• Title/Summary/Keyword: Nano-hardness

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Effects of High Neutral Beam Energy on the Properties of Amorphous Carbon Films

  • Lee, Dong-Hyeok;Jang, Jin-Nyeong;Gwon, Gwang-Ho;Yu, Seok-Jae;Lee, Bong-Ju;Hong, Mun-Pyo
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.477-477
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    • 2012
  • The effects of argon neutral beam (NB) energy on the amorphous carbon (a-C) films were investigated, while the a-C films were deposited by neutral particle beam assisted sputtering (NBAS) system. The deposition characteristics of these films were studied as a function of NB energy (or reflector bias voltage). The film structures were investigated by Raman spectroscopy. The hardness was measured by nano-indentation tests and the optical band gap was measured by UV-visible spectroscopy.

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Transmission Electron Microscopy Specimen Preparation of Delicate Materials Using Tripod Polisher

  • Cha, Hyun-Woo;Kang, Min-Chul;Shin, Keesam;Yang, Cheol-Woong
    • Applied Microscopy
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    • v.46 no.2
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    • pp.110-115
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    • 2016
  • Transmission electron microscopy (TEM) is a powerful tool for analyzing a broad range of materials and provides localized information about the microstructure. However, the analysis results are strongly influenced by the quality of the thin foil specimen. Sample preparation for TEM analysis requires considerable skill, especially when the area of interest is small or the material of interest is difficult to thin because of its high hardness and its mechanical instability when thinned. This article selectively reviews recent advances in TEM sample preparation techniques using a tripod polisher. In particular, it introduces two typical types (fl at type and wedge type) of TEM sample preparation and the benefits and drawbacks of each method; finally, a method of making better samples for TEM analysis is suggested.

Analysis of Both Hands' Two Pulse Waveforms using a Clip-type Pulsimeter Equipped with Magnetic Sensing Hall Device

  • Rhee, Jin-Kyu;Lee, Sang-Suk
    • Journal of Magnetics
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    • v.18 no.2
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    • pp.183-187
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    • 2013
  • Two concurrent signals of the pulse wave measured from both hands' radial artery in un-pressurization condition using the prototype model of two clip-type pulsimeters with a permanent magnet and Hall device are investigated. The phase differences of two pulse waves from 22 subjects have some distinct points according to the handedness. Thus, the propagation of the pulse wave calculated from phase difference is both fast and slow to each other. It is confirmed that this phenomenon comes from the difference of blood vessel hardness between right- and left-hand of each subject rather than a quantity of muscle.

Tribological Properties of Annealed Diamond-like Carbon Film Synthesized by RF PECVD Method

  • Choi, Won-Seok
    • Transactions on Electrical and Electronic Materials
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    • v.7 no.3
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    • pp.118-122
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    • 2006
  • Diamond-like carbon (DLC) films were prepared on silicon substrates by the RF PECVD (Plasma Enhanced Chemical Vapor Deposition) method using methane $(CH_4)$ and hydrogen $(H_2)$ gas. We examined the effects of the post annealing temperature on the tribological properties of the DLC films using friction force microscopy (FFM). The films were annealed at various temperatures ranging from 300 to $900^{\circ}C$ in steps of $200^{\circ}C$ using RTA equipment in nitrogen ambient. The thickness of the film was observed by scanning electron microscopy (SEM) and surface profile analysis. The surface morphology and surface energy of the films were examined using atomic force microscopy and contact angle measurement, respectively. The hardness of the DLC film was measured as a function of the post annealing temperature using a nano-indenter. The tribological characteristics were investigated by atomic force microscopy in FFM mode.

The Study on the Application of CNT Particle in High-Precision Magnetic Abrasive Polishing Process (초정밀 자기연마 공정에 탄소나노튜브 입자의 적용에 관한 연구)

  • Kwak, Tae-Kyung;Kwak, Jae-Seob
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.20 no.3
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    • pp.274-279
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    • 2011
  • In this study, new abrasives that were composed of iron powder and carbon nanotube (CNT) particle were attempted to be abrasives for magnetic abrasive polishing. Because the CNT particles itself are very small ones with high hardness and magnetic strength, these properties are effective for magnetic abrasive polishing of nonmagnetic materials. As an experimental result for evaluating the machining characteristics in magnetic abrasive polishing, the CNT particles showed better performance than the conventional abrasives such as Fe and CBN powder.

Effects of nano-particles additions on the adhesion propertis of coating layer (나노 입자 첨가에 따른 도장막의 부착력 평가)

  • Lee, Hyeon-Ju;U, Seong-Min;Kim, Ho-Hyeong;Hwang, Tae-Jin;Kim, Yang-Do
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2011.05a
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    • pp.70-70
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    • 2011
  • 표면처리는 전기적, 물리적, 화학적 처리방법 등을 통해 보호표면을 생성시킴으로서 재료의 외관미화, 내마모성, 전기절연, 전기전도성 부여 등의 폭넓은 목적을 달성시키고자 하는 일련의 조작을 말한다. 최근 스마트 휴대폰으로 대표되는 이동통신기기 산업의 빠른 성장으로 인하여 이들 기기를 보호하기 위한 표면 처리기술도 함께 발전하고 있다. 그중 대표적인 것이 나노기술을 융합한 보호막 도장기술이다. 나노입자를 분산하거나 나노상(phase)을 융합하여 제품의 표면에 보호막을 도장하는 기술이며, 그 주된 목적은 내 스크래치, 내 부식 등의 물리 화학적 보호기능을 수행하도록 층(layer)을 형성하는 것이다. 본 연구에서는 제조된 실리카 나노입자와 유기물을 사용하여 휴대폰 케이스에 도장막을 형성하였고, Scratch, Wear, hardness Test등의 분석을 통하여 유무기 하이브리드 도장막의 특성을 평가하였다.

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Synthesis and Properties of Ultra-fine (Ti, M1, M2)(CN)-Ni Cermets

  • Kang, Young-Jae;Kang, Shin-Hoo
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.644-645
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    • 2006
  • TiC-and Ti(C,N)-based cermets are excellent in semi-and final finishing of work piece during cutting operations. Typical microstructure of the cermets is a core/rim structure. The undissolved Ti(C,N) cores contribute to their high hardness while the rim phases, (Ti,M1,M2)(C,N)-type solid solutions, play great roles in enhancing the toughness. In this paper, various ultrafine pre-mixed MeC-Ni powders were synthesized and the powders were sintered or hot pressed after mixing in order to control the size and volume fractions of core and rim phases in the system. This paper will present the factors determining the microstructure along with mechanical properties.

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Fabrication and Properties of Fe-Ni Nano Thin Film and Wire by Electrodeposition Method (Electrodeposition법에 의한 Fe-Ni 나노박막 및 나노선 제조 및 특성)

  • Koo, Bon-Keup;Shin, Dong-Yul;Jung, Woo-Ram;Jung, Sang-Ok;Kim, Dae-Yong;Choi, Mok-Ryeon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.557-558
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    • 2006
  • The mechanical properties of micro-hardness and internal stress of Ni-Fe alloy thin film made by electrodeposition method have been measured as a function of bath composition and current density. And also the microstructure of $200{\AA}$ Ni-Fi nanowires made using anodic aluminum oxide(AAO) templates by electrodeposition method have been observed by SEM as a function of ultrasonic treatment time and bath composition.

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Improved Adhesion of DLC Films by using a Nitriding Layer on AISI H13 Substrate

  • Park, Min-Seok;Kim, Dae-Young;Shin, Chang-Seouk;Kim, Wang Ryeol
    • Journal of the Korean institute of surface engineering
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    • v.54 no.6
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    • pp.307-314
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    • 2021
  • Diamond-like carbon (DLC) is difficult to achieve sufficient adhesion because of weak bonding between DLC film and the substrate. The purpose of this study is to improve the adhesion between substrate and DLC film. DLC film was deposited on AISI H13 using linear ion source. To improve adhesion, the substrate was treated by dual post plasma nitriding. In order to define the mechanism of the improvement in adhesive strength, the gradient layer between substrate and DLC film was analyzed by Glow Discharge Spectrometer (GDS) and Scanning Electron Microscope (SEM). The microstructure of the DLC film was analyzed using a micro Raman spectrometer. Mechanical properties were measured by nano-indentation, micro vickers hardness tester and tribology tester. The characteristic of adhesion was observed by scratch test. The adhesion of the DLC film was enhanced by active screen plasma nitriding layer.

Mechanical Properties of the Laminated Glass Fiber-Reinforced Plastic Composites for Electromagnet Structure System (전자석 구조물용 적층 유리섬유강화 복합재료의 기계적 특성)

  • Park, Han Ju;Kim, Hak Kun;Song, Jun Hee
    • Korean Journal of Metals and Materials
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    • v.49 no.8
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    • pp.589-595
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    • 2011
  • Laminated glass fiber-reinforced plastic (GFRP) composites were applied to an insulating structure of a magnet system for a nuclear fusion device. Decreased inter-laminar strength by a strong repulsive force between coils which is induced a problem of structural integrity in laminated GFRPs. Therefore, it is important to investigate the inter-laminar characteristics of laminated GFRP composites in order to assure more reliable design and better structural integrity. Three types of the laminated GFRP composites using a high voltage insulating materials were fabricated according to each molding process. To evaluate the grade of the fabricated composites, mechanical tests, such as hardness, tensile and compressive tests,were carried out. The autoclave molding composites satisfied almost of the mechanical properties reguested at the G10 class standard, but the vacuum impregnation (VPI) and Prepreg composites did not.