• 한국분말재료학회지
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• 제17권2호
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• pp.154-159
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• 2010

In this study, the sintering behavior of (Nd, Dy)-Fe-B powder which fabricated by strip-casting was investigated with various sintering temperatures and holding times. The relative density over 99% could be obtained by both sintering at $1070^{\circ}C$ for 1h and sintering at $970^{\circ}C$ for 20h. The grain growth was observed in sintered specimen at $1050^{\circ}C$ compared to one at $970^{\circ}C$. The isothermal sintering process below $1000^{\circ}C$ led to suppress grain growth showing the improved magnetic properties. The phase transformation of Nd-rich was confirmed by X-ray diffraction pattern.

• 한국분말재료학회지
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• 제16권4호
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• pp.285-290
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• 2009

HDDR treated anisotropic Nd-Fe-B powders have been widely used, due to their excellent magnetic properties, especially for sheet motors and sunroof motors of hybrid and electric vehicles. Final microstructure and coercivity of such Nd-Fe-B powders depend on the state of starting mother alloys, so additional homogenization treatment is required for improving magnetic properties of them. In this study, a homogenization treatment was performed at $900\sim1140^{\circ}C$ in order to control the grain size and Nd-rich phase distribution, and at the same time to improve coercivity of the HDDR treated magnetic powders. FE-SEM was used for observing grain size of the HDDR treated powder and EPMA was employed to observe distribution of Nd-rich phase. Magnetic properties were analyzed with a vibrating sample magnetometer.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1999년도 춘계학술대회논문집
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• pp.82-85
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• 1999

Permanent magnets of Nd-Fe-B group have kept a key post in the permanent magnet market and used in various parts. Tube Process is a process to produce permanent magnets using a deformable tube for denslfication of powder magnets. Advantage claimed for this process is that it can accomplish both densification and anisotropication in one step forming. In this paper. the simulation has been carried out for a full Tube Process in a closed Qe considering the compressibility of material, arbitrary curved shape and deformable body contact between Nd-Fe-B powder magnet and copper tube. The results show that the analysis of Tube Process is applicable with great help in the stage of preform design.

• Journal of Magnetics
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• 제22권2호
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• pp.250-256
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• 2017

The article presents the principle of a relatively small device that makes it possible to generate a strong magnetic field in an air gap without electrical energy consumption. It describes the implemented design of this device, the method of the assembly of opposing linear arrays from two NdFeB magnet layers, its advantages, the possible ways of increasing the parameters further and its application in various areas.

• 한국자기학회:학술대회 개요집
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• 한국자기학회 2013년도 자성 및 자성재료 국제학술대회
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• pp.110-110
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• 2013

• Journal of Magnetics
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• 제18권3호
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• pp.240-244
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• 2013

The influences of Gallium doping on the magnetic microstructures and corrosion behaviors of Nd-Fe-B-Ti-C alloys are investigated. The cooling rate for obtaining fully amorphous structure is raised, and the glassforming ability is improved by the Ga addition. The High Resolution Transmission Electron Microscopy image shows that the ${\alpha}$-Fe and $Fe_3B$ soft magnetic phases become granular surrounded by the $Nd_2Fe_{14}B$ hard magnetic phase. The rms and $({\Delta}{\varphi})_{rms}$ value of Nd-Fe-B-Ti-C nanocomposite alloy thick ribbons in the typical topographic and magnetic force images detected by Magnetic Force Microscopy(MFM) decreases with 0.5 at% Ga addition. The corrosion resistances of $Nd_9Fe_{73}B_{12.6}C_{1.4}Ti_{4-x}Ga_x$ (x = 0, 0.5, 1) alloys are enhanced by the Ga addition. It can be attributed to the formation of more amorphous phases in the Ga doped samples.

• 대한치과보철학회지
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• 제40권5호
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• pp.470-483
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• 2002

The purpose of this study was to investigate further the mechanics of failure of magnets used for denture retention. Dyna magnets were retrived from denture that had failed after 34 months of clinical use. The magnets were observed and sectioned in order to analyse with high resolution scanning electron microscope. From this study, corrosion behaviors of used magnetic attachment were analysed. The results were as follows ; 1. In Nd-Fe-B based magnetic materials, the erosion-corrosion was started at ununiformed part of stainless steel cover. 2. Corrosion was initiated at weared stainless steel surface and then magnetic materials were spalled by corrosive solution. 3. Spatting was occurred in Nd-Fe-B magnet materials due to corrosion products and then corrosion rate was increased drastically. 4. Corrosion started from ununiformed stainless steel surface as well as welded zone. In conclusion, the failure of magnets may occur by either breakdown of the welding or breakdown of the encapsulating material. So, it is considered that the corrosion problem of dental magnetic materials could be solved to some extent with surface treatment of dental magnetic materials.

• 한국자기학회지
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• 제13권4호
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• pp.182-186
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• 2003

펄스자장종축성형법(pulse die press, PDP)을 이용하여 32 wt%RE-67 wt%TM-1 wt%B(RE: 희토류원소, TM: 30천이금속)조성을 갖는 소결자석을 제조함에 있어서 자장성형시 분말의 탭밀도, 성형밀도, 인가자장세기 및 인가방법의 변화에 따라 얻어지는 자석의 배향율과 감자곡선상의 각형성 변화를 조사하였다. 출발합금 제조방법으로서 strip casting process에 의하여 $\alpha$-Fe 편석없이 미세하고 균일한 조직을 갖는 합금 flake가 얻어졌고, 합금 flake를 수소처리한 후 고압가스를 이용한 건식분쇄방법(jet mill)에 의하여 평균입도, 표준편차가 각각 3.65 $\mu\textrm{m}$, 1.39인 미세하고 균일한 입도의 분말로 제조하였다. 제조된 분말은 30-50 kOe치 고펄스자장에 의하여 분말을 배향시키고 동일한 펄스자장을 인가하면서 종축성형을 실시함으로써 배향율을 향상시킬 수 있었다. 결과적으로 32 wt%RE조성의 분말을 이용하여 종전의 자장성형방법인 TDP(transverse die press)와 본 연구에서 제안된 PDP에 의하여 제조된 자석의 최대자기에너지적은 각각 42.0 MGOe 및 44.8 MGOe가 얻어져, PDP가 분말의 배향율과 감자곡선상의 각 형성을 향상시키는데 효과적인 자장성형방법임을 알 수 있었다.

• 한국자기학회지
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• 제12권2호
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• pp.51-56
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• 2002

마그네트론 스퍼터링을 이용하여 퍼멀로이 박막의 제조시 요구되는 자기이방성 조절을 위하여 필요한 조건을 NdFeB자석과 3-D전산모사를 이용하여 평가하였으며, 또한 같은 조건에서 제조된 박막의 특성을 조사하였다. 타겟과 기판과의 거리가 5cm인 경우 타겟 자석과 자기이방성 조절을 위하여 장입된 영구자석의 상호 작용에 의하여 기판에 평행한 자속을 얻기 위한 조건이 전산모사 결과 영구자석간의 거리 변화에 매우 민감하였으며, 최적의 조건의 두 영구자석의 간격이 70mm에서 가장 균질한 자속을 대면적에서 얻을 수 있음이 확인되었다. 투입전력 450 W에서 기판에 장착시킨 NdFeB 자석간 거리(48, 60, 70, 80, 85mm) 를 변화시킨 결과 포화자화 값은 10~12 kG, 보자력은 0.2~1 Oe, 비저항은 20 $\mu$$\Omega$cm의 값을 갖는 퍼멀로이가 제조되었으며, 자기적 이방성은 전산모사의 결과와 일치하였다. 그 결과 자석간의 간격이 70mm에서 제조된 두께 1 $\mu$m 퍼말로이의 유효투자율이 10 MHz에서 2500을 유지하는 결과를 얻었다.

• 한국분말재료학회지
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• 제19권4호
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• pp.247-252
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• 2012

Effect of Cu and $DyF_3$ powder mixing with Cu-free (Nd, Dy)-Fe-B jet-milled powder on the magnetic properties of sintered magnets was investigated. The coercivity of a magnet prepared from the Cu-free (Nd, Dy)-Fe-B powder was about 10 kOe even though the alloy powder already contained some Dy (3.5 wt%). When small copper powder was blended, however, the coercivity of the magnet increased almost 100%, exhibiting about 20 kOe. On the contrary, the coercivity enhancement was moderate, about 4 kOe, when dysprosium content in the sintered magnet was simply increased to 4.9 wt% by the addition of small $DyF_3$3 powder.