• Title/Summary/Keyword: Nitrogen atmosphere

Search Result 542, Processing Time 0.033 seconds

Annealing Effects on Ultra thin MOS Capacitors

  • Ng, Alvin Chi-hai;Xu, Jun;Xu, J.B.;Cheung, W.Y.
    • Electrical & Electronic Materials
    • /
    • v.16 no.9
    • /
    • pp.62.1-62
    • /
    • 2003
  • Silicon oxide with thickness lee than 9 nm is fabricated by tube furnace oxidation. Nitrogen is added to dilute the oxidation rate. Aluminum dots with radius of 0.05 cm are deposited on the oixde. High frequency capacitance-voltage(HF C-V), conductance-voltage(G-V) and current-voltage(I-V) characteristics are measured. Annealing under nitrogen atmosphere is carried out with different time and at different temperature. Densities of the interface states before and after annealing are compared. After annealing, a decrease in density of the interface states is found. Experiments show that 45$0^{\circ}C$ annealing for 30 minutes has the lowest density of the interface states.

  • PDF

Influence of Ambient Gas Composition on the Microstructure of Plasma Nitrocarburised SCM435 steel (플라즈마 질탄화처리된 SCM435강의 미세조직에 미치는 가스 조성의 영향)

  • Lee, In-Seop
    • Korean Journal of Materials Research
    • /
    • v.12 no.6
    • /
    • pp.427-430
    • /
    • 2002
  • Plasma nitrocarburizing treatment was performed for SCM 435 steel by using a plasma ion nitriding system. The effects of the variation of nitrogen and methan contents upon the hardened layer was investigated. Both the thickness of the compound layer and the amount of $\varepsilon$ phase in the compound layer increased with increasing nitrogen content. However, the thickness of the compound layer decreased due to unstable plasma for an atmosphere containing 90% $N_2$ gas content in the gas mixture. The amount of $\varepsilon$phase in the compound layer increased with increasing $CH_4$ gas content. For $CH_4$ gas content more than 2% in the gas mixture, the thickness of the compound layer decreased due to the formation of $\theta$ phase.

Effect of Carbon-Restoration on Mechanical Properties of Automobile Safety Parts (자동차용 안전부품의 기계적 성질에 미치는 복탄처리의 영향)

  • Kim, M.G.;Jung, B.H.;Jung, S.H.;Lee, B.C.;Kim, S.S.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.16 no.1
    • /
    • pp.26-31
    • /
    • 2003
  • Decarburized zone of metal tongue which is used in seat belt for automobiles was carbon-restoration quenched and tempered using nitrogen-methanol gaseous atmosphere. The effects of microstructure and mechanical properties of metal tongue on the effectiveness of carbon-restoration during tempering was studied. Metal tongue showed $20{\sim}30{\mu}m$ decarburized zone. However, after carbon-restoration, it has uniform microstructure and thus hardness without decarburized zone. Carbon-restoration quenching and tempering process resulted in better wear and corrosion resistances than quenching and tempering process.

Characterization of Shape Memory Alloy Springs by Beat Treatment Condition (열처리 조건에 따른 형상기억합금 스프링의 특성변화)

  • Kim, Myung-Soon;Na, Seung-Woo;Lee, Sang-Hoon;Lee, Seung-Ki
    • Proceedings of the KIEE Conference
    • /
    • 1996.07c
    • /
    • pp.1985-1987
    • /
    • 1996
  • Shape memory alloy springs have been fabricated and annealed at $400^{\circ}C$, $450^{\circ}C$ and $500^{\circ}C$ in atmosphere and in nitrogen gas. The optimal heat treatment condition in view of maximum generated force has been decided by the iso-thermal test with variation of annealing condition. Experimental results show that the heat treatment with high temperature in nitrogen gas is desirable for high generated force and can be used for the design of shape memory alloy springs.

  • PDF

Characteristic of Tantalum Nitride Thin-films for High Precision Resistors (고정밀 저항용 질화탄탈 박막의 특성)

  • Choi, Sung-Kyu;Na, Kyung-Il;Nam, Hyo-Duk;Chung, Gwiy-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2001.11b
    • /
    • pp.537-540
    • /
    • 2001
  • This paper presents the characteristics of Ta-N thin-film for high precision resistors, which were deposited on Si substrate by DC reactive magnetron sputtering in an argon-nitrogen atmosphere(Ar-(4~16 %)$N_2$). Structural properties studied using X-ray diffraction(XRD) indicate the presence of TaN, $Ta_3N_5$ or a mixture of Ta-N phases in the films depending on the amount of nitrogen in the sputtering gas. The chemical composition are investigated by auger electro spectroscopy(AES). The optimized conditions of Ta-N thin-film resistors were deposited in 4 % $N_2$ gas flow ratio. Under optimum conditions, the Ta-N thin-film resistors are obtained a high resistivity, $\rho=305.7{\mu}{\Omega}cm$, a low temperature coefficient of resistance, TCR=-36 $ppm/^{\circ}C$.

  • PDF

Photovoltaic Properties of Sintered CdS/CdTe Solar Cell (소결체 ITO/CdS/CdTe 태양전지의 광전압특성)

  • 김동섭;조은철;안병태;임호빈
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1994.11a
    • /
    • pp.216-220
    • /
    • 1994
  • Polycrystalline CdS films have been prepared by coating a slurry, which consisted of CdS, 11w% CdCl$_2$ and appropriate amount of propylene glycol, on glass substrate and glass substrate coated with indium tin oxide(ITO) followed by sintering in a nitrogen atmosphere. CdTe slurries consisting of Te powder and Cd powder were coated on the sintered CdS films and ITO/CdS films and were sintered in nitrogen to prepare sintered CdS/CdTe and ITO/CdS/CdTe solar cells. The value of fill factor increased due to low series resistance and open circuit voltage decreased due to low shunt resistance in the ITO/CdS/CdTe solar cells.

The Oxidation of Kovar(Fe-29Ni-17Co) in Humidified nitrogen (가습된 질소 분위기에서의 Kovar(Fe-29Ni-17Co)산화)

  • 김병수;김민호;김상우;최덕균;손용배
    • Journal of the Korean Ceramic Society
    • /
    • v.36 no.11
    • /
    • pp.1228-1234
    • /
    • 1999
  • In order to form a uniform oxidation layer and spinel crystalline phase that was supposed to help strong bonding in Kovar(Fe-29Ni-17Co)to-glass sealing the humidified nitrogen (2.3%H2O/N2) was used as an oxidation atmosphere. Kovar oxidation was diffusion-contolled and the activation energy was 2.51 kcal/mol at 600-900$^{\circ}C$ After oxidation at 600$^{\circ}C$ the oxidation layer was under 1$\mu\textrm{m}$ thickness and crystalline phase was spinel which was found to be suitable for the Kovar-to-glass sealing.

  • PDF

The effect of shielding gases on the characteristics of super duplex weld metal (슈퍼 듀플렉스 용접부에 미치는 보호가스의 영향)

  • Hong, In-Pyo;Lee, Cheol-Hwan;Kim, Yu-Gi;Kim, Dae-Sun
    • Proceedings of the KWS Conference
    • /
    • 2005.06a
    • /
    • pp.209-211
    • /
    • 2005
  • Super duplex stainless steels have been used for offshore oil and gas piping systems which are subject to corrosion atmosphere, because they have excellent resistance to Stress Corrosion Cracking (SCC) and Pitting corrosion and high strength/weight ratio. Normally, the welding for duplex stainless steels has been peformed using GTAW with Ar shielding gas. However, in case of using Ar as shielding gas, the corrosion resistance at root weld metal will be deteriorated due to loss of nitrogen from weld deposit during welding. It is wellknown that the corrosion resistance of super duplex stainless can be restored by addition of nitrogen as shielding gas. In this study, we made super duplex welding with using several kinds of shielding and purging gases and investigated the relationship between shielding gas and corrosion resistance. Consequently, it was shown that corrosion resistance of weld deposit can be restored by addition of $N_{2}$ as shielding gas.

  • PDF

Detection of Low Cycle Fatigue in Type 316 Stainless Steel using HTS-SQUID

  • Park, D.G.;Kim, D.W.;Timofeev, V.P.;Hong, J.H.
    • Corrosion Science and Technology
    • /
    • v.3 no.5
    • /
    • pp.222-225
    • /
    • 2004
  • A portable RF HTS SQUID-based susceptometer was applied to the measurement of fatigue behavior for type 316L(N) stainless steel containing 0.04% to 0.15% nitrogen content. Strain-controlled low cycle fatigue (LCF) tests were conducted at RT and $600^{\circ}C$ in air an atmosphere, and the magnetic moments were measured after the fatigue test using HTS SQUID. The magnetic moment of an as-received sample is higher than that of a fatigued sample in all the temperature ranges irrespective of the nitrogen content. The fatigue life decreased with an increasing test temperature up to $500^{\circ}C$, but increased at $600^{\circ}C$. The change of the magnetic moments by LCF test is attributed to the stress induced micro defects.

Numerical study on Comparison of Self-Pressurization Behavior of Liquid Nitrogen Cryostat for Umbilical Cord Blood Storage System Design

  • Mahfud, M.I.;Phil, K.E.
    • 한국태양에너지학회:학술대회논문집
    • /
    • 2009.11a
    • /
    • pp.409-414
    • /
    • 2009
  • Since cryogens are stored at very low temperatures, the cryogenic storage systems are quite sensitive to heat leaks. Even though the vessel operated under sealed condition with vacuum insulation and reflective coatings are used, the heat leakage into the vessel is still unavoidable. Therefore, this paper concerns with numerical study of self-pressurization used to analysis the optimum design with the variation volume fraction, effect of heat flux and storage pressure of liquid nitrogen. The result shows that as the volume fraction increases, the pressure rise reduces and the relatively at atmosphere pressure is better than the higher one. In addition, higher heat flux leads the pressure rise increases faster than low one. The additional of heat pipe system to reduce the pressure rise rate also has been done. By this comparison, the optimum design for storage umbilical cord blood can be selected.

  • PDF