• 제목/요약/키워드: P25 method

검색결과 3,010건 처리시간 0.028초

알콕사이드 가수분해법에 의핸 제조된 TiO$_2$ 분말을 이용한 Micad의 표면 개질 (Surface Modification of Mica Using TiO$_2$ prepared by Alkoxide Hydrolysis Method)

  • 한상필;윤영훈;이상훈;최성철
    • 한국세라믹학회지
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    • 제36권7호
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    • pp.691-697
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    • 1999
  • TiO2 powder was adsorbed on the surface of mica using the heterocoagulation method in water TiO2 powder was prepared from hydrolysis of titanium-iso propoxide in a mixed solvent of anhydrous ethanol and water. When the molar ratio of water to titanium iso-propoxide was 0.25 monodispersed spherical TiO2 particles were obtained. The prepared TiO2 powder showed anatase phase after heat treatment at 50$0^{\circ}C$ for 2 h and then transformed to rutile phase after heat treatment at 100$0^{\circ}C$ for 2h. The iso-electric points of TiO2 and Mica were pH 3.9 and pH 3.25 respectively which were measured by the Z-potential analysis in water base. The maximum Z-potential difference between two powders was observed in the range of pH 3.6~3.7 TiO2 powder was adsorbed on the surface of mica by heterocoagulation method in pH 3.6~3,7 The properties of prepared TiO2 powder was haracterized by TG-DTA, XRD and SEM The morphology and thermal properties of TiO2-adsorbed mica were examined.

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재래식 화재감지기와 P형 수신기에 대한 화재위치검출 및 신뢰성 개선 (Detection of Fire Location And Reliability Improvement of the Conventional Fire Detector and P-type Receiver)

  • 지승욱;김시국;양승현;이재진;김필영;이춘하
    • 조명전기설비학회논문지
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    • 제25권5호
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    • pp.39-44
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    • 2011
  • Automatic fire alarm system is set up to automatically detect fire on buildings. Because of economic reasons, P-type receiver and a conventional type fire detector is normally used for automatic fire alarm system in Korea. Because early detection of fire is regarded as important, the need of finding technique of fire location increases. This paper is studied a method to improve a reliability and add a function of fire location detection on a conventional type fire detector and P-type receiver. Fire location is detected by a method that controller attached on the receiver and the detector is read with a time lag. A reliability of fire detection alarm system is improved with a method that false fire alarm is able to decrease using two different principle detector together. This paper is studied for basic data of improvement of low-cost addressable automatic fire alarm system.

Some Aspects of Laying, Incubation and Hatching in the Great Reed-Warbler

  • Yoo, Jeong-Chil;Choi, Yu-Seong
    • The Korean Journal of Ecology
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    • 제25권4호
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    • pp.241-245
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    • 2002
  • During the breeding season of 1998, breeding ecology of the Great Reed-Warbler (Acrocephalus arundinaceus orientalis) was studied at Yangsoo-ri and Yongdam-ri of the Yangpyung-gun, Kyunggi province, Korea. Egg-weight (CV: 6.25) was more variable than either length or breadth, and breadth was the least variable of the measures. Significant variations in overall egg-weight occurred between clutches, and that more of the total variation in egg-weight and shape are due to inter-clutch variation as to intra-clutch variation when the data were pooled. The last egg tends to be larger than the remaining eggs in the clutch of the Great Reed-Warbler, suggesting the Great Reed-Warbler may adopt the brood-survival strategy. When method 3 was used, the most common incubation period is 12 days. In the Great Reed-Warbler, the length of the incubation period was related to clutch-size when method 1 (r=0.485, p<0.05) and method 2 (r=0.621, p<0.01) were employed, but not related to egg weight. The averagee number of days of hatching asynchrony was 2.5, raging 0.5~2.5. Asynchronous hatching was related to the clutch size (r=0.66, p<0.01). Hatching sequence was closely related to the laying sequence (r=0.93, p<0.001), suggesting Great Reed-Warblers incubate their eggs before clutch completion. The effect of egg weight on hatching asynchrony was found in Great Reed-Warblers (t-test, p<0.01).

Diosgenin 유도체 합성과 진통 및 항고지혈 효과 (Synthetic Derivatives of Diosgenin and Their Antinociceptive and Antihypercholesterolemic Effects)

  • 김학순;마은숙
    • 약학회지
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    • 제51권1호
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    • pp.56-62
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    • 2007
  • Twelve epoxy and hydroxydiosgenin derivatives (DI-1${\sim}$DI-12) were synthesized from diosgenin (25(R)-5-spirosten-3${\beta}$-ol). Diosgenin was epoxidized with m-chloroperoxybenzoic acid (mCPBA) to oxidize 25(R)-4${\alpha}$,5${\alpha}$-epoxyspirostane (DI-1). Diosgenin was reacted with DDQ to form 25(R)-1,4,6-spirostatrien-3-one (DI-2), which was treated with 30% H$_2$O$_2$ to give 25(R)-1${\alpha}$,2${\alpha}$-epoxy-4,6-spirostadien-3-one (DI-3) and treated with mCPBA to form 25(R)-6${\alpha}$,7${\alpha}$-epoxy-1,4-spirostadien-3-one (DI-7), respectively. DI-3 was reduced with NaBH$_4$ to afford 25(R) -1${\alpha}$,2 ${\alpha}$-epoxy-4,6-spirostadien-3${\beta}$-ol(DI-4) and reacted with Li metal in absolute ethanol to form 25(R)-2-ethoxy-1,4,6-spirostatrien-3-one (DI-5). DI-7 was reduced with NaBH$_4$ to produce 25(R)-3${\beta}$,7${\alpha}$-dihydroxy-4-spirostene (DI-8) and treated with Li metal in liquid ammonia to produce 25(R)-7${\alpha}$-hydroxy-4-spirosten-3-one (DI-9). DI-2 was reduced with NaBH$_4$ to form 25(R) -4,6-spirestadien-3${\beta}$-ol(DI-10), which was stirred with 30% H$_2$O$_2$ to synthesize 25(R)-4,6-spirostadien-3-one (DI-11) and reacted with mCPBA to give 25(R)-4${\beta}$,5${\beta}$ -epoxy-6-spirosten-3${\beta}$-ol (DI-12), respectively. The antinociceptive effects of synthesiz ed compounds were measured by hot plate method and compound DI-7 signifcantly exhibited antinociceptive effect. DI-2 decreased the serum triglyceride and total cholesterol levels in poloxamer P-407 injected rat.

유속증강 자기공명혈관조영술에서 숙임각 변화에 따른 영상의 질 연구 (A Study on the Image Quality According to the Change of Flip Angle in Flow-Related Enhancement Magnetic Resonance Angiography)

  • 구은회
    • 한국방사선학회논문지
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    • 제12권2호
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    • pp.201-208
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    • 2018
  • 본 연구는 Image J 프로그램을 사용하여 유속증가 자기공명영상기법의 숙임각 변화에 따른 SNR와 CNR을 측정하여 최적의 숙임각을 알아보기 위해 연구하였다. 총 30명의 정상인 지원자를 대상으로 1.5T 자기공명영상기기(Philips, Medical System, Achieva)를 이용하여 뇌동맥검사 후 평가를 실시하였다. 분석 방법으로 유속증가 자기공명 혈관 조영술에 대하여 4 부위에 관심영역을 설정하고 SNR와 CNR을 평가하였다. 5가지 숙임각에서의 정량적 분석으로 SNR과 CNR에 대한 통계적 유의성은 일원분산분석으로 계산되었으며, 사후 분석으로는 Bonferroni 법을 적용하였고, 통계에 사용된 프로그램은 SPSS 14.0을 이용하여 p 값을 0.05 이하일 때 유의성을 두었다. 본 실험에 대한 결과로서 전교통동맥(SNR:$876.59{\pm}14.22$, CNR:$1999.7{\pm}12.5$), 후교통동맥 (SNR: $863.48{\pm}13.29$, CNR:$1870.18{\pm}12.56$), ICA(SNR: $1116.87{\pm}08.34$, CNR:$2979.37{\pm}14.69$), 중대뇌동맥(SNR:$848.66{\pm}15.25$, CNR:$2199.25{\pm}13.48$)의 값으로 $25^{\circ}$에서 가장 높은 신호강도를 보였다(p<0.05). 작은 혈관 묘출로서 a1, a2, a3, p1, p2, p3, m1, m2, m3 값 또한 동일한 결과 이었다(p<0.05). 사후분석결과로, 숙임각에서 $25^{\circ}$ 기준으로 $10^{\circ}$, $15^{\circ}$, $20^{\circ}$에서 유의성 있는 결과를 얻었지만(p=0.000) $30^{\circ}$에서는 유의한 차이가 없었다(p>0.05). 결론적으로, 본 연구에서 $30^{\circ}$에서는 신호강도가 떨어지기 때문에 뇌혈관 자기공명조영술에서 최적의 숙임각은 $25^{\circ}$로 나타냈다.

COMPLEXITY ANALYSIS OF IPM FOR $P_*(\kappa)$ LCPS BASED ON ELIGIBLE KERNEL FUNCTIONS

  • Kim, Min-Kyung;Cho, Gyeong-Mi
    • East Asian mathematical journal
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    • 제25권1호
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    • pp.55-68
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    • 2009
  • In this paper we propose new large-update primal-dual inte-rior point algorithms for $P_*(\kappa)$ linear complementarity problems(LCPs). New search directions and proximity measures are proposed based on the kernel function$\psi(t)=\frac{t^{p+1}-1}{p+1}+\frac{e^{\frac{1}{t}}-e}{e}$,$p{\in}$[0,1]. We showed that if a strictly feasible starting point is available, then the algorithm has $O((1+2\kappa)(logn)^{2}n^{\frac{1}{p+1}}log\frac{n}{\varepsilon}$ complexity bound.

공침법에 의한 반도성 BaTiO3 제조 (Fabrication of Doped BaTiO3 by Coprecipitation Method)

  • 안영필;김복희;이태석
    • 한국세라믹학회지
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    • 제25권4호
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    • pp.315-320
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    • 1988
  • The Nb doped BaTiO3 was synthesized by coprecipitation method using H2O2 media in region from pH 8 to pH 11. The powder prepared by using this method was crystallized at about 20$0^{\circ}C$ and average particle size was controlled by heat treatment. Because of preparation having fine particle and relatively narrow particle size distribution, high performance PTC device was made of these precipitated powders.

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$^{99m}Tc$-DTPA를 이용한 신장스캔에서 사구체 여과율의 측정방법과 영상분석에서 구한 지표들에 의한 신장기능의 평가 (Estimation of Glomerular Filtration Rate(GFR) Using $^{99m}Tc$-DTPA Renal Scan and the Parameters for Renal Function)

  • 조인호;윤현대;원규장;이찬우;이형우;이현우
    • Journal of Yeungnam Medical Science
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    • 제11권1호
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    • pp.101-108
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    • 1994
  • 저자들은 Gates의 방법으로 구한 사구체 여과율과 신장스캔 시행중에서 얻을 수 있는 relative intensity of peak renal to peak aortic activity (pK/pA), time between aortic and kidney peak(A-K) 및 parenchymal renal activity at 25 min compared to peak kidney activity(25K/pK)등의 지표들이 신기능 평가에 유용하게 사용될 수 있는지를 알기 위하여 정상 및 신장질환 환자등 57명을 대상으로 Gates의 방법을 시행하여 사구체 여과율을 구하고 이를 크레아티닌 청소율과 그리고 A-K, pK/pA및 25K/pK등의 지표들과 비교분석하여 다음과 같은 성적을 얻었다. $^{99m}Tc$-DTPA를 이용한 사구체 여과율과 크레아티닌 청소율 사이에는 유의한 상관관계가 있었다.(r=0.9) A-K, pK/pA 및 25K/pK 등과 $^{99m}Tc$-DTPA를 이용한 사구체 여과율 사이에는 각각 유의한 상관 관계가 있었다.(r=-0.42, 0.66, -0.48) 이상의 결과로 Gates의 방법을 이용한 사구체 여과율의 측정은 통상적인 신장 스캔과 함께 시행함으로서 환자에게 별다른 고통을 주지 않으면서 간편하게 시행할 수 있는 검사로써 임상에 유용하게 사용할 수 있을 것으로 생각되며 그리고 A-K, pK/pA 및 25K/pK등의 지표들도 신기능의 평가에 사구체 여과율과 함께 이용할 수 있을 것으로 사료된다.

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Open-Tube에서 Zn확산을 이용한 GaAs에의 $p^+$층 형성 (Formation of $P^+-Layer$ in GaAs Using the Open-Tube Diffusion of Zn)

  • 심규환;강진영;민석기;한철원;최인훈
    • 대한전자공학회논문지
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    • 제25권8호
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    • pp.959-965
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    • 1988
  • Zinc diffusion characteristics and its applicabilities have been studied using an open-tube system. Thermal decomposition of arsenide(As) at gallium arsenide(GaAs) wafer surface was well inhibited by using Ga: poly-GaAs: Zn compositon as a diffusion source. Junction depth was obtained as 4.6x10**7\ulcorner exp)-1.25/kT) where activation energy of diffusion was 1.25eV. From Boltzmann-matano analysis, it could be identified that concentration dependencies of Zn diffusivity well consisted with those of kick-out model. The ideality factor of p+-n junction formed by Zn diffusion was about 1.6 and infrared light intensity was linearly varied in the range of sixty folds. It is concluded frodm these results that Zn diffuses according to kick-out model, and open-tube method is applicable to compound semiconductor devices.

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임상간호사의 그릿, 직무만족도와 재직의도와의 관계 (Relationships among Grit, Job Satisfaction, and the Intention to Stay of Clinical Nurses in Korea)

  • 박민희;조숙희
    • 임상간호연구
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    • 제25권3호
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    • pp.285-293
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    • 2019
  • Purpose: This descriptive study aimed to identify the relationships among grit, job satisfaction, and the intention to stay of clinical nurses in Korea. Method: Data collected from a total of 239 experienced nurses in four general hospitals of the Jeolla province. The t-test, ANOVA, and Pearson's Correlation Coefficient were performed using the IBM SPSS/WIN 21. Results: There were positive correlations between the grit and job satisfaction of the nurses (r=.31, p<.001), between their grit and intention to stay (r=.25, p<.001), and between their job satisfaction and intention to stay (r=.49, p<.001). Conclusion: Developing and adapting educational programs to enhance the grit enthusiasm, and patience can contribute to increasing the intention to stay of nurses in hospitals.