• Title/Summary/Keyword: Optimal Sintering

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Piezoelectric and dielectric Properties for Multilayer Piezoelectric Transformer Of Modified $PbTiO_3$ system ceramics (적층 압전 변압기용 변성 $PbTiO_3$ 세라믹스의 압전 및 유전 특성)

  • Yoo, Kyung-Jin;Yoo, Ju-Hyun;Jeong, Yeong-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.344-345
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    • 2006
  • In this study, in order to develop low temperature sintering piezoelectric transformer, $(Pb_{0.99-x}Ca_xSr_{0.01})Ti_{0.96}(Mn_{1/3}Sb_{2/3})_{0.04}O_3$ ceramic systems were fabricated using $Na_2CO_3-Li_2CO_3$ as sintering aids and investigated with the amount of Ca substitution. The piezoelectric transformer requires high electromechanical coupling factor $k_t$ and high mechanical quality factor $Q_{mt}$ for generating high output power At the ($PbCaSr)Ti(MnSb)O_3$ ceramics with 24mol% Ca substitution sintered at $900^{\circ}C$, electromechanical coupling factor $k_t$ and mechanical quality factor $Q_{mt}$ showed the optimal values of 0.504 and 1655 respectively, for thickness vibration mode multilayer piezoelectric transformer application.

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Development of Micro-Ceramic Heater for Medical Application (의료용 소형 세라믹스 히터 소자의 개발)

  • Lee, Seung-Min;Lee, Kwang-Ho
    • Journal of Biomedical Engineering Research
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    • v.43 no.4
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    • pp.219-229
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    • 2022
  • In this study, we propose a miniaturized micro-ceramic heater device. After screen-printing a silver paste between pre-sintered two aluminum oxide plates to integrate a heating circuit, the device was fabricated through a low-temperature sintering process. In order to configure the optimal heating circuit integration condition, the output current evaluation and heating test were performed according to the number of screen prints of the silver paste at various voltages. A silver paste-based heating circuit printed with a line width of 200 ㎛ and a thickness of 60 ㎛ was successfully integrated on a pre-sintered alumina substrate through a low-temperature sintering process. In the case of the 5 times printed device, the thermal response showed a response rate of 18.19 ℃/sec. To demonstrate feasibility of the proposed device in the medical field, such as bio-tissue suturing and hemostasis, a voltage was applied to pig tissue in the device to test tissue change due to heat generated from the device. These results show the possibility that the proposed small ceramic heater could be used in the medical field based on its excellent temperature response.

Fabrication and Sintering Behavior Analysis of Molybdenum-tungsten Nanopowders by Pechini Process (페치니 공정을 이용한 몰리브덴-텅스텐 나노 분말 제조 및 소결 특성 평가)

  • Suyeon Kim;Taehyun Kwon;Seulgi Kim;Dongju Lee
    • Journal of Powder Materials
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    • v.30 no.5
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    • pp.436-441
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    • 2023
  • Molybdenum-tungsten (Mo-W) alloy sputtering targets are widely utilized in fields like electronics, nanotechnology, sensors, and as gate electrodes for TFT-LCDs, owing to their superior properties such as high-temperature stability, low thermal expansion coefficient, electrical conductivity, and corrosion resistance. To achieve optimal performance in application, these targets' purity, relative density, and grain size of these targets must becarefully controlled. We utilized nanopowders, prepared via the Pechini method, to obtain uniform and fine powders, then carried out spark plasma sintering (SPS) to densify these powders. Our studies revealed that the sintered compacts made from these nanopowders exhibited outstanding features, such as a high relative density of more than 99%, consistent grain size of 3.43 ㎛, and shape, absence of preferred orientation.

Effect of Calcination Temperature on Al2O3-ZrO2 Ceramic Prepared by Sol-Gel Process (졸-겔법을 이용하여 제조한 Al2O3-ZrO2 세라믹스에 미치는 하소온도의 영향)

  • 우상국;김종희
    • Journal of the Korean Ceramic Society
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    • v.24 no.5
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    • pp.423-430
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    • 1987
  • Characteristics of Al2O3-ZrO2 powders prepared by sol-gel process and their sintering behavior were investigated as a function of calcination temperature. The sol-gel processed powders were calcined at 800, 900, 1000, 1100, 1200$^{\circ}C$, and analyzed by X-ray diffraction technique. Pore size and distribution of green compact of the calcined powders were measured by mercury porosimeter. It is suggested that the optimal temperature of calcination for the sintering of Al2O3-ZrO2 powder prepared by sol-gel process is 1100$^{\circ}C$. In the Al2O3-17vol.% ZrO2 sintered specimen, which was sintered at 1600$^{\circ}C$ for 2hrs in air, 69vol.% tetragonal phse existed.

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Development of Measurement mechanism of Laser Beam Spot size for Industrial SFF system (산업용 SFF 시스템에서 Laser Beam Spot size 측정 메커니즘 개발)

  • Bae, Sung-Woo;Kim, Dong-Soo;Choi, Kyung-Hyun
    • Proceedings of the KSME Conference
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    • 2007.05a
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    • pp.1383-1388
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    • 2007
  • Accuracy and processing time are very important factors when the desired shape is fabricated with Selective Laser Sintering (SLS), one of Solid Freeform Fabrication (SFF) systems. In a conventional SLS process, laser spot size is fixed during laser exposing on the sliced figure. Therefore, it is difficult to accurately and rapidly fabricate the desired shape. In this paper, to deal with those problems an SFF system having ability of changing spot size is developed. The system provides high accuracy and optimal processing time. Specifically, a variable beam expander is employed to adjust spot size for different figures on a sliced shape. Finally, Design and performance estimation of the SFF system employing a variable beam expander are achieved and the mechanism will be addressed to measure the real spot size generated from the variable beam expander.

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Flexible Dye-sensitized Solar Cells by a Low-temperature Sintering Method (저온소결법에 의한 플렉시블 염료감응 태양전지)

  • Baek, Ji-Hye;Kim, Joo-yong;Kang, Wee-Kyung
    • 한국신재생에너지학회:학술대회논문집
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    • 2007.06a
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    • pp.320-322
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    • 2007
  • A new binder-free $TiO_{2}$ paste was prepared by common ion applying effect, enabling low temperature fabrication required for flexible solar cells. The binder-free and high viscosity $TiO_{2}$ coating solution was produced by adding 7.5% aniline in $TiO_{2}$ colloid solution obtained from the high pressure water-heat response method. The resulting pastes had high level of viscosities proper for optimal coating and thus revealed excellent performances in terms of thickness uniformity and I-V characteristics.

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Effects of Expanders in Manufacture and Microstructure of ZnO Varistor with $Al_2O_3$ (ZnO 바리스터의 제조에서 분산제 영향 및 $Al_2O_3$ 첨가에 따른 미세구조 연구)

  • Soh, J.J.;Han, S.W.;Kim, H.S.
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.345-347
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    • 1995
  • ZnO varistor with composition of ZnO(90wt%)-$Bi_2O_3$(3wt%)-$Sb_2O_3$(3.61wt%)-$CO_2O_3$(1.16wt%)-NiO (0.88wt%)-$MnO_2$(0.71wt%)-$Cr_2O_3$(0.93wt%) according to $Al_2O_3$ addtive was fabricated by sintering methods. The optimal densification were established for the processing conditions of 8000 rpm 190$^{\circ}C$ spray drying and 1200$^{\circ}C$ 2hrs sintering. Then here investigated how additive compotions and processing variables affected the electrical and the phesical properties of these ZnO varistors.

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Sintering Behavior of the Net-shaped Fe-8wt%Ni Nanoalloy Powder and Related Mechanical Property

  • Cha, Berm-Ha;Kang, Yun-Sung;Lee, Sung-Ho;Lee, Jai-Sung
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.501-502
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    • 2006
  • The present investigation has been performed on full densification behavior and mechanical property of the powder injection molded Fe-8wt%Ni nanoalloy powder. The net shaping process of the nanopowder was conducted by powder injection molding (PIM) process. The key-process for fabricating fully densified net-shaped nanopowder by pressureless sintering is an optimal control of agglomerate size of nanopowder. Enhanced mechanical property of PIMed Fe-Ni nanopowder is explained by grain refinement and microstructural uniformity.

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Study for the Development of Fe-NbC Composites by Advanced PM Techniques

  • Gordo, E.;Gomez, B.;Gonzalez, R.;Ruiz-Navas, E.M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.118-119
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    • 2006
  • The development of Fe-based metal matrix composites (MMCs) with high content of hard phase has been approached by combining the use of advanced powder metallurgy techniques like high-energy milling (HEM), cold isostatic pressing (CIP) and vacuum sinterings. A 30% vol. of NbC particles was mixed with Fe powder by HEM in a planetary mill during 10h, characteristing the powder by the observation of morphology and microstructure by scanning electron microscopy (SEM). After of sintering process the variation of density, hardness,carbon content and the microstructural changes observed, permits to find the optimal conditions of processing. Afterwards, a heat treatment study was performed to study the hardenability of the composite.

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Optimization of sintering process of the far-infrared radiation ceramic (원적외선 방사 세라믹의 소결공정 최적화)

  • Park, Jae Hwa;Kim, Hyun Mi;Kang, Hyo Sang;Choi, Jae Sang;Choi, Bong Geun;Nam, Ki Woong;Nam, Han Woo;Shim, Kwang Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.26 no.1
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    • pp.28-34
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    • 2016
  • Far-infrared radiation ceramic is an attractive material that provides thermal therapy by permeating the infrared rays into the deep inside of the human skin. Therefore, it is currently used for thermal therapy devices, thermal mat, heating equipment and so on. This work aims to optimize the sintering process of the far-infrared radiation ceramic with the process parameters of temperature and time. A variety of characterization tools have been used to investigate the optimal sintering condition of far-infrared radiation. The phase of far-infrared radiation ceramic was characterized by using X-ray diffraction (XRD) and microstructure of fracture surface was studied by scanning electron microscopy (SEM). The FT-IR was also performed to measure the far-infrared emissivity.