• Journal of the Korean Chemical Society
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• v.34 no.2
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• pp.130-135
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• 1990

The title compound (C13H17NO2S) is monoclinic, space group P21/a, with a = 13.756 (3), b = 9.310(4), c = 21.305(3) $\AA$, $\beta$ = 95.0。, Z = 8, V = 2718.11 $\AA$3, Dc = 1.23$g·{\cdot}cm-3$, (Mo k$\alpha$) = 0.71069$\AA$,$\mu$ = 2.18 cm-1, F(000) = 1071.86, T = 298, R = 0.085 for 2935 unique observed reflections with I >2.0$\sigma$(I). The structure was solved by direct methods. The C-H bond lengths and the methyl groups are fixed and refined as their ideal geometry by allowing to ride on the parent atoms. Both molecules A and B have almost same structures except for two terminal ethyl groups. The ethylene-like skeleton including the nitro group in one molecule is nearly perpendicular to the plane of the methylbenzene group and two ethyl groups form a cis-type structure which has the dfferent orientations between two molecules; in the molecule A, two terminal methyl groups being the opposite directional arrangement against the plane of its skeleton, while in the B, with the same directional structure from its plane. The molecules in the crystal are packed together by non-bonded van der Waals forces.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2005.04a
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• pp.464-470
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• 2005

The numerical analysis is carried out to identify the influence of design factors to shear capacity of cast-in-place (CIP) anchor in ACI 349 Code that is available for the design of fastening system at Nuclear Power Plant (NPP) in this study. The MASA program is used to develop the numerical analysis model and the developed numerical analysis model is verified on a basis of the various test data of CIP anchor. Both $l/d_o$ and $c_1/l$ we considered as design factors. As a result, the variation of $l/d_o$ has no influence on the shear capacity of CIP anchor but $c_1/l$ has a large influence on the shear capacity of CIP anchor, Therefore, it is proved that ACI 349 Code may give a non-conservative results compared with real shear capacity of CIP anchor according to $c_1/l$.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.12 no.1
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• pp.1-8
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• 2013

This study investigates life and damage due to structural and fatigue load at speaker placer with wall hanger type. As the small stress and deformation are shown at the models of A, B and C shapes on structural analysis, there is no problem at installing speaker placer. As the largest stress is happened at the middle part of joint on the models of A, B and C shapes, this part must be considered at the design. A shape is thought to have most fatigue damage among 3 shape models. C shape model has most excellent, but A model has least at fatigue durability. This study result is applied with the design of speaker placer and it can be useful at predicting prevention and durability against its damage.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.17 no.2
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• pp.103-108
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• 2018

In interrupted cutting, the workpiece has a groove that impacts both the cutting tool and the workpiece. Therefore, cutting tool damage occurs rapidly. In this study, I performed interrupted cutting of carbon steel for machine structures (SM20C) using an uncoated carbide tool (SNMG120404, P20), and observed tool damage, cutting chip shape, and the workpiece surface. Results: Under the specific cutting conditions of feed rate = 0.066 mm/rev, cutting speed = 120 m/min, and depth of cut = 0.1 mm; and feed rate = 0.105 mm/rev, cutting speed = 120 m/min, and depth of cut = 0.2 mm, the observed tool damage was small. Similar chip shape was observed (Expt. No. 1, 3, 7). Workpiece damage was observed (Expt. No. 3, 5, 7, 9).

• Journal of the Korean Ceramic Society
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• v.28 no.11
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• pp.917-925
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• 1991

For the present experiment five Portland cement mortars are in order: mortars with two different water/ cement ratios (W/C=0.45 and 0.50, each having no chemical additive), and those with an additive such as superplasticizer, air-entraining agent or water-repelling agent. We fix the W/C ratio of mortars having additive so that their pastes can yield the same workability as that of the cement mortar of W/C=0.50 with no additive. It is shown that the freeze-thaw resistivity depends heavily on the characteristic of wide pores. Despite a good deal of wide pores, the air-entrained specimen shows a good freeze-thaw resistivity due to appropriate air-pores. And also the specimen with water-repelling agent, which proves to cause the microstructure to become hydrophobic, make good resistance to freeze-thaw cycles in spite of its high wide-porosity. Our suggestion is that the freeze-thaw durability of Portland cement mortar/concrete can be more effectively enhanced by using air-entraining agent or water-repelling agent, and simutaneously by taking proper measures against foaming and/or the increased tendency of wide-pore building due to additive.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.12
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• pp.1173-1183
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• 2009

In order to reduce the download around the Smart UAV(SUAV) at hovering, flow control using synthetic jet has been performed. Many of the complex tilt rotor flow features are captured including the leading and trailing edge separation, and the large region of separated flow beneath the wing. In order to control the leading edge and trailing edge separation, synthetic jet is located at 0.01c, $0.3c_{flap}$, $0.95c_{flap}$. As non-dimensional frequency, the flow pattern is altered and the rate of drag reduction is changed. The results show that synthetic jets shorten the vortex period and decrease the vortex size by changing local flow structure. By using leading edge jet and trailing edge jet, download is efficiently reduced compared to no control case at hovering mode.

• Applied Biological Chemistry
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• v.37 no.2
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• pp.94-99
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• 1994

Bran structure and water uptake rate for brown rices of thirteen japonica and twelve Tongil cultivars were investigated. The japonica type was shorter in length and had lower value in the ratio of length to width than Tongil one. No differences were observed in width and weight between the two types. The number of aleurone layer and the thickness of bran layer were higher in dorsal side than in ventral side in all rice cultivars. The structure in ventral side was similar but the number of aleurone layer in dosal side was higher in japonica samples. There were no significant differences in water uptake rates showed no correlation with the bran structure.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2007.04a
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• pp.84-85
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• 2007

3,3-Dimethyl-1-butene (C6H12) monomer를 이용하여 RF power와 압력에 따라 막을 증착하였다. 증착된 비정질 탄소막은 power/pressure (W/Torr)가 증가할수록 Raman 스펙트럼에서 D peak가 증가하였고, ring 구조의 막을 형성하였다. 또한 ring 구조의 막이 형성됨으로써 hardness와 modulus는 각각 12 GPa과 85 GPa로 선형적으로 증가하는 것으로 나타났다.

• Journal of the Korean Chemical Society
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• v.42 no.3
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• pp.315-322
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• 1998

A series of new dimesogenic compounds were prepared and their thermotropic and liquid crystalline properties were studied by differential scanning calorimetry and on a hot-stage of a polarizing microscope. These compounds, 1,10-bis[2,5-bis(4-substitutedphenoxycarbonyl)phenoxy]decanes, consist of two bis(ρ-substitutedphenoxy)terephthalate units interconnected through a oxydecamethyleneoxy spacer on the central terephthaloyl units resulting in the structure of "H-shaped" dimeric twin compounds. The terminal substitutent groups were changed; X=-F, -H, -I, -Cl, -Br, $-NO_2,\;-CF_3,\;-OC_4H_9,\;-CN\;and\;-C_6H_5.$ The compounds with X=$-OC_4H_9,\;-CN\;and\;-C_6H_5$ were monotropically nematic. In contrast, the compounds with $X=-F, -H, -I, -Cl, -Br, $-NO_2\;and\;-CF_3$ were non-liquid crystals. The nematic group efficiency of these compounds was in the order of -C_6H_5>-CN>-OC_4H_9.$

• Journal of the Korean Chemical Society
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• v.39 no.6
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• pp.434-439
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• 1995

Six-coordinate molybdenum(Ⅴ)-oxo complexes, (R4N)[MoO(NCS)2L](R=CH3, C2H5, n-C4, H9) with S-methyl-3-(2-hydroxy-x-phenyl)methylenedithiocarbazate(L1: x=5-H) and its derivatives (L2:x=5-CH3, L3: x=3-CH3O, L4: x=5,6-C4H4 and L5: x=5-NO2) have been synthesized and the structural, spectral and electrochemical properties of the complexes have been characterized by elemental analysis, molar conductivity, UV-Vis, IR, 1H NMR, and CV (cyclic voltammetry).