• Title/Summary/Keyword: Nano-hardness

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Mechanical Properties of PMMA / Alumina Composites Fused by Heat Treatment (용융 열처리한 PMMA/Alumina 복합체의 기계 특성)

  • Kim, D.J.;Ryu, S.C.
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.3
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    • pp.120-125
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    • 2018
  • The PMMA composited material mixed with alumina studied to find the optimal condition, the adequate ratio of mixing, for the associated mechanical properties such as anti-corrosive, weatherproof performance. The 80% of hardness and 52% of scratch coefficient improved according to increasing ratio of alumina, which is mostly 3 times higher than that of pure PMMA, on other hand 16% of tensile strength and 35% of flexural strength has lost while alumina was adding in. The most proper ratio, having the best availability in substantial production, of composite between pure PMMA and alumina is determined as 93 wt. % vs 7 wt. %. Results of related five properties had estimated by using of a pentagram.

Development of Expert System for the Diagnostic of NTM Decision-Making (특수가공법 의사결정 진단 전문가 시스템 개발)

  • Yoon, Moon-Chul;Cho, Hyun-Deog
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.19 no.1
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    • pp.94-100
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    • 2010
  • Nowadays, several nontraditional machining(NTM) processes are widely used to machine a complex and accurate shape part of hard materials, such as titanium, ceramics, high strength temperature resistant and refractory materials which are difficult to machine and having high strength, hardness, toughness. Machining of these complex shapes in such materials by traditional machining processes are very difficult. The NTM processes is important in the areas of micro- and nano scale machining, where high accuracy and superior surface characteristics are required, which can only be achieved using these NTM processes. So, for effective selection of different NTM processes, careful decision making for a given NTM application is often necessary. An appropriate NTM process for a given material and shape condition is very difficult for the novice engineers. In this paper, an expert system based on an analytic network process(ANP) is suggested for a best selection of NTM process in a NTM application considering an prior interdependency effect among various factors.

Mechanical Properties of Carbon Nanotube/Cu Nanocomposites Produced by Powder Equal Channel Angular Pressing (분말 ECAP 공정으로 제조된 탄소나노튜브/Cu 나노복합재료의 기계적 성질)

  • Yoon, Seung-Chae;Jeong, Young-Gi;Kim, Hyoung-Seop
    • Transactions of Materials Processing
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    • v.15 no.5 s.86
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    • pp.360-365
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    • 2006
  • Carbon nanotubes (CNTs) have been the subject of intensive studies for applications in the fields of nano technologies in recent years due to their superior mechanical, electric, optical and electronic properties. Because of their exceptionally small diameters (${\appros}\;several\;nm$) as well as their high Young's modulus (${\appros}1\;TPa$), tensile strength (${\appros}\;200\;GPa$) and high elongation (10-30%) in addition to a high chemical stability, CNTs are attractive reinforcement materials for light weight and high strength metal matrix composites. Although extensive researches have been performed on the electrical, mechanical and functional properties of CNTs, there are not many successful results on the mechanical properties of CNT dispersed nanocomposites. In this paper, we applied equal channel angular pressing for consolidation of CNT/Cu powder mixtures. We also investigated the hardness and microstructures of CNT/Cu nanocomposites used experimental for metal matrix composites.

Determination of the mechanical properties of coated layer in the sheet metal (표면처리강판 코팅층의 기계적 특성결정에 관한 연구)

  • 고영호;이정민;김병민
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.343-346
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    • 2004
  • In recent years, various forms of indentation testing have been increasingly used to determine the material properties of specimens. This technique, particularly the nano-indentation method , has been extended to the testing of coating systems in order to calculate the individual properties of the thin coatings and the substrates. However, the interpretation of the test data to achieve this is complex and continues to be a widely studied subject. Based on the finite element method of coated surfaces indented by a Berkovich diamond tip, this paper describes methods for combining FEM and experimental indentation testing to determine coating modulus and hardness independent of substrate effects. Using this proposed methodology, testing and FEM to measure coefficients of friction of sheet steel for outer panel were studied.

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Synthesis of Cu/Al2O3 Nanostructured Composite Powders for Electrode Application by Thermochemical Process (열화학적 방법에 의한 전극용 나노 Cu/Al2O3 복합분말 합성)

  • 이동원;배정현;김병기
    • Journal of Powder Materials
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    • v.10 no.5
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    • pp.337-343
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    • 2003
  • Nanostructured Cu-$Al_2O_3$ composite powders were synthesized by thermochemical process. The synthesis procedures are 1) preparation of precursor powder by spray drying of solution made from water-soluble copper and aluminum nitrates, 2) air heat treatments to evaporate volatile components in the precursor powder and synthesis of nano-structured CuO + $Al_2O_3$, and 3) CuO reduction by hydrogen into pure Cu. The suggested procedures stimulated the formation of the gamma-$Al_2O_3$, and different alumina formation behaviors appeared with various heat treating temperatures. The mean particle size of the final Cu/$Al_2O_3$ composite powders produced was 20 nm, and the electrical conductivity and hardness in the hot-extruded bulk were competitive with Cu/$Al_2O_3$ composite by the conventional internal oxidation process.

An Investigation of Sliding Wear and Microstructural Evolution of Ultra-Fine Grained Pure Al Fabricated by ARB Process (누적압연접합(Accumulative Roll-Bonding, ARB)에 의한 Al의 결정립 미세화와 마모 특성 연구)

  • Park K.S.;Lee T.O.;Kim Y.S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2000.10a
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    • pp.21-24
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    • 2000
  • Ultra-fine grains were produced in pure Al using an Accumulative Rolling-Bonding (ARB) process. After several cycles of the ARB process, pure Al sheets were filled with the ultra-fine grains whose diameters were several hundred nano-meters. With ARB cycles, the nature of grain boundaries of the ultra-fine grains changed from diffusive sub-boundaries to well-defined high angle boundaries. After 7 cycles, ultra-fine polycrystals with large misorientations between neighboring grains were obtained. Sliding wear tests using a pin-on-disk type wear tester were co ducted on the ultra-fine grained pure Al. Wear rates of pure Al increased with the increase of ARB cycle numbers in spite of the increase in hardness. Worn surfaces and cross-sections were examined with optical microscopy (OM) and scanning electron microscopy (SEM) In investigate the wear mechanism of the ultra-fine grained pure Al.

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A Comparative Study of HfN Coatings Deposited by DC and Pulsed DC Asymmetric Bipolar Magnetron Sputtering (DC 스퍼터법과 비대칭 바이폴라 펄스 DC 스퍼터법으로 증착된 HfN 코팅막의 물성 비교연구)

  • Jeon, Seong-Yong;Jeong, Pyeong-Geun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.103.2-103.2
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    • 2017
  • Nanocrystalline HfN coatings were prepared by reactively sputtering Hf metal target with N2 gas using a magnetron sputtering system operated in DC and ABPP (asymmetric bipolar pulsed plasma) condition with various duties and frequencies. The effects of duty and frequency, ranging from 75 to 100 % and 5 to 50 kHz, on the coating microstructure, crystallographic and mechanical properties were systematically investigated with FE-SEM, AFM, XRD and nanoindentation. The results show that pulsed plasma has a significant influence on coating microstructure and mechanical properties of HfN coatings. Coating microstructure evolves from the columnar structure to a highly dense one as duty decreases. Average grain size and nano hardness of HfN coatings were also investigated with various pulsed conditions.

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A Comparative Study of Nanocrystalline HfN Coatings Fabricated by Direct Current and Inductively Coupled Plasma Assisted Magnetron Sputtering (DC 스퍼터법과 유도결합형 플라즈마 스퍼터법으로 증착된 HfN 코팅막의 물성 비교연구)

  • Jeon, Seong-Yong;Lee, So-Yeon
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.103.1-103.1
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    • 2017
  • Nanocrystalline HfN coatings were prepared by reactively sputtering Hf metal target with N2 gas using a magnetron sputtering system operated in DC and ICP (inductively coupled plasma) condition with various powers. The effects of ICP power, ranging from 0 to 200 W, on the coating microstructure, corrosion and mechanical properties were systematically investigated with FE-SEM, AFM, potentiostat and nanoindentation. The results show that ICP power has a significant influence on coating microstructure and mechanical properties of HfN coatings. With the increasing of ICP power, coating microstructure evolves from the columnar structure of DC process to a highly dense one. Average grain size and nano hardness of HfN coatings were also investigated with increasing ICP powers.

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크립현상을 고려한 PMMA의 상온 나노압입실험에 대한 연구

  • 윤성원;김현일;강충길
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.05a
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    • pp.133-133
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    • 2004
  • 박막이나 초미세 구조체의 경도 및 탄성계수 측정을 위한 나노 압입실험에서는 Oliver & Pharr가 제안한 하중-변위 측정 나노압입법이 널리 쓰이고 있다 위 실험법에서, 나노경도(nano-hardness; H$_{n}$)는 최대하중을 계산된 접촉면적 (A$_{c}$)으로 나누어 평가하고, 압입자 및 박막의 탄성성질을 포함하는 환산 탄성계수 (reduced modulus ; E$_{r}$)는 하중제거곡선의 초기 기울기인 접촉탄성강성 (S)를 이용하여 계산한다. 그러나, 하중-변위 측정 나노압입법에서는 탄성 및 소성변형만이 고려되고 시간 의존적 변형거동 (time dependent deformation; TDD)은 고려되지 않는다.(중략)

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Improvement of Adhesion Strength of DLC Films on Nitrided Layer Prepared by Linear Ion Source

  • Shin, Chang-Seouk;Kim, Wang-Ryeol;Park, Min-Seok;Jung, Uoo-Chang;Chung, Won-Sub
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.177-179
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    • 2011
  • The purpose of this study is to enhance an adhesion between substrate and Diamond-like Carbon (DLC) film. DLC has many outstanding properties such as low friction, high wear resistance and corrosion resistance. However, it is difficult to achieve enough adhesion because of weak bonding between DLC film and the substrate. For improvement adhesion, a layer between DLC film and the substrate was prepared by dual post plasma. DLC film was deposited on nitrided layer by linear ion source. The composed compound layer between substrate and DLC film was investigated by Glow Discharge Spectrometer (GDS) and Scanning Electron Microscope (SEM). The synthesized bonding structure of DLC film was analyzed using a micro raman spectrometer. Mechanical properties were measured by nano-indentation. In order to clarify the mechanism for improvement in adhesive strength, it was observed by scratch test.

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