• Journal of the Korean Society of Tobacco Science
• /
• v.3 no.1
• /
• pp.20-24
• /
• 1981

This experiment was carried out to determine the relationships between maturity and content of the chemical components in flue-cured tobacco. The results were as follows : 1) Among the chemical components, the contents of total nitrogen, ammonia nitrogen, total alkaloids, nicotine, total volatile base, petroleum-ether extract, crude fiber, crude ash, water soluble ash, and chlorine decreased significantly, and those of total sugar, reducing sugar, and starch increased as leaf maturity progressed until the stage of ripeness, but, afterwards, a reverse tendency appeared. 2) There was a significant relationship between maturity and the contents of chemical components, such as total nitrogen, protein nitrogen, ammonia nitrogen, total volatile base, and the correlation coefficients of them were -0.743, -0.789, -0.797, and -0.642, respectively.

• Analytical Science and Technology
• /
• v.35 no.6
• /
• pp.249-255
• /
• 2022

In this study, a new method for the analysis of high-purity nitrogen was developed. A gas chromatography-flame ionization detector (GC-FID) was used for purity analysis. Certified reference materials (CRMs) at a level of 3 µmol/mol of carbon monoxide (CO), carbon dioxide (CO₂), and methane (CH₄), which may exist in high-purity nitrogen, were prepared using the gravimetric method, and these CRMs were used for purity analysis. In this new method, ultra-high-purity and high-purity nitrogen were used as carrier gases. The impurities in high-purity nitrogen were quantitatively analyzed by comparing the differences in the area values of the GC chromatograms of the prepared CRMs. We purchased liquid nitrogen and three bottles of nitrogen gas, which were produced by three different manufacturers, using high-purity nitrogen. Furthermore, to validate the developed purity analysis method, the fraction of impurities in high-purity nitrogen was compared with the results of the typical purity analysis method. The comparison results were consistent within the expanded uncertainties (k = 2).

• Journal of Nutrition and Health
• /
• v.12 no.4
• /
• pp.25-27
• /
• 1979

The analysis of nail nitrogen content reflected recent nutritional status. Therefore, estimation of nail nitrogen content has been previously reported in a small group of neonates ana school children. Nail samples were obtained from 52 economically middle and 21 low classes. The contents of nitrogen in their fingernails were determinded by micro-Kjeldahl method. Mean nail nitrogen content was $133.1{\pm}8mg/g$ in the middle class which is significantly higher than that of the low class $122.1{\pm}8mg/g$. The nitrogen contents of nails obtained in summer were found by analysis of variance and student's t-test to he lower than those obtained in winter.

• Progress in Superconductivity and Cryogenics
• /
• v.3 no.2
• /
• pp.77-83
• /
• 2001

The thermal characteristics of solid nitrogen are investigated by experiment and analysis for the purpose of evaluating its feasibility as a cooling medium for HTS (high T$_{c}$ superconductor) magnets. A cryostat to refrigerate a liquid-nitrogen container well below its freezing temperature with a 2-stage GM cryocooler is designed and constructed. The spatial distribution of temperature is measure as a function of time during the freezing and melting processes. from which the thermal diffusivity of solid nitrogen can be approximately calculated. the freezing process is formulated and solved by the integral method with an assumption of phase equilibrium at the solid-liquid interface and experimental observation. It may be concluded that the thermal diffusion in solid phase is much slower than in liquid and the degree of super-saturation is quite severe in the solidification of nitrogen.n.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
• /
• v.12 no.9
• /
• pp.825-834
• /
• 2000

A heat exchanger analysis is performed to investigate the heating characteristics of cryogenic nitrogen by ambient air for the purpose of cryogenic automotive propulsion. The heat exchanger is a concentric triple-passage for supercritical nitrogen, and the radial fins are attached on the outermost tube for the crossflow of ambient air. The temperature distribution is calculated for the nitrogen along the passage, including the real gas properties of nitrogen, the fluid convections and the conductions through the tube walls and the fins. Since the wall temperature of the outer (ambient side) tube is very low in most cases, a heavy frost can be formed on the surface, affecting the heat exchange performance. By the method of the similarity between the heat and the mass transfer of moist air, the frost growth and the time-dependent effectiveness of the heat exchanger are calculated for various operating conditions. It is concluded that the frost formation can augment the heating of nitrogen during the initial period because of the latent heat, then gradually degrades the heat exchange because of the increased thermal resistance. Practical design issues are discussed for the flow rate of nitrogen, the velocity and humidity of ambient air, and the sizes of the fin.

• Journal of the Korean Ceramic Society
• /
• v.56 no.4
• /
• pp.374-386
• /
• 2019

A process for nitrogen doping of TiO₂ ceramics was developed, whereby polycrystalline titania particles were prepared at 450-1000℃ with variation of the firing schedule under N₂ atmosphere. The effect of nitrogen doping on the polycrystallites was investigated by X-ray diffraction (XRD) and Raman analysis. The microstructure of the TiO₂ ceramics changed with variation of the firing temperature and the firing atmosphere (N₂ or O₂). The microstructural changes in the nitrogen-doped TiO₂ ceramics were closely related to changes in the Raman spectra. Within the evaluated temperature range, the nitrogen-doped titania ceramics comprised anatase and/or rutile phases, similar to those of titania ceramics fired in air. Infiltration of nitrogen gas into the titania ceramics was analyzed by Raman spectroscopy and XRD analysis, showing a considerable change in the profiles of the N₂-doped TiO₂ ceramics compared with those of the TiO₂ ceramics fired under O₂ atmosphere. The nitrogen doping in the anatase phase may produce active sites for photocatalysis in the visible and ultraviolet regions.

• Journal of Biosystems Engineering
• /
• v.35 no.2
• /
• pp.132-137
• /
• 2010

Site-specific N application for corn is one of the precision crop management. To implement the site-specific N application, various nitrogen stress sensing methods, including aerial image, tissue analysis, soil sampling analysis, and SPAD meter readings, have been used. Use of side-dressing, an efficient nitrogen application method than a uniform application in either late fall or early spring, relies mainly on the capability of nitrogen deficiency detection. This paper presents map-based variable rate nitrogen application based using a multi-spectral corn nitrogen deficiency(CND) sensor. This sensor assess the nitrogen stress by means of the estimated SPAD reading calculated from the corn leave reflectance. The estimated SPAD value from the CND sensor system and location information form DGPS of each field block was combined into the field map using a ArcView program. Then this map was converted into a raster file for a map-based variable rate application software. The relative SPAD (RSPAD = SPAD over reference SPAD) was investigated 2 weeks after the treatments. The results showed that the map-based variable rate application system was feasible.

• Journal of Microbiology and Biotechnology
• /
• v.22 no.6
• /
• pp.780-787
• /
• 2012

The maize pathogen Gibberella moniliformis produces fumonisins, a group of mycotoxins associated with several disorders in animals and humans, including cancer. The current focus of our research is to understand the regulatory mechanisms involved in fumonisin biosynthesis. In this study, we employed a proteomics approach to identify novel genes involved in the fumonisin biosynthesis under nitrogen stress. The combination of genome sequence, mutant strains, EST database, microarrays, and proteomics offers an opportunity to advance our understanding of this process. We investigated the response of the G. moniliformis proteome in limited nitrogen (N0, fumonisin-inducing) and excess nitrogen (N+, fumonisin-repressing) conditions by one- and two-dimensional electrophoresis. We selected 11 differentially expressed proteins, six from limited nitrogen conditions and five from excess nitrogen conditions, and determined the sequences by peptide mass fingerprinting and MS/MS spectrophotometry. Subsequently, we identified the EST sequences corresponding to the proteins and studied their expression profiles in different culture conditions. Through the comparative analysis of gene and protein expression data, we identified three candidate genes for functional analysis and our results provided valuable clues regarding the regulatory mechanisms of fumonisin biosynthesis.

• Journal of the Korean Society of Food Science and Nutrition
• /
• v.29 no.5
• /
• pp.965-967
• /
• 2000

An on-line FIA system in place of traditional Conway method was used for quicker and simpler analysis of volatile basic nitrogen of pork. The on-line system was developed by connecting an FIA apparatus with an ammonia electrode as a detector to a personal computer. The data from Conway method and from the on-line FIA system were in good agreement and the correlation coefficient was 0.981. One sample could be analyzed in about 4 min.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
• /
• v.30 no.1
• /
• pp.24-32
• /
• 2018

In this paper, analytical studies were conducted to obtain optimal design factors and analysis parameters of liquid nitrogen cooling exchanger applied in cryogenic refrigerator. The target value of heat transfer rate was more than 1 kW and pressure drop was less than 40 kPa. Design factors of cryogenic heat exchanger included width of channel and configuration of paths. Analytical factors of liquid nitrogen cooling exchanger included temperatures of coolant header surface and inlet liquid nitrogen. The width and number of channels in the design parameters were 0.0050~0.0150 m and 4~8, respectively. The configuration of channel path was 4 ways. Temperatures of coolant header surface and inlet liquid nitrogen in analytical parameters were 74 to 78K and 82 to 86K, respectively. As result, the design factor and analysis parameter satisfying the target values were obtained. The biggest heat transfer rate was 1.36 kW with pressure drop of 32.26 kPa.