• 제목/요약/키워드: Nb addition

검색결과 491건 처리시간 0.03초

고에너지밀링과 스파크플라즈마소결을 이용한 Ti-Nb-Mo-CPP 생체복합재료의 제조 및 특성 (Fabrication and Characteristics of Ti-Nb-Mo-CPP Composite Fabricated by High Energy Mechanical Milling and Spark Plasma Sintering)

  • 박상훈;우기도;김지영;김상미
    • 대한금속재료학회지
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    • 제50권6호
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    • pp.469-475
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    • 2012
  • A high-energy mechanical milling (HEMM) process was introduced to improve sinter-ability, and rapid sintering of spark plasma sintering (SPS) under pressure was used to make ultra fine grain (UFG) of Ti-Nb-Mo-CPP composites, which have bio-attractive elements, for increasing mechanical properties. Ti-Nb-Mo-CPP composites were successfully fabricated by SPS at $1000^{\circ}C$ within 5 minutes under 70 MPa using HEMMed powders. The Vickers hardness of the composites increased with increased milling time and addition of CPP contents. Biocompatibility and corrosion resistance of the Ti-Nb-Mo alloys were improved by addition of CPP, and the Ti-35%Nb-10%Mo-10%CPP alloy had better biocompatibility and corrosion resistance than the Ti-6Al-4V ELI alloy.

$Nb_2O_5$를 첨가한 압전 세라믹 PZT의 전기적 특성 (Electrical Properties of Piezoceramic PZT with $Nb_2O_5$ Dopant)

  • 박정학;최헌일;사공건
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1991년도 추계학술대회 논문집 학회본부
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    • pp.336-338
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    • 1991
  • Effects of $Nb_2O_5$ addition ranged from 0.0 to 0.75(wt%) on the microstructure and electrical porperties of PZT ceramics have been investigated. The Pb vacancy concentration increases with increasing NbO content. However, the experimental results show the resistivity increases with increasing $Nb^{5+}$ content. This behavior can be explained as a compensation effect and $Nb^{5+}$ can serve as a donar and contribute electrons to the conduction process. According to the law of mass action, this result may reduce the total charge carrier:thus the resistivity increase with NbO content in PZT.

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분말고속도공구강의 미끄럼마모특성에 미치는 Nb의 영향 (The Effects of Niobium on Sliding Wear Characteristics of High Speed Steel by Powder Metallurgy)

  • 이한영;배종수;김용진
    • Tribology and Lubricants
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    • 제16권3호
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    • pp.194-200
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    • 2000
  • In order to evaluate the effect of Nb on wear properties of high speed steel(HSS) by powder metallurgy, niobium-alloyed HSS have been prepared by adding 0%, 1%, 3% and 5%Nb to HSS of 6%W-5%Mo-4 %Cr-5%V-5%Co. Sliding wear tests were conducted at various sliding speed conditions under the constant pressure using a pin-on-disc type machine. The results of this study show that the wear resistance of HSS by powder metallurgy was increased by the addition of Nb within the range of sliding speed used in this experimental study. However, the amount of Nb did not improve the wear resistance. It may be due to the thermal stability of carbide and high temperature properties of the matrix containing Nb comparing to that without Nb.

자기 환원성 $Nb_2O_5$ 브리켓의 반응특성 연구 (Study on the Reaction Characteristics of Self-reducing $Nb_2O_5$ Briquettes)

  • 김민석;유병돈;위창현;윤덕재;최석우
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 춘계학술대회 논문집
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    • pp.333-336
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    • 2005
  • The reduction behavior of $Nb_2O_5$ in aluminum containing self-reducing briquettes(SRNB) was investigated. The time required for slag/metal equilibrium was estimated as about 20 minutes from the addition of SRNB on to the surface of molten steel. The maximum yield of Nb was expected with the slag composition of $60\%CaO-40\%Al_2O_3$. When $CaCO_3$ was used as a flux, the oxidation loss of Al by $CO_2$ should be compensated, and the chemical equivalent ratio of Al to $Nb_2O_5$ of about 1.43 was required to maximize the yield of Nb.

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Ag(100) 기판위에 증착된 Nb Cluster에 관한 STM연구

  • 윤홍식;유미애;한권환;이준희;양경득;여인환
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2000년도 제18회 학술발표회 논문개요집
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    • pp.140-140
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    • 2000
  • The initial growth mode of Nb on Ag(11) in sub-monolayer regime and the influence of subsequent 520K annealing are studied using UHV Scanning Tunneling Microscopy. E-beam evaporated Nb is deposited onto the substrate at RT, and STM measurements are carried out at RT and 78 K. With Nb being immiscible in bulk Ag, 3D islands formation begins at early stage and no particular ordered structure is found. After annealing to 520K, most of islands are disappeared from terrace. There exist 2 possibilities. : (1) Diffusion of Nb into the 2nd or 3rd layer of Ag substrate or (2) agglomeration of Nb on Ag at higher temperature. A model will be given to explain the evidence. In addition, we investigated the change of STM image according to bias voltage depending on island size. Possible physical mechanism responsible for such behavior together with interaction between Nb islands and reactive gases will be also discussed.

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$(Sr_{1-x}{\cdot}Ca_x)TiO_3$세라믹의 유전특성에 미치는 $Nb_2O_5$ 첨가영향 (Effect of $Nb_2O_5$ Addition on the Dielectric Properties of $(Sr_{1-x}{\cdot}Ca_x)TiO_3$ Ceramic)

  • 김진사;정익형;최운식;김중혁;이준웅
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1996년도 추계학술대회 논문집
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    • pp.256-259
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    • 1996
  • $(Sr_{1-x}{\cdot}Ca_x)TiO_3+yNb_2O_5$($0.05{\leq}x{\leq}0.2$, 0.004$1350[^{\circ}C]$ in a reducing atmosphere($N_2$ gas). Dielectric propertries were investigated with contents of $Nb_2O_5$. The grain size and dielectric constant increase with increase $Nb_2O_5$, but decrease in $Nb_2O_5$ exceed($Nb_2O_5=0.6[mol%]$). Also, the temperature characteristics of the dielectric loss factor exhibited a stable value within 0.5[%]. The capacitance characteristics appeals a stab]e value in ${\pm}10[%]$.

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Nb 첨가량에 따른 Zr-0.8Sn-xNb 3원계 합금의 미세조직 및 부식특성 연구 (Study on Microstructure and Corrosion Characteristics of Zr-0.8Sn-xNb Ternary Alloys)

  • 김현길;정용환;위명용
    • 한국재료학회지
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    • 제9권5호
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    • pp.452-459
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    • 1999
  • 고연소도 핵연료피복관용 신합금 재료를 개발하기 위한 연구로 Zr-0.8Sn-xNb(x = 0.2,0.4,0.8, 1.0) 계 합금을 제조하여 Nb 첨가량이 Zr 합금의 미세구조 및 부식특성에 미치는 영향을 조사하였다. 미세조직 관찰결과 Nb첨가량이 증가함에 따라 결정립의 크기는 강소하였고 석출물의 량은 증가하였다. $360^{\circ}C$ 물 분위기에서 부식시험 한 결과 Nb 함량이 적을수록 부식저항성이 증가하는 경향을 나타냈으며며, Zr-0.8Sn-0.2Nb 합금이 가장 우수한 부식저항성을 보였다. 동얼 두께의 산화막에 대하여 XRD 분석한 결과, 내식성이 우수한 0.2 wt.% Nb 합금에서는 산화막내 tetra-$ZrO_2$의 분율이 높게 관찰되었다. 합금설계 관점에서 Zr-O.8Sn-xNb 합금계에 Nb올 첨가할때 Nb은 고용도 이하로 첨가되어야 한다고 사료된다.

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$Bi_2O_3$ 첨가에 따른 (Na,K)(Nb,Sb)$O_3$ 세라믹스의 압전 및 유전 특성 (Piezoelectric and Dielectric Properties of (Na,K)(Nb,Sb)$O_3$ Ceramics According to the Amount of $Bi_2O_3$ Addition)

  • 이상호;류주현;정영호;박용욱
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2010년도 하계학술대회 논문집
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    • pp.305-305
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    • 2010
  • In this study, in order to develop excellent lead free piezoelectric ceramics for piezoelectric transformer application (Na,K)(Nb,Sb)$O_3$ ceramics were fabricated using conventional oxides mixed method and their piezoelectric and dielectric characteristics were investigated according to the amount of $Bi_2O_3$ addition.

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Pb(Mg1/3Nb2/3)O3계의 유전성에 미치는 BaTiO3첨가량 및 열처리 온도의 영향 (PMN-BaTiO3계 세라믹스의 합성 및 유전성) (Influence of BaTiO3 Content and Firing Temperature on the Dielectric Properties of Pb(Mg1/3Nb2/3)O3 Ceramics)

  • 윤기현;강동헌
    • 한국세라믹학회지
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    • 제26권2호
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    • pp.249-257
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    • 1989
  • Dielectric properties and the stability of the perovskite phase in the Pb(Mg1/3Nb2/3)O3 system have been investigated as a function of amount of BaTiO3 and firing temperature. In the specimens fired at 120$0^{\circ}C$, the pyrochlore phase was eliminated by the addition of 10-15m/o BaTiO3 and also the dielectric constant increased. However, the dielectric constant decreased with further addition of BaTiO3 even though no pyrochlore phase was found to be present. The reducing tendency of the pyrochlore phase decreased with lowering the firing temperature in the system of Pb(Mg1/3Nb2/3)O3 with BaTiO3. Dielectric properties in PMN ceramics were affected by the character of the BaTiO3 rather than the pyrochlore phase.

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$MoO_3$첨가에 따른 $BiNbO_4$의 마이크로파 유전특성 (The Microwave Dielectric Properties of $BiNbO_4$ as The Addition of $MoO_3$)

  • 박영순;김덕규;김규도;박춘배
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1999년도 추계학술대회 논문집
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    • pp.232-235
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    • 1999
  • In this paper, We described the effect of $MoO_3$ Addition and firing temperature on the microwave dielectric properties of $BiNb0_4$ ceramics. The specimens prepared by conventional mixed method was addicted by 0 - 0.03 wt% $MoO_3$ and fired at 860 - $950^{\circ}$ for 3hr. Density increased when $MoO_3$ is below O.Olwt% but decreased when over O.Olwt%. $BiNb0_4$ ceramics addicted with CuO 0.03wt % and $MoO_3$ 0.01 wt% showed microwave dielectric properties, Dielectric constant 37.5, Quality factor[Qx$f_0$]5500, Temperature coefficient of resonance frequency 15ppm/$^{\circ}$

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