• Title/Summary/Keyword: Particle Morphology

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Effect of Particles Drift on Dendritic Growth

  • Park, Min Sik;Im, Dongmin
    • Journal of Electrochemical Science and Technology
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    • v.5 no.2
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    • pp.53-57
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    • 2014
  • With the use of diffusion-limited aggregation modeling, we have investigated the effect of particle drift for dendritic growth. It is found that the morphology of dendritic growth is sensitive to the particle drift, i.e., the larger drift effect results in the denser growth of dendrite. From the analysis using the correlation function, we found the fractional dimension of each dendrite increases as the particles drift increases. Furthermore, we showed the height of dendrite significantly decrease for the slight change of particles drift. Finally, we discussed the strategy to reduce dendritic growth by modifying the transport properties of electrolytes.

Microstructural Change in Rheocast AZ91D Magnesium Alloys with Stirring Rate and Isothermal Stirring Temperature (교반속도 및 등온교반온도에 따른 AZ91D 마그네슘합금 반응고 주조재의 미세조직 변화)

  • Yim, Chang-Dong;Shin, Kwang-Seon
    • Journal of Korea Foundry Society
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    • v.23 no.3
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    • pp.130-136
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    • 2003
  • Rheocasting of AZ91D magnesium alloys yielded the microstructure consisted of the spherical primary particles in the matrix which is different from conventional casting. Rheocast ingots were produced under various processing conditions using batch type rheocaster. Morphology of primary particles was changed from rosette-shape to spherical shape with increasing stirring rate$(V_s)$ and decreasing isothermal stirring temperature$(T_s)$. With increasing $V_s$, more effective shearing between the particles occurred rather than the agglomeration and clustering, so the primary particle size decreased. But with decreasing $T_s$, primary particle size increased mainly due to sintering and partially Ostwald ripening. The sphericity of primary particles increased with increasing $V_s$ and decreasing $T_s$ due to enhanced abrasion among the primary particles. The uniformity of primary particle size increased with increasing Vs and $T_s$.

Preparation and Physical Properties of Poly(Styrene/Acrylate) Core-Shell Latex Particles (Poly(Styrene/Acrylate) Core-Shell 라텍스 입자의 제조와 물성에 관한 연구)

  • Lee, Kyoung-Goo;Park, Keun-Ho
    • Journal of the Korean Applied Science and Technology
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    • v.20 no.1
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    • pp.27-32
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    • 2003
  • The core-shell latex particles were prepared by sequential emulsion polymerization of alkyl methacrylate and styrene(ST) by using an water-soluble initiator(APS) after preparing monomer pre-emulsion in the presence of an anionic surfactant(SDBS). In organic/organic core-shell polymerization, the pre-emulsion method, which minimized required quantity of sulfactant, has been used to increase the conversion rate and the stability of core-shell latex particles as well as to reduce the formation of secondary particle that cause problems of soap-free emulsion during shell polymerization. We used several methods to observe the core-shell structure. The core-shell structure was studied by measuring pH change during hydrolysis by NaOH, glass transition temperature($T_g$) by differential scanning calorimeter(DSC), morphology of latex by transmission electron microscope(TEM) and change of particle size and distribution by a particle analyzer.

Natural Dyeing of Cotton Fabrics Using Charcoal (숯을 이용한 면직물의 천연염색)

  • Jo, Won-Joo;Lee, Jeong-Sook
    • Fashion & Textile Research Journal
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    • v.6 no.6
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    • pp.803-809
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    • 2004
  • In order to activate the characteristics of charcoal in fiber systems, this was carried out to experiment with the particle size from two micrometers to ten micrometers of charcoal powders on cotton fabrics. The results obtained were as follows; The fabrics were dyed with gray colors by charcoal. The K/S values, that were indicative of the dye affinity, became higher as the increase of dyeing temperature, dyeing time, and dyeing concentration. Also it was confirmed the morphology of the fiber surfaces adsorbed with the particle size from two micrometers to four micrometers of charcoal powder by scanning electronmicronscope. The cotton fabrics dyed by charcoals generally recorded 3-4 degree of wash fastness, 4-5 degree of dry-cleaning fastness, 4-5 degree acidic and alkaline perspirations and water fastness. In connection with the functional properties, cotton fabrics dyed with charcoal appeared that antibacterial, deodorization, far infrared emissivity were improved. Especially the deodorization was improved greatly by using charcoal.

The influence of Jelly strength and Hardening agent on microcapsules by complex coacervation (복합상분리법에 의한 마이크로캡슐 제조 -젤리강도 및 경화제에 따른 특성변화-)

  • 김혜림;송화순
    • Journal of the Korean Society of Clothing and Textiles
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    • v.27 no.9_10
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    • pp.1172-1177
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    • 2003
  • Microcapsules were prepared by complex coacervation between gelatin and gum arabic. The object of this work is evaluation of the effect of jelly strength, hardening agent on the particle size distribution, surface morphology and DSC. It was found that the 300bloom jelly strength caused microcapsules' size larger. When the amount of hardening agent increased, the particle mean diameter was larger. The amount of hardening agent was determined to be 10m1 for getting suitable size to finish the fabric.

Heat Treatment Properties of Water Atomized Iron Powder for Powder Metallurgy (분말야금용 수분사 철분의 열처리 특성)

  • Kim, Y.C.
    • Journal of the Korean Society for Heat Treatment
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    • v.9 no.1
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    • pp.62-68
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    • 1996
  • In order to establish making process of water atomized iron powder for powder metallurgy, effect of heat treatment condition on change of powder properties and impurities was investigated at each tempeature of $850{\sim}950^{\circ}C$. The results are as follows. Particle morphology of iron powder changed slightly from sphercial type to irregular type and the amount of fine particle decreased more and more with increasing of heat treatment time at each temperature. The flow rate and apparent desity of iron powder also decreased due to particle coalescence in order of $850^{\circ}C$, $950^{\circ}C$, $900^{\circ}C$. Those powder Properties became to decrease particularly at $900^{\circ}C$ in alpha iron region. On the other hand, residual carbon and oxygen contents in iron powder decreased extremely with increasing of heat treatment temperature and time.

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Preparation of composite particles by Rapid Expansion of Supercritical fluid Solutions and Release behavior

  • Ryu, Han-Won;Kim, Jung-Hwan;Kim, Young-Do;Shin, Kun-Chul
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1998.09a
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    • pp.117-121
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    • 1998
  • The Rapid Expansion of supercritical fluid Solutions (RESS) process was applied to particles coating. Experiments were conducted in a fluidized bed with an internal nozzle in the center of the reaction tube. Microcapsules (mean particle size : 49$\mu\textrm{m}$) prepared by spray drying method were used as the core particles. Supercritical CO2 solutions of paraffin were expanded through the nozzle in to the bed that was fluidized by air. Surface morphology prepared particles was observed by SEM. For the inspection of particle size change, particle size distributions were measured before and after coating. The releasing behavior of Mg2+ ions inspected by AA.

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Influence of the Morphology and the Particle Size on the Processing of Bronze 90/10 Powders by Metal Injection Moulding (MIM)

  • Contreras, Jose M.;Jimenez-Morales, Antonia;Torralba, Jose M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.503-504
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    • 2006
  • The MIM technology is an alternative process for fabricating near net shape components that usually uses gas atomised powders with small size $(<\;20\;{\mu}m)$ and spherical shape. In this work, the possibility of changing partially or totally spherical powder by an irregular and/or coarse one that is cheaper than the former was investigated. In this way, different bronze 90/10 components were fabricated by mixing three different types of powder, gas and water atomised with different particle sizes, in order to evaluate how the particle shape and size affect the MIM process.

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Analysis of Deposited Dust Particles using SEM/EDX (SEM/EDX 분석법을 이용한 침착먼지에 대한 분석사례)

  • Ha, Eun-Ji;Park, Jeong-Ho
    • Journal of Environmental Science International
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    • v.30 no.3
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    • pp.279-287
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    • 2021
  • In this study, the composition and morphology of deposited dust particles with size ranging from a few to tens ㎛ were investigated using SEM/EDX (scanning electron microscopy with energy dispersive x-ray spectrometer). Then deposited dust particles were classified into 8 groups: quartz, aluminosilicates, ca-rich, Fe/Ti oxide, carbon-rich, industrial particle, Fe-rich, and biogenic particle. The sources of deposited dust were high in the order of aluminosilicates 41% > biogenic 18% > Fe-rich 11% > quartz and C-rich 8% > industrial 7% > Fe/Ti oxide 5% > Ca-rich 1%. In particular, the ratio of biogenic particles was relatively high due to influence of pollen. The ratio of carbon-rich was 11% at YM site, 10% at MD site, and 4% at MO site, and the site close to the large emission source was high.

Characteristics in Size Distributions and Morphologies of Wear Particles Depending on Types of Abrasion Testers

  • Eunji Chae;Seong Ryong Yang;Sung-Seen Choi
    • Elastomers and Composites
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    • v.58 no.2
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    • pp.87-94
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    • 2023
  • Abrasion tests of an SBR compound were conducted using four different types of abrasion testers (cut and chip, Lambourn, DIN, and LAT100). The abrasion test results were analyzed in terms of size distributions and morphologies of the wear particles. Most wear particles were larger than 1000 ㎛. The wear particle size distributions tended to decrease as the particle size decreased. Except for the Lambourn abrasion test, the wear particles smaller than 212 ㎛ were rarely generated by the other three abrasion tests, implying that small wear particles were produced through friction by introducing talc powder. Shapes of the wear particles varied depending on the abrasion testers. The wear particles generated from the Lambourn abrasion tester had stick-like shapes. The cut and chip abrasion test showed a clear abrasion pattern, but the DIN abrasion test did not show any specific abrasion pattern. The Lambourn and LAT100 abrasion tests showed irregular abrasion patterns.