventional polyol process, the effect of the gas purging conditions on the characteristics of Pt/C was examined. By the optimization of the gas environment during the reaction, it was possible to obtain high loading of 39.5wt% with a 2.8 nm size of Pt particle. From the single cell test, it was found that operating in ambient $O_{2}$ at 70oC can deliver high performance of more than 0.6 V at 1.44 A $cm^{-2}$.

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서울시의 1993년 가을철 시정 및 입자 특성 측정 및 분석 (Measurement and Analysis of Visibility and the Characteristics of Particles during the Fall, 1993 in Seoul)

  • 백남준;김태오;김성주;김용표;문길주
    • 한국대기환경학회지
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    • 제10권1호
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    • pp.32-40
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    • 1994
  • Continuous measurements of the extinction coefficient( $b_{ext}$ ) and scattering coefficient due to Particle( $b_{sp}$ ) were made during the fall 1993 in Seoul along with the measurements of the size distribution, ionic composition of particles. On the average, $b_{sp}$ values are 55% and 79% of $b_{ext}$ values during the clear and smoggy Periods respectively. Also the average values of $b_{ext}$ and $b_{sp}$ were 0.791$\times$10$^{-3}$ $m^{-1}$ (visual range 4.9km) and 0.628$\times$10$^{-3}$ $m^{-1}$ (visual range 6.2km) during the smoggy Period, and 0.297$\times$10$^{-3}$ $m^{-1}$ (visual range 13.1km) and 0.164$\times$10$^{-3}$ $m^{-1}$ (visual range 23.8km) during the clear period, respectively. The Peak at about 1${\mu}{\textrm}{m}$ of the Particle size distribution during the smoggy period is about four times higher than that during the clear period while the peaks at about 5${\mu}{\textrm}{m}$ during both periods are similar. Also, the concentrations of sulfate and nitrate at about 1${\mu}{\textrm}{m}$ during the smoggy Period are much higher than these during the clear Period.eriod.

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다이아몬드 배열 무전해 니켈 도금층/무산소동 기판의 열전도도 특성 (Thermal Properties of Diamond Aligned Electroless Ni Plating Layer/Oxygen Free Cu Substrates)

  • 정다운;김송이;박경태;서석준;김택수;김범성
    • 한국분말재료학회지
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    • 제22권2호
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    • pp.134-137
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    • 2015
  • The monolayer engineering diamond particles are aligned on the oxygen free Cu plates with electroless Ni plating layer. The mean diamond particle sizes of 15, 23 and $50{\mu}m$ are used as thermal conductivity pathway for fabricating metal/carbon multi-layer composite material systems. Interconnected void structure of irregular shaped diamond particles allow dense electroless Ni plating layer on Cu plate and fixing them with 37-43% Ni thickness of their mean diameter. The thermal conductivity decrease with increasing measurement temperature up to $150^{\circ}C$ in all diamond size conditions. When the diamond particle size is increased from $15{\mu}m$ to $50{\mu}m$ (Max. 304 W/mK at room temperature) tended to increase thermal conductivity, because the volume fraction of diamond is increased inside plating layer.

Dispersion Behavior and Size Analysis of Thermally Purified High Pressure-high Temperature Synthesized Nanodiamond Particles

  • Kwon, Hansang;Park, Jehong;Leparoux, Marc
    • 한국분말재료학회지
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    • 제24권3호
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    • pp.216-222
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    • 2017
  • Synthesized monocrystalline nanodiamond (nD) particles are heat-treated at various temperatures to produce highly structured diamond crystals. The heat-treated nDs show different weight loss ratios during thermogravimetric analysis. The crystallinities of the heat-treated nDs are analyzed using Raman spectroscopy. The average particle sizes of the heat-treated nDs are measured by a dynamic light scattering (DLS) system and direct imaging observation methods. Moreover, individual dispersion behaviors of the heat-treated nD particles are investigated based on ultrasonic dispersion methods. The average particle sizes of the dispersed nDs according to the two different measurement methods show very similar size distributions. Thus, it is possible to produce highly crystallized nD powder particles by a heat-treatment process, and the nD particles are relatively easy to disperse individually without any dispersant. The heat-treated nDs can lead to potential applications such as in nanocomposites, quantum dots, and biomedical materials.

Hydrogeological Characteristics of a Riverine Wetland in the Nakdong River Delta, Korea

  • Jeon, Hang-Tak;Cha, Eun-Ji;Lim, Woo-Ri;Yoon, Sul-Min;Hamm, Se-Yeong
    • 한국지구과학회지
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    • 제42권4호
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    • pp.425-444
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    • 2021
  • Investigating the physical and chemical properties of riverine wetlands is necessary to understand their distribution characteristics and depositional environment. This study investigated the physical (particle size, color, and type) and chemical properties (organic, inorganic, and moisture contents) of sediments in Samrak wetland, located in the Nakdong River estuary area in Busan, South Korea. The particle size analysis indicated that the hydraulic conductivity values for the coarse grain and the mixture of coarse and fine grains ranged from 2.03 to 3.49×10-1 cm s-1 and 7.18×10-3 to 1.24×10-7 cm s-1, respectively. In-situ water quality and laboratory-based chemical analyses and radon-222 measurement were performed on groundwater and surface water in the wetland and water from the nearby Nakdong River. The physical and chemical properties of Samrak wetland was characterized by the sediments in the vertical and lateral direction. The concentrations of chemical components in the wetland groundwater were distinctly higher than those in the Nakdong River water though the wetland groundwater and Nakdong River water equally belonged to the Ca-HCO3 type.