• Title/Summary/Keyword: NbC

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Analysis of Acoustic Reflectors for SAW Temperature Sensor and Wireless Measurement of Temperature (SAW 온도센서용 음향 반사판 분석 및 무선 온도 측정)

  • Kim, Ki-Bok;Kim, Seong-Hoon;Jeong, Jae-Kee;Shin, Beom-Soo
    • Journal of the Korean Society for Nondestructive Testing
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    • v.33 no.1
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    • pp.54-62
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    • 2013
  • In this study, a wireless and non-power SAW (surface acoustic wave) temperature sensor was developed. The single inter-digital transducer (IDT) of SAW temperature sensor of which resonance frequency is 434 MHz was fabricated on $128^{\circ}$ rot-X $LiNbO_3$ piezoelectric substrate by semiconductor processing technology. To find optimal acoustic reflector for SAW temperature sensor, various kinds of acoustic reflectors were fabricated and their reflection characteristics were analyzed. The IDT type acoustic reflector showed better reflection characteristic than other reflectors. The wireless temperature sensing system consisting of SAW temperature sensor with dipole antenna and a microprocessor based control circuit with dipole antenna for transmitting signal to activate the SAW temperature sensor and receiving the signal from SAW temperature sensor was developed. The result with wireless SAW temperature sensing system showed that the frequency of SAW temperature sensor was linearly decreased with the increase of temperature in the range of 40 to $80^{\circ}C$ and the developed wireless SAW temperature sensing system showed the excellent performance with the coefficient of determination of 0.99.

Geology and Mineral Resources of the Ogcheon Zone: Mineralization in the Pyeongchang-Jucheon Area, Kangwon-Do, Korea (옥천대(沃川帶)의 지질(地質) 및 광물자원(鑛物資源)에 관(關)한 연구(硏究) -평창(平昌)~주천지역(酒泉地域)에 있어서의 광화작용(鑛化作用)-)

  • Yun, Suckew;So, Chil Sop;Kim, Kyu Han
    • Economic and Environmental Geology
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    • v.19 no.1
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    • pp.1-18
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    • 1986
  • A group of 16 $Zn+Pb{\pm}Ag$ deposits distributed in the Pyeongchang-Jucheon area, Kangwon-do, South Korea, were semi-regionally investigated. These deposits are contact metasomatic and/or hydrothermal replacement types hosted in the carbonate-dominated Cambrian Machari Formation and Ordovician Ibtanri Formation, and also in the carbonate interbeds of the Precambrian argillic metasediments. Comparing some key aspects of the individual deposits, it is found that the ore deposits hosted in the Machari and Ibtanri Formations are mostly of steeply-dipping chimneys with or without skarn minerals and are rich in Ag and Pb>Zn in metal grade whereas those occuring in the carbonate interbeds of the Precambrian argillic metasediments are gently-dipping conformable lenticular orebodies mostly with skarn minerals and are generally poor in Ag and Zn>Pb. The skarn mineralization in the area appears to have occurred during the lower Cretaceous (118.7Ma) to mid-Cretaceous (107.8Ma) time assumed from the K-Ar dates of the Dowon and Pyeongchang granites which are closely associated with the skarn ore deposits. The Rb/Ba/Sr ratios of these granites indicate that they are of strongly differentiated anomalous granites, and the Nb vs. Y and Rb vs. Y+Nb plots fall on the field of volcanic arc setting. The contact aureoles are zoned, giving the sequence in order of increasing distance from igneous contact: garnet-wollastonite, granet-wollastonite-clinopyroxene and garnet-clinopyroxene in such as the Pyeongchang and Yeonwol 114 areas. Electron microprobe analyses reveal that garnets and clinopyroxenes are generally low in Fe and Mn. Garnets are grossular to intermediate grandite except for those from the Ogryong exoskarn which are richer in andradite, pyrope and spessartine fractions. This indicates that the oxidation state of skarn-forming environment at Ogryong was higher than at the other deposits. Clinopyroxenes are mostly salitic except for those from the Ogryong exoskarn which involve considerable amounts of hedenbergite and johansenite fractions. The ${\delta}^{18}O$ value of Jurassic biotite granite at Ogryong is higher (+10.21‰) than that of Cretaceous one at Chodun (+8.41‰). The ${\delta}^{13}C$ values of carbonate rocks range from -0.89‰ to 0.68‰ and the ${\delta}^{18}O$ values range from +11.91‰ to + 19.34‰ indicating that these carbonate rocks are of marine origin. However, the ${\delta}^{13}C$ values of skarn calcite and vein calcite are -4.80‰ and -12.92‰, and the ${\delta}^{18}O$ values are +5.56‰ and +10.32‰, respectively, indicating that these calcites are of hydrothermal origin. The ${\delta}^{34}S$ values of sulfide minerals range from +4.4‰ to +8.7‰ suggesting that the sulfurs are of magmatic origin.

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Stress Distribution in Microvascular Anastomotic Coupler (AnaFix®) Micropins with Respect to the Fillet Radius (필렛효과에 따른 미세혈관 문합커플러(AnaFix®) 마이크로핀의 응력분포)

  • Jee, Dae-Won;Kim, Cheol-Woong
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.35 no.11
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    • pp.1139-1145
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    • 2011
  • An automated anastomotic ring-pin system consisting of both the anastomotic ring-pin system and the coupler device has eliminated the drawbacks of the suture method. High density polyethylene (HDPE), a material with outstanding biocompatibility and injection molding capability, was used in the ring. SUS316 stainless steel, Ti-6Al-4Nb, Ti-6Al-4V, and unalloyed titanium were used in FEM simulations of the micropin. The authors categorized the microvascular anastomotic ring micropins into short neck (SN) and long neck (LN) groups in order to evaluate the effect of the micropin's fillet radius and neck length on the von Mises stress. The micropins were further divided into those with and without fillet. On the basis of the fillet radius rate (FRR), which represents the rate of change in the von Mises stress with respect to the availability and shape of the fillet, and the neck length rate (NLR), which represents the rate of change in the von Mises stress with respect to changes in the length of the neck within the fillet shape, it can be concluded that the SN-3 neck design is the most stable.

The Design and Characteristics of the Inductive Coupler Using the Nanocrystalline Materials (나노 결정립 재료를 이용한 비접촉식 커플러의 설계 및 특성)

  • Kim, Jong-Ryung;Kim, Hyun-Sik;Huh, Jeong-Sub;Lee, Hae-Yeon;Lee, Jun-Hui;Oh, Young-Woo;Byun, Woo-Bong
    • Journal of the Korean Magnetics Society
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    • v.16 no.6
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    • pp.300-304
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    • 2006
  • The varied heating temperatures were used for magnetic core materials, which nano sized ${\alpha}-Fe$ crystalline was created in nanocrystalline Fe-Si-B-Nb-Cu materials, with hish permeability and low power loss. The highest permeability and lowest power loss were obtained to the specimen heat-treated at $510^{\circ}C$. The signal transmission characteristics of inductive coupler, which was manufactured by using the magnetic core materials prepared in this study, at low frequency range, was influenced strongly by magnetic property of magnetic core materials as this result is corresponding to the permeability as a function of heat treatment temperature, as well, it was improved by impedance matching at high frequency range. Over $500{\mu}m$ of air gap in coupler is required to maintain the magnetic properties without magnetic saturation on the subterranean line transferred hish current of 300 A. The inductive coupler for PLC, which has an attenuation characteristics of less than 5dB, was manufactured using nano-crystalline magnetic core materials through the above mentioned research results.

Fabrication and Electrical Properties of High Tc $A_{2}B_{2}O_{7}$ Piezoelectric Ceramics Using the Powders Prepared by the Molten Salt Synthesis Method (용융염합성법에 의한 $A_{2}B_{2}O_{7}$ 고온압전세라믹스의 제작과 전기적특성)

  • Park, In-Ho;Kim, Tae-Gyu;Nam, Hyo-Duk
    • Journal of Sensor Science and Technology
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    • v.5 no.3
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    • pp.93-100
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    • 1996
  • Polycrystalline $Sr_{2}(Ta_{1-x}Nbx)_{2}O_{7}$ and $La_{2}Ti_{2}O_{7}$ ceramics having very high Curie temperatures were synthesized by the conventional oxide mixing method (CON) and the molten salt synthesis method (MSS). Physical characteristics and phase relationship of calcined powders, as well as the sintering behavior, the grain-orientation and dielectric properties of sintered ceramics were investigated as a function of composition and firing temperature. The single $A_{2}B_{2}O_{7}$ phase was synthesized by using the MSS method at 100 - $150^{\circ}C$ lower temperature compared to the CON method. As Nb content increased in $Sr_{2}(Ta_{1-x}Nbx)_{2}O_{7}$ ceramics, the Curie temperature and the dielectric constant at Curie temperature were raised, and the sintering behavior and the degree of grain-orientation were also improved at the same time. The use of MSS-derived powders made it possible to lower the sintering temperature and to improve the dielectric properties of the sintering samples. However, the piezoelectric properties as well as the grain-orientation were not improved any further by the MSS route.

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Study on the Dielectric Properties of $(Sr_{1-x}{\cdot}Ca_x)_mTiO_3$ Grain Boundary Layer Ceramics) ($(Sr_{1-x}{\cdot}Ca_x)_mTiO_3$ 입계층 세라믹의 유전특성에 관한 연구)

  • Kim, Jin-Sa;Choi, Woon-Shik;Shin, Chul-Gi;Kim, Sung-Yeol;Lee, Joon-Ung
    • Proceedings of the KIEE Conference
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    • 1994.11a
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    • pp.215-218
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    • 1994
  • Dielectric properties of $(Sr_{l-x}{\cdot}Ca_x)_mTiO_3+0.006Nb_2O_5$($0.05{\leq}x{\leq}0.2$, 0.996$N_2$) were painted on the surface with CuO paste, and then annealed at $1100^{\circ}C$ for 2hr. Grain size increased with increasing substitutional contents of Ca up to 15[mol%], but decreased with further substitution. In the specimens with $10{\sim}15[mol%]$ of Ca and m=1, excellent dielectric properties were obtained as follows; dielectric constant <25000, dielectric loss($tan{\delta}[%]$) <0.3[%] and capacitance change rate with temperature <${\pm}10[%]$, respectively. All the specimens in this study exhibited dielectric relaxation with frequency as a function of the temperature. The dispersive frequency was over $10^6[Hz]$.

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Crystal Structure Analysis of $LiN(D_xH_{1-x}){_4}SO_4$ by X-ray and Neutron Diffraction (X-선과 중성자 회절을 이용한 강유전체 단결정 $LiN(D_xH_{1-x}){_4}SO_4$의 결정구조 연구)

  • Kim, Shin-Ae;Kim, Seong-Hoon;So, Ji-Yong;Lee, Jeong-Soo;Lee, Chana-Hee
    • Journal of the Mineralogical Society of Korea
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    • v.20 no.4
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    • pp.351-356
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    • 2007
  • The crystal structure of $Li(ND_4)SO_4$ was analyzed by X-ray and neutron diffraction methods. The crystal is a deuterated $Li(NH_4)SO_4$ and one of the ferroelectric materials with hydrogen atoms. The crystal is orthorhombic at room temperature, $P2_1nb$, with lattice parameters of $a=5.2773(5)\;{\AA},\;b=9.1244(23)\;{\AA},\;c=8.7719(11)\;{\AA}$ and Z=4. Neutron intensity data were collected on the Four-Circle diffractometer (FCD) at HANARO in Korea Atomic Energy Research Institute and X-ray date were given by Prof. Y. Noda of Tohoku University Japan. The structure was refined by full-matrix least-square to final R value of 0.070 for 1450 observed reflections by X-ray diffraction and to final R=0.049 for 745 observed reflections by neutron diffraction. With X-ray data we obtained only one hydrogen atomic position. However, not only all atomic positions of four hydrogen atoms at $NH_4$ but also the occupation factors of D and H were refined with neutron data. From this results we obtained the average chemical structure of this sample, $LiND_{3.05}H_{0.95}SO_4$.

Microwave Dielectric Properties of Low Temperature Fired (${Pb_{0.45}}{Ca_{0.55}}$) [(${Fe _{0.5}}{Nb_{0.5}}$)$_{0.9}{Sn_{0.1}}$]$O_3$Ceramics with Various Additives

  • Ha, Jong-Yoon;Park, Ji-Won;Yoon, Seok-Jin;Kim, Hyun-Jai;Yoon, Ki-Hyun
    • Journal of the Korean Ceramic Society
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    • v.38 no.7
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    • pp.597-601
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    • 2001
  • The effect of CuO, $B_2$ $O_3$, $V_2$ $O_{5}$ and CuO-B $i_2$ $O_3$additives on microwave dielectric properties of (P $b_{0.45}$C $a_{0.55}$) [(F $e_{0.5}$N $b_{0.5}$)$_{0.9}$S $n_{0.1}$] $O_3$(PCFNS) were investigated. The PCFNS ceramics were sintered at 11$65^{\circ}C$. To decrease the sintering temperature for using as a low-temperature co-firing ceramics (LTCC), CuO, $B_2$ $O_3$, $V_2$ $O_{5}$ and CuO-B $i_2$ $O_3$were added to the PCFNS. As the content of CuO increased, the sintered density and dielectric constant increased and the temperature coefficient of resonance frequency ($\tau$$_{f}$) shifted to the positive value. When the CuO-B $i_2$ $O_3$were added, dielectric properties were $\varepsilon$$_{r}$ of 83, Q. $f_{0}$ of 6085 GHz, and $\tau$$_{f}$ of 8ppm/$^{\circ}C$ at a sintering temperature of 100$0^{\circ}C$. The relationship between the microstructure and properties of ceramics was studied by X-ray diffraction and scanning electron microscopy.icroscopy.y.icroscopy.y.

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Effect of Ti and C Contents on Prior Austenite Grain Size in Ti Added Steels (Ti 첨가강의 Ti와 C 함량에 따른 초기 오스테나이트 입도 변화)

  • Kim, Woo-Jin;Kang, Nam-Hyun;Kim, Sung-Ju;Do, Hyung-Hyup;Nam, Dae-Geun;Cho, Kyung-Mox
    • Korean Journal of Materials Research
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    • v.21 no.4
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    • pp.187-191
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    • 2011
  • Prior austenite grain size plays an important role in the production of high strength hot-rolled steel. This study investigated the effect of Ti and C contents on the precipitates and prior austenite grain size. Steel with no Ti solutes had prior austenite grain size of about 620 ${\mu}m$. The addition of Ti ~ 0.03 wt.% and 0.11 wt.% reduced the prior austenite grain size to 180 ${\mu}m$ and 120 ${\mu}m$, respectively. The amount of Ti required to significantly decrease the prior austenite grain size was in the range of 0.03 wt.%. However, the amount of carbon required to significantly decrease the prior austenite grain size was not present from 0.04 wt.% to 0.12 wt.%. Oxides of Ti ($Ti_2O_3$) were observed as the Ti content increased to 0.03 wt.%. The specimen containing 0.11 wt.% of Ti exhibited the complex carbides of (Ti, Nb) C. The formation of Ti precipitates was critical to reduce the prior austenite grain size. Furthermore, the consistency of prior austenite grain size increased as the carbon and Ti contents increased. During the reheating process of hot-rolled steel, the most critical factor for controlling the prior austenite grain size seems to be the presence of Ti precipitates.

Piezoelectric property variation with respect to the frit addition for lower temperature sintering in PNW-PMN-PZT ceramic system (PNW-PMN-PZT 압전 세라믹의 저온소결을 위한 프리트 첨가 압전 특성평가)

  • Ryu, Sung-Lim;Kwon, Soon-Yong;Woo, Duck-Hyun;An, Sang-Gi;Jeong, Ji-Hyun;Um, Ju-Chul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.191-191
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    • 2008
  • 강유전성 세라믹스 재료로써는 PZT계열의 세라믹재료가 널리 쓰이고 있다. 이는 우수한 유전 및 압전특성을 가지고 있으나, PbO을 다량 함유하고 있어 $1000^{\circ}C$이상에서 PbO가 급격하게 휘발되는 성질 때문에 조성의 변동이 생겨 재현성이 어려우며 이를 방지하기 위하여 PbO를 과잉 첨가시키기 때문에 PbO휘발로 인한 강한 독성이 인체에 유해하고, 비환경 친화적인 물질로 최근에는 환경문제가 대두됨에 따라 대체 또는 보완 할 수 있는 방안에 검토되고 있다. 본 연구는 그 해결책의 한 방안으로 압전특성이 우수한 $(Pb_{0.94}Sr_{0.06})[(Ni_{1/2}W_{1/2})_{0.02}(Mn_{1/3}Nb_{2/3})_{0.07}(Zr_{0.51}Ti_{0.49})_{0.91}]O_3$계 조성을 설계하고 Glass frit(0~1.1 wt%)를 소량 첨가하여 액상 소결 특성을 부여하고 $1000^{\circ}C$ 이하의 저온에서 소결하여 유전 및 압전 특성을 평가하였다. 실험방법은 일반적인 세라믹스 제조공정으로 24시간 ball milling하고 $850^{\circ}C$에서 2시간 하소 후 Glass frit를 소결조제로 소랑 첨가하여 $1000^{\circ}C$ 이하 온도에서 소결을 진행하여 각 소결온도에 따른 유전 및 압전 특성을 평가하였다. 최종 소결된 시편의 밀도와 수축율을 분석하여 최적의 소결온도를 확립하였으며 XRD분석을 통해 perovskite구조를 확인하고 미세구조확인을 위해 SEM으로 관찰하였다. 압전 특성을 평가하였다.

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