• Title/Summary/Keyword: Nitrogen storage

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Development of a Cost-Effective 20K Hydrogen BET Measurement for Nanoporous Materials (나노다공체 물성 측정을 위한 극저온(20K) 수소 BET 개발 및 응용)

  • Park, Jaewoo;Oh, Hyunchul
    • Korean Journal of Materials Research
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    • v.27 no.9
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    • pp.466-470
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    • 2017
  • With the matters of climate change, energy security and resource depletion, a growing pressure exists to search for replacements for fossil fuels. Among various sustainable energy sources, hydrogen is thought of as a clean energy, and thus efficient hydrogen storage is a major issue. In order to realize efficient and safe hydrogen storage, various porous materials are being explored as solid-states materials for hydrogen storage. For those purposes, it is a prerequisite to characterize a material's textural properties to evaluate its hydrogen storage performance. In general, the textural properties of porous materials are analyzed by the Brunauer-Emmett-Teller (BET) measurement using nitrogen gas as a probe molecule. However, nitrogen BET analysis is sometimes not suitable for materials possessing small pores and surfaces with high curvatures like MOFs because the nitrogen molecule may sometimes be too large to reach the entire porous framework, resulting in an erroneous value. Hence, a smaller probe molecule for BET measurements (such as hydrogen) may be required. In this study, we describe a cost-effective novel cryostat for BET measurement that can reach temperatures below the liquefaction of hydrogen gas. Temperature and cold volume of the cryostat are corrected, and all measurements are validated using a commercial device. In this way, direct observation of the hydrogen adsorption properties is possible, which can translate directly into the determination of textural properties.

Effects of Gamma Irradiation on Inhibition of Urease Activity and Fishy Smell in Mackerel (Scomber japonicus) during Refrigerated Storage

  • Jeong, So-Mi;Kim, Han-Ho;Ryu, Si-Hyeong;Kang, Woo-Sin;Lee, Ji-Eun;Kim, Su-Ryong;Lee, Ga-Hye;Xu, Xiaotong;Byun, Eui-baek;Ahn, Dong-Hyun
    • Journal of Microbiology and Biotechnology
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    • v.32 no.6
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    • pp.808-815
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    • 2022
  • In this study, gamma-irradiated mackerel (Scomber japonicus) meat was stored in a refrigerator for 20 days to examine the physicochemical changes related to fishy smell. The effect of gamma irradiation on the inhibition of the activity of crude urease extracted from Vibrio parahaemolyticus was also evaluated. Increased levels of trimethylamine (TMA) and volatile basic nitrogen (VBN) content, which are the main components causing fishy smell, were significantly reduced by day 20 of storage after gamma irradiation, indicating that freshness was maintained during storage. The ammonia nitrogen contents of 3, 7, 10, and 20 kGy gamma-irradiated groups were significantly decreased by 6.5, 15.2, 17.4, and 23.9%, respectively, compared to non-irradiated groups on day 20 of storage. In addition, urease activity decreased in a gamma irradiation intensity-dependent manner. Volatile organic compounds (VOCs) were measured during the storage of gamma-irradiated mackerel meat. The contents of ethanol, 2-butanone, 3-methylbutanal, and trans-2-pentenal, which are known to cause off-flavors due to spoilage of fish, were significantly reduced by day 20 of storage. Therefore, gamma irradiation can be considered useful for inhibiting urease activity and reducing fishy smell during fish storage.

Physicochemical Changes of Wanja-jeon during Cold Storage for Hospital Cook/Chill Foodservice System (병원의 냉장저장급식제도를 위해 조리된 완자전의 냉장저장 중 이화학적 성분변화)

  • 임양이;김혜영;강태수
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.26 no.6
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    • pp.1221-1227
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    • 1997
  • To measure nutritional components and physical quality of Wanja-jeon(Korean pan fried meat balls)was investigated during storage in a simulated hospital cook/chill foodservice system. The Wanja-jeon was cooked and stored for 4 weeks in chill conditions of 2 and 7$^{\circ}C$ and then reheated in the microwave oven. Moisture, protein, and fat contents were decreased little during 4 weeks storage at 2 and 7$^{\circ}C$. Total unsaturated fatty acids(TUFA) and polyunsaturated fatty acids(PUFA) increased slightly at 7$^{\circ}C$ storage. Total free amino acid contents were reduced after 4 weeks of storage, while total amino acids were affected little during chilled storage. However, volatile basic nitrogen(VBN) increased during the 4 weeks storage from 11.2mg%, immediately after cooking, to 14.1~14.2mg%. After reheating, thiobarbituric acid(TBA) value increased more significantly to 0.19 and 0.20.

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Removal Effect of Nitrogen and Phosphorus of Acorus cazamus var. angustatus oil Its Growth Stage and Water-storage Time (생장단계와 체류시간에 따른 창포의 질소와 인 제거효과)

  • Seo Byung-Soo;Park Chong-Min
    • Korean Journal of Environment and Ecology
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    • v.19 no.1
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    • pp.1-8
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    • 2005
  • The removal affect of nitrogen and phosphorus were analyzed using a Acorus calamus var. angustatus. The nutrient concentration, growth stage of plants and the storage time of polluted water were considered. The results of this study were as follows: after an hour the content of nitrogen and phosphorus were considerably reduced in the Acorus calamus var. angustatus, while after two-four hours the rate of reduction was extremely low. This situation was the same in the early growth stage, growing stage and highest growth stage of the plant. The removal rate of nitrogen and phosphorus with the Acorus calamus var. angustatus was higher, when these two minerals remained in high levels of water. The Acorus calamus var. angustatus was more effective to remove nitrogen than that of phosphorus. The plant removed the most nitrogen and phosphorus when in the highest growth stage, but this was not clear in the growth stages. The removal rate was higher, in the case of moving polluted water to other plants after two days, than in the case of four days of growth in the same plants.

Preservation of Toxoplasma gondii (RH strain) in liquid nitrogen for 5 years (톡소플라즈마원충(原蟲)(RH주(株))의 5년간 동결보존시험)

  • Jeon, Yeong;Jang, Hwan
    • Korean Journal of Veterinary Research
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    • v.33 no.2
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    • pp.285-287
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    • 1993
  • Toxoplasma gondii frozen by the method of very slow cooling ($-30^{\circ}C/3hrs.{\rightarrow}\;-60^{\circ}C/lhr.{\rightarrow}\;-196^{\circ}C$ of liquid nitrogen)were inoculated mice after storage in the liquid nitrogen for 5 years. The results obtained were as follows; 1. Toxoplasma gondii was detected in mice 4~5th day after intraperitoneal inoculation of organisms stored in the liquid nitrogen once a year for 5 years. 2. Toxoplasma gondii could be preserved longer than 5 years in liquid nitorgen being evidenced by the in vivo test.

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A Study on the storage of Ginseng Powder by r-Irradiation (방사선조사에 의한 인삼분말의 저장성에 관한 연구)

  • 민옥녀
    • Journal of Environmental Health Sciences
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    • v.8 no.1
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    • pp.45-53
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    • 1982
  • To determine the effect of r-irradiation on the microorganisms destruction and the changes of general constituents of Ginseng Powder, three samples were analyzed at 1st and 3rd month after r-irradiation. The results were as follows: 1. Total bacterial counts were decreased during storage as the irradiation dose increased. It seems that about 300 Krad was satisfactory to the regulation of ginseng powder. ($5.0 \times 10^4 /g$) 2. Coliform group was also decreased during storage as the irradiation dose increased. Coliform group was not detected at the irradiation dose higher than 500 Krad. 3. Total bacterial counts and coilform group were in proportion to the content of moisture in ginseng powder. 4. The contents of moisture, ash, crude protein, crude lipid and total sugar in ginseng powder during storage had nearly no changes. 5. The content of reducing sugar in ginseng powder during storage had the increasing tendencies as the irradiation dose increased. 6. The content of amino-nitrogen in ginseng powder during storage had the decreasing tendencies as the irradiation does increased.

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Changes in the Quality of Pork Organ during Frozen Storage (돈 내장육의 냉동저장에 따른 품질변화)

  • 양재영
    • The Korean Journal of Food And Nutrition
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    • v.2 no.1
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    • pp.12-17
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    • 1989
  • This experiment was carried out to investigate the changes in quality of pork organs such as the meat of large intestine, small intestine and liver during frozen storage at -18$\pm$1$^{\circ}C$. The result obtained were as follows ; 1 The moisture contents in the meat of large intestine, small intestine and liver was 61.1%, 65.1% and 71.3% and the content of crude fat was 27.1%, 21.5% and 5.0% respectively, 2. Weight loss increased In the course of storage period, and liver showed the least weight loss in them. 3. Total lipid in the meat of large intestine, small intestine and liver was 24.4%, 19.2% and 4.3% respectively, and which decreased gradually in the course of storage period. 4. The content of volatile basic nitrogen in raw meat was 20 mg% within and without before storage treatment, and that of the value was 24.2 mg% within after 3 weeks storage.

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Quality changes of salted and semi-dried mackerel fillets by UV treatment during refrigerated storage (자외선 처리가 반염건 고등어 필레의 냉장저장중 품질변화에 미치는 영향)

  • Song, Hyo-Nam;Lee, Dae-Gyu;Han, Sung-Wook;Yoon, Hye-Kyung;Hwang, In-Kyeong
    • Korean journal of food and cookery science
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    • v.21 no.5
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    • pp.662-668
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    • 2005
  • To investigate the quality retention method of salted and semi-dried mackerel fillets, pH, volatile basic nitrogen (VBN), trimethylamine (TMA) and total bacterial counts in the fillets that were UV treated for 1, 3, and 4 hr were periodically measured during 48 days of refrigerated storage. The moisture, crude protein, crude lipid, and ash contents were 45.46 %, 18.87 %, 33.75 %, and 2.99 %, respectively. The freshness as determined by pH measurement could be maintained up to 25 days for the control and 31 days for the UV-treated fillets. VBN contents were continually increased over the storage time. The control reached the initial putrid level after 21 days while the UV-treated fillets after $25{\sim}31$ days. A similar tendency was shown for the changes of trimethylamine TMA contents, although the period differed slightly and the increase of the UV treatment time could decrease the TMA contents. The changes on the total bacterial counts of the fillets were maintained under 105 CFU/g during 48days. Especially, due to the effective decrease of the microorganism count by UV treatment at the beginning of the storage, UV -treated fillets showed lower bacterial counts than control over the whole period. E. coli. and Listeria were not detected in any fillets. Combining the above data and the sensory changes, the storage period of the fillets could be prolonged from 15 days at present to 30 days by UV treatments.

Effect of Lotus (Nelumbo nucifera) Leaf Powder on the Quality Characteristics of Chicken Patties in Refrigerated Storage

  • Choi, Yun-Sang;Choi, Ji-Hun;Kim, Hack-Youn;Kim, Hyun-Wook;Lee, Mi-Ai;Chung, Hai-Jung;Lee, Sung-Ki;Kim, Cheon-Jei
    • Food Science of Animal Resources
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    • v.31 no.1
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    • pp.9-18
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    • 2011
  • This study was aimed at comparing the pH, color, thiobarbituric acid (TBA), volatile basic nitrogen (VBN), textural properties, and sensory evaluations of chicken meat patties containing lotus (Nelumbo nucifera) leaf powder, and assessing their shelf-life at refrigeration temperature ($4{\pm}1^{\circ}C$). In the refrigerated storage, the pH, lightness, yellowness, springiness values, and sensory properties scores of the control as well as all the treated samples decreased as the storage increased. The hardness, gumminess, chewiness, TBA, and VBN-values of control and all the samples treated with lotus leaf increased during refrigerated storage. At the end of the storage period (day 28), chicken patties containing lotus leaf powder had lower pH, redness, yellowness, TBA, VBN, hardness, gumminess, and chewiness values than those of control. The results of this study showed that a lotus leaf powder can increase storage stability in chicken meat products.

Preparation and Storage Conditions of Oleoresin from Root Portion of Peeled Garlic (박피마늘 뿌리부분을 이용한 Oleoresin의 제조 및 저장조건)

  • Kim, Sang-Kyun;Cha, Bo-Sook;Kim, Woo-Jung
    • Korean Journal of Food Science and Technology
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    • v.30 no.6
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    • pp.1321-1326
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    • 1998
  • Extraction and storage conditions of oleoresin were studied from root portion of peeled garlic, an waste of garlic industry. Extraction with ethanol and methanol showed an high solid yields of $27{\sim}37%$ at the temperature range of $30{\sim}50^{\circ}C$. Two hours of extraction were found to be economic because of no significant increase in furthur extraction. Storage of the oleoresin under anaerobic condition such as vaccum or nitrogen resulted in a less changes in pH, total acidity, color and thiosulfinate content, than those changes under aerobic condition. Most of the thiosulfinate was decreased for all conditions after 14 days of storage at $25^{\circ}C$. Glucose and sucrose were increased and most of organic acids were decreased during storage under nitrogen condition. Addition of ascorbic acid and cysteine into oleoresin retained the garlic flavor, effectively.

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