• Advances in nano research
• /
• v.3 no.2
• /
• pp.81-96
• /
• 2015

Octahedral shaped single crystalline undoped and Ga-doped indium oxide nano-and microcrystals were fabricated using vapor-solid growth process. Effects of Ga doping on the crystallinity, defect structure, and optical properties of the nano-/microstructures have been studied using scanning electron microscopy, microRaman spectroscopy, transmission electron microscopy and cathodoluminescence spectroscopy. It has been observed that incorporation of Ga does not affect the morphology of $In_2O_3$ structures due to its smaller ionic radius, and similar oxidation state as that of In. However, incorporation of Ga in high concentration (~3.31 atom %) causes lattice compression, reduces optical band gap and defect induced CL emissions of $In_2O_3$ nano-/microcrystals. The single crystalline Ga-doped, $In_2O_3$ nano-/microcrystals with low defect contents are promising for optoelectronic applications.

• Korean Journal of Metals and Materials
• /
• v.50 no.11
• /
• pp.847-854
• /
• 2012

Al-doped ZnO (AZO) thin films were grown on quartz substrates by the sol-gel method. The effects of the Al mole fraction on the structural and optical properties of the AZO thin films were investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), and UV-VIS spectroscopy. The particle size of the AZO thin films decreased with an increase in Al concentrations. The optical parameters, the optical band gap, absorption coefficient, refractive index, dispersion parameter, and optical conductivity, were studied in order to investigate the effects of Al concentration on the optical properties of AZO thin films. The dispersion energy, single-oscillator energy, average oscillator wavelength, average oscillator strength, and refractive index at an infinite wavelength of the AZO thin films were affected by the Al incorporation. The optical conductivity of the AZO thin films also increased with increasing photon energy.

• Bulletin of the Korean Chemical Society
• /
• v.33 no.5
• /
• pp.1647-1652
• /
• 2012

With the objective to design and synthesis of Schiff's base symmetrical liquid crystal dimmers and to study the effect of molecular structure variation ($o-ortho$, $m-meta$, $p-para$) and change in alkoxy terminal chain length on mesomorphic properties of liquid crystals, We have synthesized Schiff base dimers from dialdehyde derivative containing 2-hydroxy-1,3-dioxypropylene as short spacer with aniline derivatives having different lengths of terminal alkoxy chains ($n$ = 5, 7, 9). The chemical structure of the final products was characterized by proton nuclear magnetic resonance ($^1H$ NMR) spectroscopy and fourier transform infrared (FT-IR) spectroscopy. The mesomorphic properties and optical textures of the resultant dimers were characterized by differential scanning calorimetry (DSC) and polarized optical microscopy (POM). The existence of smectic A phase transition was confirmed by the observation of batonnets and fan shaped textures in optical microscopy when compound were heated from crystalline phase. All of the dimers of this series, with the exception of $\mathbf{2S_5}$ -ortho, -meta, -para, were thermotropic liquid crystal. The compound $\mathbf{2S_9}$ -meta was monotropic, while the rest were enantiotropic. It was found that the change in terminal alkoxy chain length has pronounced effect on the mesomorphic properties. The temperature range of smectic A phase window widens with increasing alkoxy chain length.

• Korean Journal of Optics and Photonics
• /
• v.23 no.4
• /
• pp.135-142
• /
• 2012

We have developed a measurement method of the refractive index profile of an optical fiber by using diffraction phase microscopy. In the microscope system, the reference light was extracted directly from the probe light that passed through the sample by means of pinhole filtering with a diffraction grating. The spatial interference pattern produced by the probe light and the reference light was processed to generate the phase image of the sample fiber. The index profile was obtained by the inverse Abel transform of the phase profile. In order to remove the background phase that originated from the index difference between the cladding and the surrounding medium, the background phase was calculated from the phase data of the cladding to make a core phase profile that can be directly transformed to the index profile of the core without the full phase image that includes the entire cladding part.

• Proceedings of the KIEE Conference
• /
• 1993.11a
• /
• pp.362-364
• /
• 1993

The properties of near-field diffraction by small aperture are investagated and using of optical fiber taper as a small aperture are proposed. Near-field diffracted by aperture smaller than one wave length can overcome the resolution of conventional microscopy and optical component. In this paper production methods of sub-wave length optical fiber taper using solenoid are also proposed.

• Proceedings of the Optical Society of Korea Conference
• /
• 2001.02a
• /
• pp.60-61
• /
• 2001

We present our experimental results on the recording and retrieving of multiplexed near-field holograms using near-field scanning optical microscopy (NSOM) and a conventional rectangular-parallelepiped or cubic photorefractive crystal. Experimental results show that we can get the angular selectivity comparable with that of the volume hologram and the retrieved spot size was smaller than the Rayleigh's limit. The results also show that the angular selectivity and the retrieved spot size are strongly dependent on the recording distance between the object and the recording medium.

• Proceedings of the Optical Society of Korea Conference
• /
• 2001.02a
• /
• pp.120-121
• /
• 2001

고분해능을 장점으로 하는 근접장 광학 현미경(NSOM)은 최근 높은 관심을 모으고 있으나, 그 촬영 속도가 너무 느린 이유로 실제적인 활용이 미비한 상황이다. scanning 속도를 높이고자 하는 노력들이 많이 진행되고 있으나[1-2] 아직도 실시간 촬영과는 거리가 멀다. 기존의 근접장 광학 현미경(NSOM)은 tuning fork를 사용하여 탐침을 진동시키고 그 진동의 진폭 또는 위상의 변화를 측정함으로써 탐침과 시료의 거리를 측정하는 방식을 사용한다. (중략)

• Proceedings of the Optical Society of Korea Conference
• /
• 2002.11a
• /
• pp.260-261
• /
• 2002

For Near-field Scanning Optical Microscopy measurements, the fiber tip is glued on the side of one of the tuning fork prongs vertically to its extended direction. Higher Q-factor is attainable in this geometry than in the arrangement with the fiber tip parallel to the prong. A simple mechanical design is applied to hold the fiber tip above the gluing point. The overall tuning fork-fiber tip assembly gives another advantage of the flexible Q-factor enhancement. With this treatment, Q-factor higher than 3000 is easily achievable. As an operating instance, a grating is scanned for its one dimensional topographical image.

• Laser Solutions
• /
• v.7 no.2
• /
• pp.11-18
• /
• 2004

We propose a novel application of optical coherence tomography (OCT) to monitor pit formation in laser irradiated optical storage materials. A multilayer optical storage recordable compact disk, is composed of multiple layers, each of different structure. Disks were irradiated with aQ-Switched Nd:YAG laser with an energy of 373 mJ. Post-irradiated disks were evaluated by OCT and those images were compared with optical microscopy. Our results indicate that OCT is a useful instrument to investigate pit formation in multilayer optical storage disks and might also provide information to optimize optical memory technology.

• Proceedings of the Materials Research Society of Korea Conference
• /
• 2011.05a
• /
• pp.22.2-22.2
• /
• 2011

Reliability and degradation mechanism of conventional phosphor-converted white GaN-based light-emitting diodes (LEDs) were investigated. Under electro-thermal stress condition, the optical output degraded rapidly at the initial stress time accompanied by the change of chromatic properties. This could be attributed to the optical degradation of packaged materials, in particular, the browning of encapsulants and the darkening of reflective packages. At longer stress times, the optical output gradually decreased according to the degree of the reverse leakage currents, namely, the generation ofnonradiative recombination defects. This indicates that the optical degradation of white LEDs are dominated by the darkening of packaged materials and the generation of defects depending on the injection current and ambient temperatures. Using analyses of electroluminescence spectra, optical microscopy, electrical, optical, and thermal properties, optical degradations of white LEDs are discussed.