• Analytical Science and Technology
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• v.16 no.4
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• pp.277-282
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• 2003

The amount of water for the cultivation of citrus is different based on the growing period. The effect of water stress induces to enhance of sugar accumulation in citrus. The water content in the leaves of citrus can be a index for watering during cultivation. The purpose of this study is to determine the water content of citrus leaves non-destructively by using near infrared spectroscopy (NIRS). Citrus leaves were prepared from 'Okitsu' Satusuma mandarin leaves (Citrus unshiu Marc.) ranging from 20.80 to 69.98% of water content by loss on drying method, and NIR reflectance spectra of citrus leaves were acquired by using a fiber optic probe. It was found that the variation of absorbance band 1450 nm from OH vibration of water depending on the water content change. Partial least squares regression (PLSR) was applied to develop a calibration model over the spectral range 1100-1700 nm. The calibration model predicted the water content for the validation set with a standard errors of prediction (SEP) of 0.97%. In order to validate the developed calibration model, routine analyses were performed using independently prepared citrus leaves. The NIR routine analyses showed good results with those of loss on drying method with a SEP of 0.81%. The rapid and non-destructive determination of the water content in citrus leaves was successfully performed by portable NIR system.

• Korean Journal of Agricultural Science
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• v.48 no.2
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• pp.299-310
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• 2021

Glycerol is a non-volatile compound with no aromatic properties that contributes significantly to the quality of wine by providing sweetness and richness of taste. In addition, it is also the third most significant byproduct of alcoholic fermentation in terms of quantity after ethanol and carbon dioxide. In this study, Fourier transform infrared (FT-IR) spectroscopy was employed as a fast non-destructive method in conjugation with multivariate regression analysis to build a model for the quantitative analysis of glycerol concentration in wine samples. The samples were prepared by using three varieties of red wine samples (i.e., Shiraz, Merlot, and Barbaresco) that were adulterated with glycerol in concentration ranges from 0.1 to 15% (v·v^-1), and subjected to analysis together with pure wine samples. A net analyte signal (NAS)-based methodology, called hybrid linear analysis in the literature (HLA/GO), was applied for predicting glycerol concentrations in the collected FT-IR spectral data. Calibration and validation sets were designed to evaluate the performance of the multivariate method. The obtained results exhibited a high coefficient of determination (R²) of 0.987 and a low root mean square error (RMSE) of 0.563% for the calibration set, and a R² of 0.984 and a RMSE of 0.626% for the validation set. Further, the model was validated in terms of sensitivity, selectivity, and limits of detection and quantification, and the results confirmed that this model can be used in most applications, as well as for quality assurance.

• Journal of the Korean Wood Science and Technology
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• v.36 no.1
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• pp.61-68
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• 2008

The effect of rupture on the speed of ultrasonic wave was investigated with the PUNDIT and the effective detecting method of defects, moving transmitter and receiver. The speed of ultrasonic wave according to the course of rupture was not affected by transmitter and receiver and in the course of parallel rupture, but only in the course of vertical rupture. When rupture was not located on the ultrasonic wave progressing course, rupture was not detected. However, if rupture was formed perpendicularly to the ultrasonic wave progressing course but located on the ultrasonic wave progressing direction, rupture can be detected. Also, the rupture can be detected, when one transmitter and receiver was placed at top and the other at bottom. After detecting rupture in a part, rupture was determined accurately, placing and moving two transmitters and receivers at width.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.34 no.2
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• pp.415-424
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• 2014

The carrying capacity of existing concrete structures is evaluated by the measured data from displacement and strain gauges for given loads and the results of numerical analysis that are compared with the measured ones. Consequently, this process could be accomplished in doing the direct measurement of residual stress on existing concrete. This study is concerned with the development of IITC (Instrumented Indentation Technique for Concrete) system which is based on the experimental stress analysis technique using non-destructive test method to evaluate the residual stress of concrete structures depending on the types of applied loadings in analysing indentation load - indentation depth curve derived experimentally on concrete surface. As a result, in this paper, almost all of systematized H/W and S/W were newly developed to estimate the residual stresses of concrete structures. Thus, the creation of new experimental equations for deriving residual stresses and automatical calculations of residual stresses using the empirical formula can lead to evaluate the structural resistances conveniently in the structures from construction phase to maintenance stage.

• Journal of the Korean Society for Nondestructive Testing
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• v.15 no.2
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• pp.378-385
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• 1995

The ultrasonic non-destructive testing uses the directivity of the ultrasonic pulse wave which propagates in one direction. The directivity is expressed as the relationship between the propagate direction and its sound pressure. The directivity of ultrasonic wave is closely related to determination of probe arrangement, testing sensitivity, scanning pitch and defect location and characterization. The paper measured the directivity of shear wave, which reflected from artificial defect located in weld metal zone in butt welded joint similar model made of pyrex glass by using visualization method. 2 MHz and 4 MHz angle probes were used to measure the directivity of reflection wave at the artificial defect. The directivity of shear waves reflected from the defect was different according to the probe position and the shape of butt welded joint. The difference of directivity of reflection wave was existed between 2 MHz and 4 MHz angle probes. The angle of reflection wave became equal to angle of incidence as increase of the height of excess metal.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.1
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• pp.177-189
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• 1998

The contents of this paper include a non-destructive technique for evaluating the degradation of the boiler superheater tube in a fossil power plant through an electrochemical polarization test. Correlation between Ip of polarization parameter and SP-DBTT for the superheater tubes in long-term use was obtained. 1.0Cr-0.5Mo steel was degraded by softening, and the degree of degradation was dependent upon carbides with Cr and Mo elements. Since brittle fracture at low temperature and ductile fracture mode at high temperature were shown, similarity between standard Charpy and small punch tests could be found. In addition, SP-DBTT showing the degree of degradation was higher, as the time-in use of the materials got longer. Electrolyte including picric acid of 1.3 g in distilled water of 100ml at 25.deg. C temperature and sodium tridecylbenzene sulfonate with 1g could be applied to evaluate the degradation of 1.0Cr-0.5Mo steel by means of the electrochemical polarization test. Ip and Ipa values measured through the electrochemical test are the appropriate parameters for representing the degradation of the superheater tube(1.0Cr-0.5Mo steel) for the fossil power plant. It is poassible to evaluate the degradation of materials with different time histories electrochemically, by Ip value only, at field test.

• Journal of the Korean Society for Nondestructive Testing
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• v.36 no.4
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• pp.300-307
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• 2016

The faults in railway vehicle components may result in either the stoppage of the service and the derailment of the vehicle. Therefore, it is important to diagnose and monitor the main components of a railway vehicle. The use of temperature is one of the basic methods for the diagnosis of abnormal conditions in the rotational components of a railway vehicle, such as bearings, reduction gears, brake discs, wheels and traction motors. In the present study, the diagnose of the rotational components using infrared thermography and a pattern recognition technique was carried out and a field test was performed. The results show that this method of diagnosis using infrared thermography can be used to identify abnormal conditions in rotational components of a railway vehicle.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.32 no.3
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• pp.30-36
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• 2004

As fiber reinforced composite materials are widely used in aircraft, space structures and robot arms, the study on the non-destructive testing methods of the composite materials has become an important research area for improving their reliability and safety. In this paper, the AE signal analyzer with the resonance circuit to extract the specified frequency of the acoustic emission signal were designed and fabricated. The noise levels of the fabricated AE signal analyzer by the disturbance such as impact or mechanical vibration had a very small value comparable to those of the conventional AE signal analyzer. Also, the fabricated AE signal analyzer was proved to have about the same crack detection capabilities with the conventional AE signal analyzer under the static and dynamic tensile tests of the composite materials.

• Food Science and Preservation
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• v.12 no.6
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• pp.608-612
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• 2005

Fourier transform-near infrared (FT-NIR) spectroscopy is a simple, rapid, non-destructive technique which can be used to make quantitative analysis of chemical composition in grain. An interest in total dietary fiber (TDF) of grain such as rice has been increased due to its beneficial effects for health. Since measuring methods for TDF content were highly depending on experimental technique and time consumptions, the application of FT-NIR spectroscopy to determine TDF content in milled rice. Results of enzymatic-gravimetric method were $1.17-1.92\%$ Partial least square (PLS) regression on raw NIR spectra to predict TDF content was developed Accuracy of prediction model for TDF content was certified for regression coefficient (r), standard error of estimation (SEE) and standard error of prediction (SEP). The r, SEE and SEP were 0.9705, 0.0464, and 0.0604, respectively. The results indicated that FT-NIR techniques could be very useful in the food industry and rice processing complex for determination of TDF in milled rice on real time analysis.

• The Journal of Advanced Prosthodontics
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• v.8 no.2
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• pp.101-109
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• 2016

PURPOSE. To investigate the void parameters within the resin cements used for fiber post cementation by micro-CT (${\mu}CT$) and regional push-out bonding strength. MATERIALS AND METHODS. Twenty-one, single and round shaped roots were enlarged with a low-speed drill following by endodontic treatment. The roots were divided into three groups (n=7) and fiber posts were cemented with Maxcem Elite, Multilink N and Superbond C&B resin cements. Specimens were scanned using ${\mu}CT$ scanner at resolution of $13.7{\mu}m$. The number, area, and volume of voids between dentin and post were evaluated. A method of analysis based on the post segmentation was used, and coronal, middle and apical thirds considered separately. After the ${\mu}CT$ analysis, roots were embedded in epoxy resin and sectioned into 2 mm thick slices (63 sections in total). Push-out testing was performed with universal testing device at 0.5 mm/min cross-head speed. Data were analyzed with Kruskal-Wallis and Mann-Whitney U tests (${\alpha}=.05$). RESULTS. Overall, significant differences between the resin cements and the post level were observed in the void number, area, and volume (P<.05). Super-Bond C&B showed the most void formation ($44.86{\pm}22.71$). Multilink N showed the least void surface ($3.51{\pm}2.24mm^2$) and volume ($0.01{\pm}0.01mm^3$). Regional push-out bond strength of the cements was not different (P>.05). CONCLUSION. ${\mu}CT$ proved to be a powerful non-destructive 3D analysis tool for visualizing the void parameters. Multilink N had the lowest void parameters. When efficiency of all cements was evaluated, direct relationship between the post region and push-out bonding strength was not observed.