• Textile Coloration and Finishing
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• 제16권4호
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• pp.1-9
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• 2004

In recent, development of nano fiber has been one of the most active subjects in the world. Nano fiber is defined as a ultra fine yarn with a diameter unit of $10-100\times10^{-9}meter$, which is possible to be produced by an electro-spinning technology. In this study, physical characteristics and dyeing properties of nylon 66 nano fiber were investigated. Nylon 66 nano fiber was dyed with levelling type acid dyes. X-ray diffraction method and DSC analysis were used for the measurement of the degree of crystallization. Analysis of amino end groups was also performed in order to examine a relationship between number of amino groups and its dyeing property as well as water absorption behavior. The maximum exhaustion % of dyes and dyeing rate under various dyeing conditions, such as dyeing temperature and pH in dye bath, along with build-up properties for 2 acid dyes were evaluated. It was found that the degree of crystallization of nano fiber was smaller than that of regular fiber, and amino end groups of nano fiber were less than regular fiber. Half dyeing time of nano fiber was shorter than regular fiber because of the bigger specific surface area. Effect of pH on exhaustion % was small in case of nano fiber. Exhaustion of nano fiber increased with higher concentration of dye.

• Fibers and Polymers
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• 제6권1호
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• pp.35-41
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• 2005

Research and development of nano fiber products is very active over the world. Physical characteristics and dyeing properties of nylon 66 nano fiber were investigated in this study. X-ray diffraction, DSC, analysis of amino end group, and water absorption were performed to get information concerning physical properties of nano fiber. Nylon 66 nano fiber was dyed with high molecular mass acid dyes. Effects of dyeing temperature, pH of dyeing solution, and concentration of acid dyes on dyeing properties such as rate of dyeing and the extent of exhaustion, were examined and compared to those of regu­lar fiber. It was found that nano fiber adsorbed acid dyes at lower temperature, got rapidly dyed, and its extents of exhaustion at specific dyeing temperature were higher than regular fiber. It was also observed that nano fiber could adsorb a large amount of acid dye without a significant loss in the extent of exhaustion. Washing fastness of the dyed nano fiber was lower by $1/2\~1$ grade, light fastness by 1 grade than the dyed regular fiber.

• Geomechanics and Engineering
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• 제37권1호
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• pp.85-95
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• 2024

This study investigates the influence of nano-silica and basalt fiber content, curing duration, and freeze-thaw cycles on the static and dynamic properties of soil specimens. A comprehensive series of tests, including Unconfined Compressive Strength (UCS), static triaxial, and dynamic triaxial tests, were conducted. Additionally, scanning electron microscopy (SEM) analysis was employed to examine the microstructure of treated specimens. Results indicate that a combination of 1% fiber and 10% nano-silica yields optimal soil enhancement. The failure patterns of specimens varied significantly depending on the type of additive. Static triaxial tests revealed a notable reduction in the brittleness index (IB) with the inclusion of basalt fibers. Specimens containing 10% nano-silica and 1% fiber exhibited superior shear strength parameters and UCS. The highest cohesion and friction angle were obtained for treated specimens with 10% nano-silica and 1% fiber, 90 kPa and 37.8°, respectively. Furthermore, an increase in curing time led to a significant increase in UCS values for specimens containing nano-silica. Additionally, the addition of fiber resulted in a decrease in IB, while the addition of nano-silica led to an increase in IB. Increasing nano-silica content in stabilized specimens enhanced shear modulus while decreasing the damping ratio. Freeze-thaw cycles were found to decrease the cohesion of treated specimens based on the results of static triaxial tests. Specimens treated with 10% nano-silica and 1% fiber experienced a reduction in shear modulus and an increase in the damping ratio under freeze-thaw conditions. SEM analysis reveals dense microstructure in nano-silica stabilized specimens, enhanced adhesion of soil particles and fibers, and increased roughness on fiber surfaces.

• Journal of The Korean Society of Agricultural Engineers
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• 제55권3호
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• pp.113-121
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• 2013

Recently, it has been studied for the application of nano-materials in the concrete. Applied a small amount of nano-materials can achieve the goal of high strength, high performance and high durability. The small addition of nano clay improves strength, thermal stability, and durability of concrete because of the excellent dispersion. The present study has investigated the effectiveness, when varying with the contents of nano clay, influencing the pull-out behavior of macro synthetic fibers in nano materials cement mortar. Pullout tests conducted in accordance with the Japan Concrete Institute (JCI) SF-8 standard for fiber-reinforced concrete test methods were used to evaluate the pullout performance of the different nano clay. Nano clay was added to the 0, 1, 2, 3, 4 and 5 % of cement weight. The experimental results demonstrated that the addition of nano clay led to improve the pull-out properties as of the load-displacement curve in the precracked and debonded zone. Also, the compressive strength, flexural strength and pullout performance and of Mix No. 1 and No. 2 increased up to the point when nano clay used increased by 2 and 3 % contents, respectively, but decreased when the exceeded 3 and 4 %, respectively. It was proved by verifying increase of the scratching phenomenon in macro synthetic fiber surface through the microstructure analysis on the surface of macro synthetic fiber.

• Textile Coloration and Finishing
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• 제18권2호
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• pp.1-7
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• 2006

In order to prepare PAN nano fiber web, PAN/DMF solution was prepared and electrospun. The diameter of fiber was depended on the polymer concentration (7.5-15wt%) and the applied voltage (10-16kV). The average diameter of fiber increased with an increase of the polymer concentration and decreased with the applied voltage. At 7.5wt% concentration, many beads were found. So, we prepared a nano PAN fiber by electrospinning at concentration of 10wt% and 16kV. PAN fibers were reduced with litium aluminium hydride and the dyeability to acid dye was checked. The reduced nano PAN fiber showed much better dyeability compared with the reduced ordinary PAN fiber. It was considered that the increase of specific surface area have an important role in dyeing with acid dye.

• Journal of Sensor Science and Technology
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• 제17권2호
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• pp.95-99
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• 2008

Various etching methods of optical fiber and formation of metal nano particles on the optical fiber have been proposed for fabrication of fiber optic localized surface plasmon resonance (FO LSPR) biosensors. Different types of etched optical fiber are possible by removing the cladding of optical fiber using HF (hydrofluoric acid) solution and BHF (buffered hydrofluoric acid) solution, which results in improved surface roughness when BHF solution is used. Localized surface plasmon can be formed and measured by formation of silver and gold nano particles on the etched optical fiber. The characteristics of the etched optical fiber and metal nano particles on the etched surface of the optical fiber play a key role in dictating the sensitivity of the LSPR sensors, so that the proposed results can be expected to be applied for related research on fiber optic based biosensors.

• Textile Coloration and Finishing
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• 제17권4호
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• pp.27-34
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• 2005

In order to prepare acetate nano filter for the adsorption of nicotine/tar in tobbaco, acetate nano fiber was fabricated by elecrospining from acetate solution dissolved in acetone/DMAc(2/1). Above a critical polymer concentration($15\%$), the nano fiber was formed. The average diameter of nano fiber was decreased with the applied voltage and increased with the feeding rate. Appropriate spinning condition was considered to be $15wt\%$ polymer concentration, 11.25kV applied voltage, 0.6ml/h feeding rate, and 13-15cm TCD. Using the nano fiber, acetate nano filter was fabricated. It showed good nicotine/tar adsorption ability compared with general tobbaco filter. It was considered that the increase of surface area and the development of microporous structure in filter was much affected to the adsorption of nicotine/tar.

• Proceedings of the Korean Fiber Society Conference
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• 한국섬유공학회 2007년도 학술발표회 논문집
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• pp.485-486
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• 2007

• Proceedings of the Korean Society of Precision Engineering Conference
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• 한국정밀공학회 2009년도 추계학술대회 논문집
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• pp.71-72
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• 2009

• Korean Journal of Metals and Materials
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• 제50권2호
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• pp.93-99
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• 2012

The mechanical properties of nano composites were evaluated for structural performance in order to enhance their applicability to the car and machine industrial fields. Carbon fiber reinforced plastics (CFRP) and GFRP were manufactured by vacuum-assisted resin transfer molding (VARTM) process with good mechanical properties. Tensile test was conducted to obtain the process factor of each composite. Also, carbon nano fiber (CNF) was dispersed in the composites and the relationship between the mechanical property and the CNF fraction was compared. The tensile strength and stiffness of 0/90 laminated CFRP were the best. CFRP/CNF (0.5 wt.%) was confirmed to be an excellent material for its elasticity and tensile strength.