• Title/Summary/Keyword: Optical Measurement

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Fabrication and characterization of GaN substrate by HVPE (HVPE법으로 성장시킨 GaN substrate 제작과 특성 평가)

  • Oh, Dong-Keun;Choi, Bong-Geun;Bang, Sin-Young;Eun, Jong-Won;Chung, Jun-Ho;Lee, Seong-Kuk;Chung, Jin-Hyun;Shim, Kwang-Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.20 no.4
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    • pp.164-167
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    • 2010
  • Bulk GaN single crystal with 1.5 mm thickness was successfully grown by hydride vapor phase epitaxy (HVPE) technique. Free-standing GaN substrates of $10{\times}10,\;15{\times}15$ mm size were fabricate after lift-off of sapphire substrate and their optical properties were characterized properties for device applications. X-ray diffraction patterns showed (002) and (004) peak, and the FWHM of the X-ray rocking curve (XRC) measurement in (002) was 98 arcsec. A sharp photoluminescence spectrum at 363 nm was observed and defect spectrum at visible range was not detected. The hexagonal-shaped etch-pits are formed on the GaN surface in $200^{\circ}C\;H_3PO_4$ at 5 minutes. The defect density calculated from observed etch-pits on surface was around $5{\times}10^6/cm^2$. This indicates that the fabricated GaN substrates can be used for applications in the field of optodevice, and high power electronics.

Properties of Pt/${Al_0.33}{Ga_0.67}N$ Schottky Type UV Photo-detector (Pt 전극을 이용한 ${Al_0.33}{Ga_0.67}N$ 쇼트키형 자외선 수광소자의 동작특성)

  • 신상훈;정영로;이재훈;이용현;이명복;이정희;이인환;한윤봉;함성호
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.40 no.7
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    • pp.486-493
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    • 2003
  • Schottky type A $l_{0.33}$G $a_{0.67}$N ultraviolet photodetectors were fabricated on the MOCVD grown AlGaN/ $n^{+}$-GaN and AlGaN/AlGaN interlayer/ $n^{+}$-GaN structures. The grown layers have the carrier concentrations of -$10^{18}$, and the mobilities were 236 and 269 $\textrm{cm}^2$/V.s, respectively. After mesa etching by ICP etching system, the Si3N4 layer was deposited for passivation between the contacts and Ti/AL/Ni/Au and Pt were deposited for ohmic and Schottky contact, respectively. The fabricated Pt/A $l_{0.33}$G $a_{0.67}$N Schottky diode revealed a leakage current of 1 nA for samples with interlayer and 0.1$\mu\textrm{A}$ for samples without interlayer at a reverse bias of -5 V. In optical measurement, the Pt/A $l_{0.33}$G $a_{0.67}$N diode with interlayer showed a cut-off wavelength of 300 nm, a prominent responsivity of 0.15 A/W at 280 nm and a UV-visible extinction ratio of 1.5x$10^4./TEX>.

An Analysis of Global Solar Radiation using the GWNU Solar Radiation Model and Automated Total Cloud Cover Instrument in Gangneung Region (강릉 지역에서 자동 전운량 장비와 GWNU 태양 복사 모델을 이용한 지표면 일사량 분석)

  • Park, Hye-In;Zo, Il-Sung;Kim, Bu-Yo;Jee, Joon-Bum;Lee, Kyu-Tae
    • Journal of the Korean earth science society
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    • v.38 no.2
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    • pp.129-140
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    • 2017
  • Global solar radiation was calculated in this research using ground-base measurement data, meteorological satellite data, and GWNU (Gangneung-Wonju National University) solar radiation model. We also analyzed the accuracy of the GWNU model by comparing the observed solar radiation according to the total cloud cover. Our research was based on the global solar radiation of the GWNU radiation site in 2012, observation data such as temperature and pressure, humidity, aerosol, total ozone amount data from the Ozone Monitoring Instrument (OMI) sensor, and Skyview data used for evaluation of cloud mask and total cloud cover. On a clear day when the total cloud cover was 0 tenth, the calculated global solar radiations using the GWNU model had a high correlation coefficient of 0.98 compared with the observed solar radiation, but root mean square error (RMSE) was relatively high, i.e., $36.62Wm^{-2}$. The Skyview equipment was unable to determine the meteorological condition such as thin clouds, mist, and haze. On a cloudy day, regression equations were used for the radiation model to correct the effect of clouds. The correlation coefficient was 0.92, but the RMSE was high, i.e., $99.50Wm^{-2}$. For more accurate analysis, additional analysis of various elements including shielding of the direct radiation component and cloud optical thickness is required. The results of this study can be useful in the area where the global solar radiation is not observed by calculating the global solar radiation per minute or time.

Synthesis and Magnetic Properties of Nanosized Ce-substituted Yttrium Iron Garnet Powder Prepared by Sol-gel Method (졸-겔법에 의한 Cerium 치환 Nanosize YIG 분말의 합성 및 자기적 특성)

  • 장학진;김광석;윤석영;김태옥
    • Journal of the Korean Ceramic Society
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    • v.38 no.11
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    • pp.1008-1014
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    • 2001
  • Nanosize YIG powders added by Cerium which is exellent element in magneto-optical effect were synthesized by Sol-Gel method using Ethylene Glycol solvent. In 120 to 150 minute reaction time, stable sol solution which showed no change in viscosity, pH, and aging time was obtained. Monolithic YIG was synthesized at 80$0^{\circ}C$ with DTA and XRD measurement and its lattice parameter had a tendency to increase from 12.3921 $\AA$. Increasing annealing temperature from 80$0^{\circ}C$ to 105$0^{\circ}C$, average particle size was in the range of 40 nm to 330 nm. Saturation magnetization (M$_{s}$) value was increased from 18.37 to 21.25 emu/g due to enhancement of YIG crystallity and decreasing of orthoferrite phase. On the other hand, coercivity (H$_{c}$) value increased up to 90$0^{\circ}C$ and then decreased above 90$0^{\circ}C$. With increasing Ce addition, coercivity was almost not changed but saturation magnetization value was maximum at Ce 0.1 mol% and then decreased because of increasing a orthoferrite amount. Also, curie temperature (T$_{c}$) of YIG were not changed with Ce addition.ion.

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The study for fabrication and characteristic of Li$_2$O-2SiO$_2$conduction glass system using conventional and microwave energies (마이크로파와 재래식 열원을 이용한 고체 전지용 Li$_2$O-2SiO$_2$계 전도성 유리의 제조 및 특성에 관한 연구)

  • Park, Seong-Soo;Kim, Kyoung-Tae;Kim, Byoung-Chan;Park, Jin;Park, Hee-Chan
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.10 no.1
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    • pp.66-72
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    • 2000
  • The behavior of nucleation and crystallization in the $Li_2O_3-SiO_2$ glass heat-treated at different condition under the conventional and microwave processing was studied by differential thermal analysis (DTA), X-ray diffractometry (XRD), optical microscopy (OM), and electrical conductivity measurement. Nucleation temperature and temperature of maximum nucleation rate in both conventionally and microwave heat-treated samples were 460~$500^{\circ}C$ and $580^{\circ}C$, respectively. It was expected that the probability for bulk crystallization increased in microwave heat-treated sample, compared to conventionally heat-treated one. Degree of crystallization increased with increasing crystallization temperature in both conventionally and microwave heat-treated samples. However, pattern of crystallization growth under microwave processing appeared to be quite different from that under the conventional one due to its internal or volumetric heating. Electrical conductivity of conventionally and microwave heat-treated samples were 1.337~2.299, 0.281~~$0.911{\times}10^{-7}\Omega {\textrm}{cm}^{-1}$, respectively.

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Effect of Concentration and Surface Property of Silica Sol on the Determination of Particle Size and Electrophoretic Mobility by Light Scattering Method (광산란법에서 실리카 졸의 농도 및 표면특성이 입자 크기 및 전기영동 이동도 측정결과에 미치는 영향)

  • Cho, Gyeong Sook;Lee, Dong-Hyun;Kim, Dae Sung;Lim, Hyung Mi;Kim, Chong Youp;Lee, Seung-Ho
    • Korean Chemical Engineering Research
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    • v.51 no.5
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    • pp.622-627
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    • 2013
  • Colloidal silica is used in various industrial products such as chemical mechanical polishing slurry for planarization of silicon and sapphire wafer, organic-inorganic hybrid coatings, binder of investment casting, etc. An accurate determination of particle size and dispersion stability of silica sol is demanded because it has a strong influence on surface of wafer, film of coatings or bulks having mechanical, chemical and optical properties. The study herein is discussed on the effect of measurement results of average particle size, sol viscosity and electrophoretic mobility of particle according to the volume fraction of eight types of silica sol with different size and surface properties of silica particles which are presented by the manufacturer. The measured particle size and the mobility of these sol were changed by volume fraction or particle size due to highly active surface of silica particle and change of concentration of counter ion by dilution of silica sol. While in case the measured sizes of small particles less than 60 nm are increased with increasing volume fraction, the measured sizes of larger particles than 60 nm are slightly decreased. The mobility of small particle such as 12 nm are decreased with increase of viscosity. However, the mobility of 100 nm particles under 0.048 volume fraction are increased with increasing volume fraction and then decreased over higher volume fraction.

Study on the Preparation and Characterization of Ophthalmic Polymer with High and Low-Water Content

  • Lee, Min-Jae;Sung, A-Young
    • Journal of the Korean Chemical Society
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    • v.61 no.6
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    • pp.346-351
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    • 2017
  • This study was planned considering the chain length, hydrophilicity, and hydrophobicity of the additives to be used in the polymerization, while various ophthalmic lenses that use various additives with similar water contents were manufactured before their optical and physical properties were compared and analyzed. With regard to the additives required for manufacturing high-, medium-, and low-water content lens groups, HEA (hydroxyethyl acrylate), PVP (polyvinylpyrrolidone), and NMV(N-methyl-N-vinylacetamide) were used as additives for preparing the high-water content lens group, HEMA(2-hydroxyethyl methacrylate), HPMA(hydroxypropyl methacrylate) and BD(1,4-butanediol) were used for the medium-water content lens group. For the low-water content lens group, BMA(buthyl methacrylate), BDDA(1,4-butanediol diacrylate), and Bis-GMA(bisphenol A glycerolate diacrylate) were used, respectively. The average water content of HEA was 40.14%; that of PVP, 39.63%; and that of NMV, 40.52%. The mean of water content was 35.92% for HEMA, 35.74% for BD, and 34.62% for HPMA. For the low-water content lens group, the mean of water content was 26.69% for BMA, 27.76% for BDDA, and 26.14% for Bis-GMA. With regard to the results of the water content measurement using a moisture analyzer, the average water content of the high-water content lens group was 41.34% for HEA, 42.62% for PVP, and 42.73% for NMV. Finally, for the low-water content lens group, the average water content was 28.62% for BMA, 28.82% for BDDA, and 28.32% for Bis-GMA. The measurements of the water contents of the lenses using the two methods showed that the water content and refractive index of the lenses were similar in all the lens groups. The measurements of the contact angles, however, showed a different wettability value for each lens with a similar water content. Also, the change tendency of the lens curvature according to the change of time showed that the change amount became larger and the recovery time became longer from the lens samples with a lower water content to those with a higher water content. Based on these results that will be helpful for the study of ophthalmic lenses.

Improvement of PWM Driving Control Characteristics for Low Power LED Security Light (저전력형 LED 보안등의 PWM형 구동제어 특성 개선)

  • Park, Hyung-Jun;Kim, Nag-Cheol;Kim, In-Su
    • Journal of IKEEE
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    • v.21 no.4
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    • pp.368-374
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    • 2017
  • In this Paper, we developed a low power type LED security light using LED lighting that substitutes a 220[V] commercial power source for a solar cell module instead of a halogen or a sodium lamp. in addition, a PWM type drive control circuit is designed to minimize the heat generation problem and the drive current of the LED drive controller. in developed system, The light efficiency measurement value is 93.6[lm/W], and a high precision temperature sensor is used inside the controller to control the heat generation of the LED lamp. In order to eliminate the high heat generated from the LED lamp, it is designed to disperse quickly into the atmosphere through the metal insertion type heat sink. The heat control range of LED lighting was $50-55[^{\circ}C]$. The luminous flux and the lighting speed of the LED security lamp were 0.5[s], and the beam diffusion angle of the LED lamp was about $110[^{\circ}C]$ by the light distribution curve based on the height of 6[m].

Fabrication and Characterization of Wavelength Conversion Device with Periodically Poled Ridge-type Waveguide in MgO:LiNbO3 (주기적으로 분극 반전된 MgO:LiNbO3를 이용한 리지형 광도파로 파장가변 소자 제작 및 특성)

  • Lee, H.M.;Yang, W.S.;Kim, W.K.;Lee, H.Y.;Jeong, W.J.;Kwon, S.W.;Koo, K.H.;Song, M.G.
    • Korean Journal of Optics and Photonics
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    • v.19 no.3
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    • pp.199-207
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    • 2008
  • Wavelength converting devices with a ridge-type waveguide in periodically poled $MgO:LiNbO_3$ are made and characterized. The experimental results are compared with theoretical analysis on the effects of waveguide dimension and duty ratio of the periodically poled structure. To show the relationship of the conversion efficiency to those factors, a new measurement system is configured. That experimental results show that the center wavelength, normalized conversion efficiency and full width half maximum of the conversion efficiency curve are 1067.45 nm, 90.7%/$Wcm^2$ and 0.17 nm, respectively. Also, the estimated results of the duty period and full width half maximum of the conversion efficiency from theoretical calculations agreed well with experimental results with the errors of 0.016 ${\mu}m$ and 0.01 nm.

Study on the Non-isothermal Crystallization Kinetics of Branched Polypropylene (분지형 폴리프로필렌의 비등온결정화 거동 연구)

  • Yoon, Kyung-Hwa;Shin, Dong-Yup;Kim, Youn-Cheol
    • Polymer(Korea)
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    • v.36 no.2
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    • pp.245-250
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    • 2012
  • Branched polypropylenes (PP) with long chain branch were prepared by solid state reaction with three different branching agent of 0.3 wt% content. The chemical structures, non-isothermal crystallization behavior and complex viscosity of the branched PP were investigated by FTIR, DSC, optical microscope, and dynamic rheological measurement. The chemical structure of the branched PP was confirmed by the existence of =C-H stretching peak of the branching agent at 3100 $cm^{-1}$. There was no distinct change in melting temperature in case of PP-D-0-3 and PP-F-0-3, but PP-H-0-3 indicated a decrease in melting temperature. The decrease in melting temperature was interpreted by the fact that the degradation reaction of PP was more dominant than branched reaction, and confirmed by a decrease in complex viscosity. The non-isothermal crystallization behavior of the branched PP was analyzed using by Avrami equation. The Avrami exponent of PP was 3, and the values of the branched PP with DVB and FS were below 3. The activation energy of PP calculated by Kissinger method was 25 kJ/mol, and there were no big difference in activation energies of the branched PPs compared to PP.