DOI QR코드

DOI QR Code

Sintering Behavior and Phase Analysis of (Nd, Dy)-Fe-B Powder

(Nd, Dy)-Fe-B 분말의 소결특성 및 상변화 연구

  • Kim, Se-Hoon (Department of Materials Science and Engineering, Hanyang University) ;
  • Kim, Jin-Woo (Department of Materials Science and Engineering, Hanyang University) ;
  • Kim, Young-Do (Department of Materials Science and Engineering, Hanyang University)
  • Published : 2010.04.28

Abstract

In this study, the sintering behavior of (Nd, Dy)-Fe-B powder which fabricated by strip-casting was investigated with various sintering temperatures and holding times. The relative density over 99% could be obtained by both sintering at $1070^{\circ}C$ for 1h and sintering at $970^{\circ}C$ for 20h. The grain growth was observed in sintered specimen at $1050^{\circ}C$ compared to one at $970^{\circ}C$. The isothermal sintering process below $1000^{\circ}C$ led to suppress grain growth showing the improved magnetic properties. The phase transformation of Nd-rich was confirmed by X-ray diffraction pattern.

Keywords

References

  1. D. Brown, B.-M. Ma and Z. Chen: J. Magn. Magn. Mater., 248 (2002) 432. https://doi.org/10.1016/S0304-8853(02)00334-7
  2. S. H. Kim, Y. D. Kim and T. S. Jang: J. Korean Powder Metall. Inst., 15 (2008) 263 (Korean). https://doi.org/10.4150/KPMI.2008.15.4.263
  3. H.-S. Kim, S. H. Kim, J. W. Kim and Y. D. Kim: J. Korean Powder Metall. Inst., 17 (2010) 1 (Korean). https://doi.org/10.4150/KPMI.2010.17.1.001
  4. S. H. Kim, H.-S. Kim, D. H. Kim and Y. D. Kim: J. Korean Powder Metall. Inst., 15 (2008) 531 (Korean).
  5. S. J. Chu: Ultra-strong permanent magnet materials, Ulsan Univ. Pub., Ulsan, (1999).
  6. D. Lemarchand, P. Vigier and B. Labulle: IEEE Trans. Magn., 26 (1990) 2649. https://doi.org/10.1109/20.104826
  7. Y. Shinba, T. J. Konno, K. Ishikawa and K. Hiraga, J. Appl. Phys. 97 (2005) 053504. https://doi.org/10.1063/1.1851017
  8. F. Vial, F. Joly, E. Nevalainen, M. Sagawa, K. Hiraga and K. T. Park: J. Magn. Magn. Mater., 242-245 (2002) 1329 . https://doi.org/10.1016/S0304-8853(01)00967-2
  9. M. Matsuura, S. Sugimoto, R. Goto and N. Tezuka: J. Appl. Phys. 105 (2009) 07A741. https://doi.org/10.1063/1.3076050
  10. R. Ramensh, G. Thomas and B. M. Ma: J. Appl. Phys., 70 (1991) 6453. https://doi.org/10.1063/1.349928
  11. B. D. Cullity: Introduction to Magnetic Materials, Addison- Wesley, London, (1972).
  12. S. Nishio, R. Goto, M. Matsuura, N. Tezuka and S. Sugimoto: J. Jpn. Inst. Met., 72 (2008) 1010. https://doi.org/10.2320/jinstmet.72.1010

Cited by

  1. Magnetic Properties and Sintering Behavior of (Nd,Dy)-Fe-B Permanent Magnet by Spark Plasma Sintering vol.19, pp.2, 2012, https://doi.org/10.4150/KPMI.2012.19.2.105
  2. Crystallographic and Mössbauer studies of sintered Nd-Fe-B magnet vol.62, pp.11, 2013, https://doi.org/10.3938/jkps.62.1641