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Preparation and Physical Properties of Poly(Styrene/Acrylate) Core-Shell Latex Particles

Poly(Styrene/Acrylate) Core-Shell 라텍스 입자의 제조와 물성에 관한 연구

  • Lee, Kyoung-Goo (Dept. of Chemical Engineering, Changwon National University) ;
  • Park, Keun-Ho (Dept. of Chemical Engineering, Changwon National University)
  • 이경구 (창원대학교 화공시스템공학과) ;
  • 박근호 (창원대학교 화공시스템공학과)
  • Published : 2003.03.31

Abstract

The core-shell latex particles were prepared by sequential emulsion polymerization of alkyl methacrylate and styrene(ST) by using an water-soluble initiator(APS) after preparing monomer pre-emulsion in the presence of an anionic surfactant(SDBS). In organic/organic core-shell polymerization, the pre-emulsion method, which minimized required quantity of sulfactant, has been used to increase the conversion rate and the stability of core-shell latex particles as well as to reduce the formation of secondary particle that cause problems of soap-free emulsion during shell polymerization. We used several methods to observe the core-shell structure. The core-shell structure was studied by measuring pH change during hydrolysis by NaOH, glass transition temperature($T_g$) by differential scanning calorimeter(DSC), morphology of latex by transmission electron microscope(TEM) and change of particle size and distribution by a particle analyzer.

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