• Title/Summary/Keyword: Pak1

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MEDIUM RESOLUTION SPECTRAL LIBRARY OF LATE-TYPE STELLAR TEMPLATES IN NEAR-INFRARED BAND

  • Nguyen, Huynh Anh Le;Pak, Soo-Jong;Im, Myung-Shin;Kang, Won-Seok;Lee, Sang-Gak;Ho, Luis C.;Pyo, Tae-Soo;Jaffe, Daniel T.
    • The Bulletin of The Korean Astronomical Society
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    • v.36 no.1
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    • pp.69.2-69.2
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    • 2011
  • We present medium resolution spectra in the near-infrared (IR) band 1.4-1.8 microns at a resolving power of R = 5000-10000 of template stars in G, K, and M types with luminosity classes of III observed by the echelle spectrometer, IRCS, at the SUBARU 8.2 m telescope. Identification of lines in the template star spectra has been completed base on the reference of Arcturus spectrum. We measured equivalent width (EW) of the lines, and analyze the trends of EW through the stellar spectral types.

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Seperation of foreground stars using proper motion data in the Large Magellanic Cloud

  • Kim, Jae-Yeong;Pak, Soo-Jong;Choi, Min-Ho;Kandori, Ryo;Tamura, Motohide;Nagata, Tetsuya;Kwon, Jung-Mi;Kato, Daisuke;Jaffe, Daniel T.
    • The Bulletin of The Korean Astronomical Society
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    • v.36 no.1
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    • pp.31.1-31.1
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    • 2011
  • We present wide-field near-IR imaging polarimetry of 30 Doradus in the Large Magellanic Cloud, using the InfraRed Survey Facility (IRSF). We obtained polarimetry data in J, H, and Ks bands using the JHKs-simultaneous imaging polarimeter SIRPOL. Since many Galactic field stars along the line-of-sight to the Large Magellanic Cloud are contaminated in our data, we developed methods to identify the foreground sources using the proper motion data. We investigated polarimetric properties between the Galactic foreground stars and the stars in the LMC.

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Study on analytical method of residual macrolide antibiotics in livestock products by LC/MS (LC/MS를 이용한 축산물 중 잔류 마크로라이드계 항생물질 분석법 연구)

  • 황래홍;윤은선;김연주;김동언;양윤모;이정학;이병동
    • Korean Journal of Veterinary Service
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    • v.25 no.3
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    • pp.221-227
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    • 2002
  • This study was carried out to confirm analytical method of residual macrolides in livestock products by LC/MS. 1. Macrolides were analyzed by LC/MS on XTerra C$\sub$18/ column with 0.1% TFA(trifluoroacetic acid)-methanol in a gradient mode as mobile phase, and that were identified by positive chemical ionization with selective ion monitoring at 50~1000 mass range. 2. Residual macrolides were extracted from tissue with acetonitrile, and the extract is purified with a Sep-pak C$\sub$18/ cartridge, and elute macrolides with 0.1M methanolic ammonium acetate. 3. The procedure confirms the presence of each macrolide at 50$\mu\textrm{g}$/kg in spiked sample.

The Simultaneous Analysis of Oxytetracycline, Chloramphenicol and Sulfamethoxazole in Pork by HPLC (HPLC를 이용한 돈육 중의 Oxytetracycline, Chloramphenicol 및 Sulfamethoxazole의 동시검출)

  • 조혜연;조진국;이치호
    • Food Science of Animal Resources
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    • v.21 no.1
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    • pp.64-70
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    • 2001
  • The extraction procedure and HPLC condition were modified to analyze the residues of oxytetracycline, sulfamethoxazole and chloramphenicol in pork, simultaneously. The antibacterial agents in pork were extracted with 0.02M EDTA-Mcilivine buffer:ethanol:acetonitrile (5:3:2). After the removal of fat with n-hexane, the extracts were evaporated and purified with Sep-pak $C_{18}$ cartridge column using 0.01M oxalic acid 0.1% (v/v) triethylamine (TEA) in acetonitrile. The peak of antibacterial agents was detected with $\mu$ Bondapak C18 column, UV detector (280nm) and 0.01M oxalic acid: methanol: acetonitrile (7.5:2.0:0.5). Detection limits for three antibacterial standards were 0.03 ppm. Calibration curves were linear between 0.03 and 2.0 ppm (R$^2$>0.999). When spiked the level of 1.0 ppm of oxytetracycline, sulfamethoxazole and chloramphenicol into meats, the recoveries from meats were 77.3%, 79.7% and 59.3%, respectively. These results showed that the modified extraction method provided good analytical resolution and the recoveries of the above antibacterial agents in meats.

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Identification and HPLC Quantification of a Phytoecdysone and Three Phenolic Glycosides in Lamium takesimense Nakai

  • Nugroho, Agung;Park, Kyoung-Sik;Seo, Dong-Jin;Park, Hee-Juhn
    • Natural Product Sciences
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    • v.24 no.4
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    • pp.241-246
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    • 2018
  • The herbs of Lamium takesimense Nakai (Lamiaceae) is used to treat spasmodic and inflammatory disease. The four polar compounds, ecdysterone, isoacteoside, rutin and lamiuside C, were isolated and identified from the BuOH fraction of the L. takesimense MeOH extract. HPLC quantification was performed on a Capcell Pak C18 column ($5{\mu}m$, $4.6mm{\times}250mm$) with a gradient elution of $H_2O$ and 0.05% acetic acid in MeOH. The HPLC method was validated in terms of linearity, sensitivity, stability, precision, and accuracy. The quantitative level in plant material was determined as the following order: lamiuside C (4, 3.75 mg/g dry weight) > ecdysterone (1, 1.93 mg/g) > isoacteoside (2, 1.32 mg/g) > rutin (3, 0.97 mg/g).

Demonstration of Modeling Process using Giant Magellan Telescope Software Development Kit

  • Han, Jimin;Pi, Marti;Filgueira, Josema;Cox, Marianne;Molgo, Jordi;Swett, Hector;Kurkdjian, Pierre;Lee, Hye-In;Ji, Tae-Geun;Pak, Soojong
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.1
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    • pp.72.1-72.1
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    • 2019
  • The Giant Magellan Telescope Organization (GMTO) is developing the GMT Software Development Kit (SDK) for the Observatory Control System (OCS). The SDK models a subsystem of the GMT using a Domain Specific Language (DSL) which can generate a skeleton code and validates the availability of the model automatically. The OCS includes a Device Control System (DCS) and all the devices are connected with the DCS via EtherCAT. The DCS has a component (Hardware Adapter) to communicate with EtherCAT slaves. In this presentation, we demonstrate the modeling process and describe the importance and usage plan of the SDK.

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Simultaneous Determination of Curcumin and Glycyrrhizin Contents by High-performance Liquid Chromatography in Two Different Oriental Herbal Preparations of Kamijadowhan

  • Kim, Eun-Young;Choi, Seung-Hun;Kwon, Oh-Seung
    • Proceedings of the PSK Conference
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    • 2002.10a
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    • pp.389.1-389.1
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    • 2002
  • A high-performance liquid chromatographic method was developed to determine the quantities of curcumin and glycyrrhizin in two different oriental herbal preparations of Kamijadowhan (KMD. NKMD). Two compounds were separated in less than 10 min with a Nova-Pak $C_{18}$ column ($3.9{\times}150$ mm ($5{\mu}$ particle size) by linear gradient elution using 0.03% (v/v) phosphoric acid-acetonitrile (60:40. v/v% at 0 min; 40:60 v/v% at 6 mini as the mobile phase at a flow-rate of 0.8 ml $min^{-1}$. (omitted)

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Control of Mg and P Ion Concentration as a Precondition to Use N, K and Ca Ion Sensors in Closed Hydroponics (N, K, Ca의 한정된 이온센서 이용을 전제로 한 순환식 수경재배에서 P, Mg의 조절 방법)

  • Choi, Gyeong Lee;Yeo, Kyung Hwan;Rhee, Han Cheol;Lee, Seong Chan;Lee, Jung-Sup;Kang, Nam Jun;Kim, Hak Jin;Jung, Dae Hyun
    • Horticultural Science & Technology
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    • v.34 no.6
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    • pp.871-877
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    • 2016
  • Recycling nutrient solutions in closed hydroponic production systems is usually accompanied by an imbalance of nutrient solutions when concentration is controlled according to electrical conductivity (EC) levels. This study investigated whether it was possible to automatically control the concentrations of five essential elements nitrogen (N), phosphorus (P), potassium (K), calcium (Ca) and magnesium (Mg) using only N, K and Ca ion sensors. N, P, K, Ca, and Mg uptake was measured in the nutrient solution, and relationships between absorbed ions were analyzed through twice-repeated experiments in lettuce. Results confirmed that the pattern of $PO_4$ ion uptake was similar that of N, and the pattern of Mg ion uptake was similar that of Ca. $PO_4$ ion uptake was most highly correlated with N, and Mg was most highly correlated with Ca. Regression coefficients of N and $PO_4$ were significantly different at 1.04 and 0.55, respectively, but were similar between Ca and Mg at 0.35 and 0.40, respectively. Additional experiments were conducted to measure nutrient uptake in pak choi and rose plants, both to confirm the results from the first experiment in lettuce, and to assess possible application to other crops. Coefficients of determination both for N and $PO_4$, and Ca and Mg were considerably high ($R^2=0.86$) in cultured pak choi, and similar results were observed in cultured rose ($R^2=0.87$ and 0.73, respectively). Regression coefficients for cultured pak choi were 0.56 and 0.24, respectively, and for rose were 0.51 and 0.16, respectively. Although the results obtained for N and $PO_4$ were not consistent between the lettuce experiments, N and $PO_4$ have similar regression coefficients for all crops. No common coefficient was found between Ca and Mg.

Effects of Light Sources, Light Quality on the Growth Response of Leafy Vegetables in Closed-type Plant Factory System (완전제어형 식물공장에서 광원, 광질에 따른 엽채류 6종의 생육반응)

  • Kim, Sang Bum;Lee, Kyung Mi;Kim, Hae Ran;You, Young Han
    • Korean Journal of Ecology and Environment
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    • v.47 no.1
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    • pp.32-40
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    • 2014
  • This study was conducted to evaluate the growth response of economical six leafy vegetables that are crown daisy, pak-choi and four kinds of lettuce (Red leaf lettuce, Green leaf lettuce, Head lettuce, Romaine lettuce) by light treatment of LED in plant factory. The light treatments were composed of red, blue, red+farred, red+blue, red+blue+white LEDs, irradiation time ratio of the red and blue LED per minute (1 : 1, 2 : 1, 5 : 1, 10 : 1), and duty ratio of mixed light (100%, 99%, 97%). The following results were obtained in different LED light sources treatments: Shoot biomass and S/R ratio of romaine lettuce were the highest under mixed red+blue LEDs. S/R ratio of head lettuce was higher under mixed red+blue+white LEDs than red+blue LEDs. The others showed no difference in LED light treatment. Shoot biomass, total biomass and S/R ratio of green lettuce, head lettuce and pak-choi were highest in the higher red ratio (5 : 1) on irradiation time of red : blue LED ratios. By the different duty ratio (red+blue and red+blue+white LEDs), Under the mixed light of red+blue, shoot and root biomass of crown daisy and romaine lettuce were high in duty ratio of 100% and 99%, and S/R ratio was highest in all the 6 kinds in duty ratio of 97%. All the 6 kinds showed a fine growth state in low duty ratio (97%). Green lettuce, romaine lettuce and pak-choi showed relatively high shoot biomass and total biomass in low duty ratio of 97% under the mixed light of red+blue+white. S/R ratio of romaine lettuce and head lettuce were highest in the duty ratio of 97% with red+blue+white LEDs. Thus, we can cultivate stably without reference to external factors, if we use appropriate light sources and light quality in closed-type plant factory.

Validation of an analytical method of dieckol for standardization of Ecklonia cava extract as a functional ingredient (감태추출물의 기능성원료 표준화를 위한 지표성분 dieckol의 분석법 검증)

  • Xu, Yan;Kim, Eun Suh;Lee, Ji-Soo;Kim, Gun-Hee;Lee, Hyeon Gyu
    • Korean Journal of Food Science and Technology
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    • v.51 no.5
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    • pp.420-424
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    • 2019
  • An HPLC analysis method was developed and standardized for the detection of dieckol as a functional food ingredient in Ecklonia cava extracts. HPLC was performed using a Capcell Pak C18 column ($250{\times}4.6mm$, $5{\mu}m$) with a gradient elution of water and acetonitrile, both containing 0.1% (v/v) trifluoroacetic acid, at a flow rate of 1.0 mL/min at $25^{\circ}C$. The eluate was detected at 230 nm. For validation, the specificity, linearity, accuracy, precision, limit of detection (LOD), and limit of quantification (LOQ) of dieckol were measured. The calibration curve for the detection of dieckol had high linearity ($R^2=0.9994$), with LOD and LOQ values of 0.38 and $1.16{\mu}g/mL$, respectively. Recovery of the quantified compound ranged from 99.61 to 100.71%. The relative standard deviation values of the intra-day and inter-day precisions were less than 1.7 and 1.25%, respectively. These results indicate that the reported HPLC method is simple, reliable, and reproducible for the detection of dieckol in Ecklonia cava extracts.