• Analytical Science and Technology
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• v.31 no.3
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• pp.107-111
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• 2018

Currently, ultraviolet-visible spectrophotometry and titration methods are used for assay tests of tramadol hydrochloride injection and raw material in the Korean Pharmacopoeia XI (KP XI). Titration has also been used in the British Pharmacopoeia (BP 2013) for the assay test of tramadol hydrochloride, and the HPLC assay for tramadol hydrochloride raw material has been used in the United States Pharmacopeia (USP 39). In this study, we developed an alternative HPLC assay method for tramadol hydrochloride injection that is up to date and specific, and employs the same method as tramadol hydrochloride capsules. Validation of the HPLC method was conducted to determine linearity, precision, accuracy, system suitability, and robustness. The linearity of the calibration curves in the desired concentration range was good ($r^2$ > 0.9999). RSDs of intra-day precision obtained were 0.05-0.08 % and inter-day precision obtained were 0.08-0.19 %. Accuracy was obtained with recoveries in the range of 98.16 % and 100.90 %. As a result of the system's suitability, the RSD of both retention time and the peak area obtained were 0.07 %. The values of the plate number and tailing factor of tramadol hydrochloride obtained were 7076 and 1.16, respectively. Because of the intermediate precision and robustness of the developed assay, it is expected to become a valuable tool for revising the Korean Pharmacopoeia (KP XI).

• Journal of the Korean Institute of Landscape Architecture
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• v.18 no.4
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• pp.17-28
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• 1991

The purpose of this study is to investigate and present a method for measuring public accessibility to urban open spaces. A basic assumption is that, for urban open space policies, accessibility is more important than per capita area. In this study, for the purpose of simplicity, a residential area is assumed to have access to open space if it is within a certain distance from an urban open space. Official city planning map is overlayed with a 200m grid and each cell of dwelling area is checked whether it is within a certain distance from a cell categorized as urban open space. A computer program for widely commercialized personal computer is developed for data processing so that local governments without access to more sophisticated systems can carry out similar studies for their own jurisdictions. Five cities, big, small, old and new, are selected to test the proposed method. Dwelling areas of Ansan new Town have highest accessibility to open spaces(93.4% of dwelling cells have open space cell within 500m). Seoul (91.2%), Suwon(78.2%), Pusan(73.8%), and Inchon(61.4%) have less accessibility. If we assume the Ansan City residents are evenly distributed over the dwelling area, 93.4% of the population has open spaces within walking distance of 500m. However, if we consider physical barriers such as arterial roads, railroads, and streams that reduce the accessibility, less than 93.4% of Ansan city residents enjoy good access to open spaces. Though a further detailed analysis is needed to picture the microscopic accessibility, this method can serve as a useful tool for urban open space policy and open space alternatives evaluations.

• Journal of Korean Society on Water Environment
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• v.36 no.2
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• pp.148-152
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• 2020

The quantitative accuracy of dry rehydratable film method was compared with the standard culture method to analyze the applicability of dry rehydratable film in the total aerobic bacteria test for water. The materials used in this study were 500 cases of water and were tested according to the Korean official test method for drinking water. The mean value of the total aerobic bacteria in plate count agar(PCA) and MC-Media Pad AC(MAC) were 2.6 ± 1.1 Log cfu/mL and 2.6 ± 1.2 Log cfu/mL. The p value and correlation coefficient(R²) were 0.933 and 0.9985 between the PCA and MAC, respectively, indicating no significant difference and very high correlation. According to the water types, the p value and R² were 0.887 and 0.9911 in the PCA and MAC. In the purified water, the p value was 0.973 and R² was 0.9934 in the PCA and MAC of other water. In each type of water, there were no significant differences between the PCA and MAC, and the correlation was very high. Thus, it is suggested that the MAC would be available for total aerobic bacteria test for water.

• The Korean Journal of Applied Statistics
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• v.23 no.5
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• pp.891-908
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• 2010

In Korea, the small area estimation method is currently unpopular in generating o cial statistics. Because it may be difficult to determine the reliability for small area estimation, although small area estimation ha a sufficiently good advantage to generate small area statistics for Korea. This paper inspects the method of making small area unemployment through the small area estimation method. To estimate small area unemployment we used an EBLUP-type estimator based on a logistic linear mixed model. To evaluate the EBLUP-type estimator we accomplished the real data analysis and simulation experiment from the population and housing census data. In addition, small area estimates are compared to large sample survey estimates. We found the provided method in this paper is highly recommendable to generate small area unemployment as the official statistics.

• Korean Journal of Environmental Agriculture
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• v.13 no.1
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• pp.90-97
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• 1994

This experiment was conducted to improve the analytical method of tricyclazole- and IBP-combined dust. When the tricyclazole and IBP active ingadients were analyzed by the official analytical method, their recovery rates were 89.5 and 100%, respectively. A reason of the lower recovery rate in tricyclazole was found to be due to strong binding to the minor inorganic compoments, $Al_2O_3$, $Fe_2O_3$, CaO and MgO, of talc and kaoline. However, addition of 0.2% dimethylamine to extraction solvent for tricyclazole- and IBP-combined dust effectively raised the recovery rate of tricyclazole by providing higher basicity than tricyclazole. We have suggest an improved analytical method which is applicable to effective and simultaneous analysis of the active ingradients of tricyclazole- and IBP-combined dust.

• Journal of KIISE
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• v.43 no.9
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• pp.1060-1065
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• 2016

Recently, there is an emerging need for parallel UHD video processing, and the usage of computing systems that have an asymmetric processor such as ARM big.LITTLE is actively increasing. Thus, a new parallel UHD video processing method that is optimized for the asymmetric multicore systems is needed. This paper proposes a novel HEVC tile partitioning method for parallel processing by analyzing the computational power of asymmetric multicores. The proposed method analyzes (1) the computing power of asymmetric multicores and (2) the regression model of computational complexity per video resolution. Finally, the model (3) determines the optimal HEVC tile resolution for each core and partitions/allocates the tiles to suitable cores. The proposed method minimizes the gap in the decoding time between the fastest CPU core and the slowest CPU core. Experimental results with the 4K UHD official test sequences show average 20% improvement in the decoding speedup on the ARM asymmetric multicore system.

• Journal of the Korean Chemical Society
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• v.38 no.12
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• pp.880-884
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• 1994

An indirect spectrophotometric method, presumably heretofore unmentioned, for the rapid determination of COD in the presence of chloride of high concentration is described. The alkaline sample is refluxed to react with a definite amount of permanganate, present in excess. A photometric measurement at 535 nm for the extent of the fading of the permanganate color after refluxing completes the procedure. The optimum conditions which give the absorbance-concentration plot the maximum linearity and slope in the range of 0∼5 ppm COD are as follows: reflux at $100\circC$ for 10 min in the presence of 0.15 mM permanganate and 0.2% NaOH with a sample size of 5 ml. An overall running time was less than 15 min. The t-test reveals that the proposed method is not significantly different from the official method.

• Analytical Science and Technology
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• v.14 no.2
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• pp.173-179
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• 2001

The study was carried out to analyze the pollutant Fe, Cu, Cr, Zn, Cd for sediments collected from lake in K river basin. Three analytical methods currently used in Korea, Japan, U.S.A, were compared. Pretreatment using microwave digestion showed higher analytical results for Fe, Cu, Cr, Zn, Cd than Korean Official Method(KOM) and American Toxicity Characteristic Leaching Procedure(TCLP) Method. Also, analytical results using microwave digestion, TCLP and KOM were as follows: 38.1-48.0 mgFe/kg, 10.2-15.9 mgFe/kg AND 3.5-12.6 mgFe/kg, 37.0-50.1 mgCu/kg, 0.06-0.24 mgCu/kg and 0.01-0.03 mgCu/kg, 137.0-152.0 mgZn/kg, 0.67-0.82 mgZn/kg and 0.3-0.5 mgZn/kg, respectively. From this result, a new analytical method for the determination of heavy metal in sediment should be developed for the accurate estimation of pollution degree in sediment.

• Journal of Internet Computing and Services
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• v.17 no.1
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• pp.73-81
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• 2016

This paper deals with the practical experience and lessons to develop a method of course-embedded assessment for program outcomes in Computer Science & Information Engineering. In engineering education, ABEEK(Accreditation Board for Engineering Education of Korea) has been nominated as an official accreditation from Korean government under some conditions of fulfillment. One of the conditions is enforcement of course-embedded assessment for program outcomes. In this paper, a method of course-embedded assessment in Computer Science & Information Engineering is suggested. The case study was done in a basic project course which includes the special assessment methods in project courses. The case study of course-embedded assessment in a basic project course was given with consideration for each step, that is, set up of program outcomes which are highly related to the course, selection of assessment tools such as written examination and project-based assessment, set up of assessment criteria, implementation of course-embedded assessment, and analysis of results. The proposed method is expected to be a good example to construct the whole strategy for course-embedded assessment in Computer Science & Information Engineering.

• Journal of the Korea Institute of Information and Communication Engineering
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• v.19 no.6
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• pp.1277-1282
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• 2015

This paper describes a research for improvement official approval of information processing in national technical qualification. In this paper, we analysis the contents of current exams and propose the new evaluation method of practical exam in information processing fields through grafting new trends of ICT and ability unit, fulfillment criteria in national competency standards(NCS). Also, we have verified the effect of exam through the pilot test. In the future, we will apply the new exams after the revision of guidelines for marking questions by expert group in its duty fields basis on this research