• Title/Summary/Keyword: Nano-Porous Alumina

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Basic Experimental Investigations to UV Laser Micro-Machining of Nano-Porous Alumina Ceramic Material (나노 다공 구조를 가진 알루미나 재료의 UV 레이저 미세가공에 관한 실험적 기초 연구)

  • Shin, Bo-Sung;Lee, Jung-Han
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.11 no.1
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    • pp.62-67
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    • 2012
  • Recently UV laser is widely used to process micro parts using various materials such as polymers, metals and ceramics because it has a very high intensity at the focused spot area. It is generally known that there are still some difficulties for alumina($Al_2O_3$) ceramics to directly make micro patterns like holes and lines on the surface of working material using 355nm UV laser because the alumina has a very low absorption coefficient at that wavelength. But nowadays new alumna with nano-porous holes is developed and applied to advanced micro functional parts of IT, BT and BT industries. In this paper, we are going to show the mechanism of photo-thermal ablation for nano-porous ceramics. Inside hole there is a lot of multiple reflections along the depth of hole. Experimentally we can find the micro hole drilling and micro grooving on the surface of nano-porous alumina.

Fabrication of Nano Metal Compounds Using Porous Aluminum Oxide Films (기공성 알루미나 산화 피막을 이용한 나노 금속화합물의 제조)

  • Oh, Han-Jun;Jeong, Yong-Soo;Chi, Choong-Soo
    • Journal of the Korean institute of surface engineering
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    • v.43 no.5
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    • pp.248-254
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    • 2010
  • Porous $Al_2O_3$ film can be utilized as template for fabrication of nano-structured materials. Porous anodic alumina layer as template was prepared by anodization of aluminum in oxalic acid, and the pore diameter and barrier-type alumina layer can be controlled for proper anodizing parameter by widening process in $H_3PO_4$ solution. The $SiO_2$ nanodot and Ni nanowire was fabricated using anodic alumina template and their characteristics were investigated using SEM and TEM with EDS. Especially the growth mechanism of $SiO_2$ nanodot in alumina membrane compared with thinning of the alumina barrier layer during anodization was also investigated.

Improvement of output coupling efficiency of organic light emitting device by using porous anodic alumina

  • Lee, Hyung-Sup;Choi, Ji-Young;Gao, Xinwei;Kim, Seong-Su;Lee, K.W.
    • 한국정보디스플레이학회:학술대회논문집
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    • 2004.08a
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    • pp.625-628
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    • 2004
  • Porous anodic alumina(PAA) which has arrays of nano size holes, was incorporated into organic light emitting devices. Porous anodic alumina on glass scattered the light generated from emitting layer and was decreased the waveguiding modes within the glass. An increase in the device coupling-out factor for the scattering structure is demonstrated.

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Formation and Chemical Dissolution Behaviors of Nano Porous Alumina (나노 기공성 알루미나의 생성과 화학적 용해 거동)

  • Oh, Han-Jun;Jeong, Yong-Soo;Chi, Choong-Soo
    • Journal of the Korean institute of surface engineering
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    • v.43 no.5
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    • pp.217-223
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    • 2010
  • For an application as templates of high performance with proper pore size and shape, porous anodic alumina films were prepared by anodization in oxalic acid, and formation behaviors of anodic alumina layer as well as dissolution process in acid solution have been investigated. The surface characteristics on anodic alumina layer were shown to be dependent on the fabrication parameters for anodization. For the dissolution behaviors of anodic alumina, the thickness of the barrier-type alumina layer decreased linearly with the rate of 0.98 nm/min in $H_3PO_4$ solution at $30^{\circ}C$. The changes of the anodic alumina layers were analyzed by SEM and TEM.

Preparation of Nano Wire by Anodic Oxidation I. Characteristics of Alumina Nano-Template by Anodic Oxidation (양극산화법에 의한 나노와이어 제조I. 알루미나 나노 템플레이트의 특성)

  • Jo, Su-Haeng;O, Han-Jun;Park, Chi-Seon;Jang, Jae-Myeong;Ji, Chung-Su
    • Korean Journal of Materials Research
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    • v.12 no.2
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    • pp.121-128
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    • 2002
  • Anodic alumina layer can be used as templates for preparation of nano-structured materials, because porous oxide layer on aluminum shows a uniform pore size and a high pore density. In order to find out possibility for template material to prepare nano wire, the effects of the anodic applied potential, anodic time and the temperature of electrolyte on pore diameter of anodic alumina layer were studied using SEM and AFM. The pore diameter of anodic alumina layer increased with applied anodic potential and electrolytic temperature. Especially, the pore diameter of anodic oxide layers formed in chromic acid can be well replicated by widening process in $H_3$$PO_4$solution.

A Study of Nanoscale Structure of Anodic Porous Alumina film (다공성 알루미나 박막의 나노 스케일 구조에 관한 연구)

  • 정경한;신훈규;권영수
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.9
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    • pp.801-806
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    • 2003
  • In recent years, there has been large interest in the fabrication of the self organized nanoscale structures since not only their potential utilization in electronic, optoelectronic, and magnetic devices but also their fundamental interest such as uniformity and regularization. An attractive candidate of these materials is anodic porous alumina film(Al$_2$O$_3$) which is formed by the anodization of aluminum in an appropriate acid solution. In this study to fabricate the porous alumina film with very uniform and nearly parallel pores the anodization was carried out under constant voltage mode in 0.3M oxalic acid as an electrolyte. The hexagonally ordered arrays with a few $\mu\textrm{m}$ in size two-dimensional polycrystalline structure were obtained of which pore densities were 1.1${\times}$10$\^$10//$\textrm{cm}^2$.

Nano-porous $Al_2O_3$ used as a protecting layer of AC Plasma Display Panel

  • Park, Sung-Yun;Hong, Sang-Min;Shin, Bhum-Jae;Cho, Jin-Hoon;Kim, Seong-Su;Park, Sung-Jin;Lee, Kyu-Wang;Choi, Kyung-Cheol
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.359-361
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    • 2003
  • Nano-porous alumina was investigated as a protecting layer in an AC Plasma Display Panel. A 2 ${\mu}m$ thick nano-porous $Al_2O_3$ layer inserted with MgO was formed on the dielectric layer instead of the conventional 500 nm-thick MgO thin film. Both nano-porous $Al_2O_3$layer and inserted MgO were prepared by wet process. The luminance and luminous efficiency of 3-inch test panel adopting nano-porous $Al_2O_3$ was higher than that of the conventional PDP.

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Preparation of Nano Wire by Anodic Oxidation II. Production of Nano Wire Using Anodic Alumina Template (양극산화법에 의한 나노와이어 제조 II. 알루미나 템플레이트를 이용한 나노와이어 제조)

  • Jo, Su-Haeng;O, Han-Jun;Park, Chi-Seon;Jang, Jae-Myeong;Jo, Nam-Don;Ji, Chung-Su
    • Korean Journal of Materials Research
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    • v.12 no.1
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    • pp.89-93
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    • 2002
  • To investigate the effect of properties of pores in anodic alumina template(AAT) on the formation and characteristics of metal nano wires, Cu and Ni nano wires were manufactured using anodic alumina template formed in various electrolytes. The characteristics of prepared metal nano wires using AAT could be replicated from those of pores in AAT. The diameters of nano wires could be controlled by the widening process of anodic porous film in $H_3PO_4$ solution. The shape ratio of the nano wire was shown to be $170{\pm}30$ for Ni nano wire formed by AAT made in sulfuric acid.

Fabrication of Nano-mask Using Porous Alumina Membrane (다공성 알루미나 박막을 이용한 나노마스크 제작)

  • Jung, Kyung-Han;Ryu, Kil-Yong;Chang, Jeong-Soo;Kwon, Young-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.364-365
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    • 2006
  • One of the promising routes for producing highly ordered nanostructures is a template method using the porous alumina membrane (PAM). Because the PAM is mechanically, chemically, thermally stabile with highly ordered structure, many researchers have studied under various experimental conditions to fabricate nanostructures. We present the information on the fabrication of about 300 nm nano-mask which have important applications for various patterned nanostructures.

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Effect of 2nd Anodization on the Pore Formation for Alumina Nano Templates (알루미나 나노템플레이트의 기공형성에 미치는 2차 양극산화의 영향)

  • Cho, S.H.;Oh, H.J.;Joo, E.K.;Yoo, C.W.;Chi, C.S.
    • Korean Journal of Materials Research
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    • v.12 no.7
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    • pp.533-539
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    • 2002
  • Porous anodic aluminum oxide layer for nano templates was prepared in acidic solutions. In order to investigate effects of 2nd anodization on ordered formation behaviors of the porous oxide layers, electrochemical and microstructural studies were performed, primarily using TEM, FE- SEM, AFM, and Ultramicrotomy. The pore diameter of the anodic oxide layer increased approximately linearly with increasing voltages, and to the contrary, the pore density decreased. It was shown that 2nd anodizing on the cell base after dissolving 1st anodic oxide layer was remarkably effective for forming ordered array of the pores, comparing with the case for 1st anodization only. And for controlling the diameter of pores, widening method by chemical dissolution seemed more practical than by electrochemical methods.