• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1995.05a
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• pp.204-207
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• 1995

This paper deals with the dielectric characteristics of $SF_{6}$ gas stressed by non-oscillating and oscillating impulse voltages in inhomogeneous field perturbed by a fixed needle shaped-protrusion. The breakdown voltage-time characteristics were measured for both polarities and over the gas pressure range from 0.1 to 0.5 [MPa], and the temporal developments of the prebreakdown were observed. The dependence of the leader stepping time on the gas pressure were obtained.

• Journal of the Korean Ceramic Society
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• v.30 no.3
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• pp.215-221
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• 1993

The Hydroxyapatite powders were prepared by Wet-direct and Hydrothermal synthesis using Ca(NO3)2.4H2O and (NH4)2.HPO4.Stoichiometric and good cristalline HAp powders were obtained 9$0^{\circ}C$ by wet-direct process. The aspect ratio of HAp powders prepared by hydrothermal synthesis was increased with increasing synthetic temperature. The HAp particles obtained at 20$0^{\circ}C$ for 10hr were needle shaped ultra fine crystals, about 100nm in size. Small amount of TCP was obtained above 80$0^{\circ}C$ after heat-treatment of hydrothermally synthesized HAp but good crystalline HAp phase was maintained up to 120$0^{\circ}C$ as the primary phase.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.9 no.1
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• pp.24-29
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• 2000

This paper is experimental study of machining characteristics about martensitic heat resisting steel STR11. Machining characteristics are different according to internal quality(chemical compositions, microscopic structure and nonmetallic inclusion) mechanical properties(tensile strength value impact value and hardness) and dynamic cutting force. Following are the results : 1. In analyzing internal quality test materials have typical martensite structure and a minute needle-shaped structure. 2. Tensile strength and reduction of area and hardness are larger. But values of elongation and impact values are smaller. Fracture surface of tensile specimen is ductile. 3, Cutting force is decreasing with cutting speed increasing 4. Cutting force is increasing with feed speed increasing.

• Electrical & Electronic Materials
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• v.10 no.3
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• pp.247-254
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• 1997

Internal voids in insulators give rise to partial discharge, which causes a local breakdown and even entire insulation breakdown. Recently, the necessity of establishing the way to diagnose the aging of insulation materials and to predict of insulation breakdown become important. The purpose of our work are to investigate the treeing phenomena with an artificial needle shaped void by the charge of discharge and acoustic emission pulse in each phase angle area at the same time. We analyzed the .PHI.-QA-t pattern and .PHI.-AEA-t pattern using statistic operators such as pulse magnitude, pulse number, skewness, kurtosis. Therefore, the relation between the charge of discharge and acoustic emission pulse will be helpful to predict the breakdown just before the breakdown occur.

• Journal of the Korean Ceramic Society
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• v.53 no.2
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• pp.222-226
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• 2016

The synthesis of pure calcium carbonate nanocrystals was achieved using a simultaneous injection method to produce nano particles of uniform size. These were characterized using scanning electron microscopy and powder X-ray diffraction. The nano particles were needle-shaped aragonite polymorphs, approximately 100-200 nm in length. The aragonite polymorph of calcium carbonate was prepared using aqueous solutions of $CaCl_2$ and $Na_2CO_3$, which were injected simultaneously into double distilled water at $50^{\circ}C$ and then allowed to react for 1.5 h. The resulting whisker-type nano aragonite with high aspect ratio (30) is biocompatible and potentially suitable for applications in light weight plastics, as well as in the medical, pharmaceutical, cosmetic and paint industries.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1997.04a
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• pp.1073-1077
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• 1997

In this paper, we have studied internal quality including chemical compositions, microscopic structure and nonmetalic inclusion of test materials. We have analyzed machining characteristics including tensile strength value, impact value, hardness value etcs. Test materials are usd martensitic heat resisting steel, STR11 and STS420J2. The obtined results are as follows : 1. In analyzing internal quality, STR11 and STR420J2 have typical martensite structure and a minute needle-shaped structure. 2. Tensile strength and reduction of area and hardness value are large STR11 than STS420J2. But elongation impact are smaller STR11 than STS420J2. 3. Fracture surface of tensile speciman is ductile in STR11 and STS420J2.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.13 no.1
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• pp.52-59
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• 2000

In order to develop the transparent anti-static film with higher than 80% transparency to visible light, organic conductive compounds, N-methyl phenazinium 7,7,8,8-tetracyanoquinonedimethane (TCNQ) com-plex salts was synthesized and bar-coated on the polythylene terephthalate (PET) film using polymer binders. The best surface properties were obtained when acrylic binder was used. A single layer of TCNQ made of a acrylic binder showed a surface resistance of 10\ulcorner $\Omega$/ , a conductivity of 10\ulcorner S/cm, and a transparency of 75%. An optical microscopic examination revealed that the binder was first solidi-fied on the surface of PET film over which the needle-shaped TCNQ crystals were grown. An acrylic polyol coating over the TCNQ layer improved the transparency to 87%, becuase the acrylic polyol covers the surface of TCNQ crystals to reduce the surface roughness. This conductive material has thermal stability at room temperature and 4$0^{\circ}C$ over 4,000 h.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1996.05a
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• pp.137-141
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• 1996

This paper deals with the prebreakdown phenomena of $SF_{6}$ gap stressed by non-oscillating and oscillating impulse voltages in a strong inhomogeneous field disturbed by a fred needle shaped-protrusion on the earth-side electrode. The breakdown voltage-time characteristics were measured for both positive and negative polarities and over the gas pressure range of 0.1∼0.5 MPa, and the temporal developments of the 77breakdown were observed by a shunt of 50 n. The dependence of the leader stopping time on the gas pressure were obtained. The local field enhancement due to the space charges, which is produced by the streamer corona, has influence with the electrical breakdown of the test gap. The test streamer corona is oxy a necessary condition for the electrical breakdown and the subsequent ionization activities launch the leader at the local field region.

• Journal of the Korean Chemical Society
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• v.19 no.1
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• pp.34-37
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• 1975

3-Hydroxy-canthaxanthin, reddish purple needle shaped crystals, has been isolated from the abdominal skin of Bombina Orientalis. Its structure has been established by visible and IR spectral characteristics, chromatographic behaviors, and physical and chemical properties.

• Proceedings of the KIEE Conference
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• 2000.07c
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• pp.1999-2001
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• 2000

Impulse breakdown voltage characteristics of sulphur-hexafluoride/nitrogen ($SF_{6}-N_{2}$) mixtures were presented. The applied voltages were the positive and negative lightning impulse (1.2/44${\mu}s$) and oscillating impulse ($0.4{\mu}s$/2.08MHz) voltages. The predischarge current was observed to clarify the breakdown mechanism. The electrode system was consisted of plane to plane configuration with a needle-shaped protrusion whose length and diameter are 10mm and 1mm. The measurements were carried out at the gas pressure of mixtures up to 0.5MPa with nitrogen concentrations varying from 5 to 20%. The electrical breakdown in $SF_{6}-N_{2}$ mixtures develops with steplike pulses in leader mechanism. The minimum breakdown voltages for the negative lightning and oscillating impulse voltages were higher than those for the positive.