• Title/Summary/Keyword: Nano- and microstructure

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Mechanical Properties and Microstructure of Nano Grain Nickel Alloy Deposit

  • Seo, Moo Hong;Kim, Jung Su;Kim, Seung Ho;Wyi, Jung Il;Hwang, Woon Suk;Jang, Si Sung;Jung, Hyun Kyu;Chun, Byung Sun
    • Corrosion Science and Technology
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    • v.2 no.4
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    • pp.197-201
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    • 2003
  • In this study, Ni-P layers were electroplated on the surface of stainless steel in order to investigate the effects of an additive and agitation on their mechanical properties and microstructure. The concentration of the additive in the plating solution increased, the pores formed in the layer decreased, while the residual stress developed in the layers during electroplating increased. Agitation of the solution during electroplating was observed to force to increase local pores in the layer, which lowers its tensile properties. Grain growth was suppressed due to very fine $Ni_3P$ precipitates formed at its grain boundaries during heat treatment at $343^{\circ}C$ for 1 hr in air.

Damping Capacity of Heat-Treated Mg-Nd Alloy (열처리한 Mg-Nd 합금의 진동감쇠능)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.26 no.4
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    • pp.185-190
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    • 2013
  • Influence of solution treatment (T4) and peak-aging (T6) on damping capacity was investigated in permanent-mold cast Mg-3%Nd alloy. In as-cast state, the microstructure was characterized by eutectic $Mg_{12}Nd$ intermetallic phase network in the intergranular region. T4 treatment resulted in a dissolution of the eutectic particles, but small amount of the particles still remained in the microstructure. After T6 treatment, nano-sized ${\beta}^{\prime}(Mg_{12}Nd)$ particles were precipitated within the matrix. T4 microstructure showed higher damping capacity than as-cast and T6 ones. In view of the microstructural features, this may well be associated with the dissolution of second-phase particles which play a role in pinning the dislocations acting as a damping source.

Study properties of soft subgrade soil stabilized by sewage sludge/lime and nano-SiO2

  • Lin, Deng-Fong;Luo, Huan-Lin;Chen, Chien-Ta;Cai, Ming-Du
    • Geomechanics and Engineering
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    • v.10 no.6
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    • pp.793-806
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    • 2016
  • The pozzolanic characteristics of a sludge incinerated into ash were determined in this study. Lime is commonly used as a stabilizer for the treatment of soils, whereas sewage sludge ash (SSA) is often applied with lime to improve soft subgrade soil. In this study, a cohesive soil categorized as A-4 (low-plasticity clay) by AASHTO classifications was mixed with SSA/lime with a 3:1 ratio. Nano-$SiO_2$ was also added to the soil. To identify changes in the workability, strength, permeability, and shear strength of the soft subgrade soil, basic soil tests were conducted, and the microstructure of the treated soil was analyzed. The results indicate that SSA/lime mixtures improve the properties of soft subgrade soil and transform the soil from "poor subgrade soil" to "good to excellent subgrade soil" with a CBR > 8. Additionally, the addition of 2% nano-$SiO_2$ increases the unconfined compressive strength of soft subgrade soil treated with SSA/lime mixture by approximately 17 kPa. However, the swelling of the treated soil increased by approximately 0.1% after the addition of nano-$SiO_2$ and lime. Thus, soil swelling should be considered before lime and nano-$SiO_2$ are applied to soft subgrade soil.

Microstructure Evaluation of Nano-thick Au-inserted Nickel Silicides (나노급 Au층 삽입 니켈실리사이드의 미세구조 변화)

  • Yoon, Ki-Jeong;Song, Oh-Sung
    • Korean Journal of Materials Research
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    • v.18 no.1
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    • pp.5-11
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    • 2008
  • Thermally evaporated 10 nm-Ni/1 nm-Au/(30 nm-poly)Si structures were fabricated in order to investigate the thermal stability of Au-inserted nickel silicide. The silicide samples underwent rapid thermal annealing at $300{\sim}1100^{\circ}C$ for 40 seconds. The sheet resistance was measured using a four-point probe. A scanning electron microscope and a transmission electron microscope were used to determine the cross-sectional structure and surface image. High-resolution X-ray diffraction and a scanning probe microscope were employed for the phase and surface roughness. According to sheet resistance and XRD analyses, nickel silicide with Au had no effect on widening the NiSi stabilization temperature region. Au-inserted nickel silicide on a single crystal silicon substrate showed nano-dots due to the preferred growth and a self-arranged agglomerate nano phase due to agglomeration. It was possible to tune the characteristic size of the agglomerate phase with silicidation temperatures. The nano-thick Au-insertion was shown to lead to self-arranged microstructures of nickel silicide.

Effect of Austempering on Microstructure and Mechanical Properties of High-Carbon Nano-Bainite Steels (고탄소 나노 베이나이트강의 미세조직과 기계적 특성에 미치는 오스템퍼링의 영향)

  • Lee, J.M.;Ko, S.W.;Ham, J.H.;Song, Y.B.;Kim, H.K.;Hwang, B.
    • Transactions of Materials Processing
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    • v.28 no.4
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    • pp.219-225
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    • 2019
  • This study deals with the effect of austempering temperature and time on the microstructures and mechanical properties of high-carbon nano-bainite steels. Although all the austempered specimens are mainly composed of bainite, martensite, and retained austenite, the specimens which are austempered at lower temperatures contain finer packets of bainite. As the duration for austempering increases, bainite packets are clearly seen due to larger amount of carbon atoms being redistributes into bainite and retained austenite during bainite transformation. As the austempering time increases, the hardness of the specimens gradually decreases as a result of lower martensite volume fraction, and later increases again due to the formation of nano-bainite structure. The Charpy impact test results indicate that the impact toughness of the austempered specimens can be improved if the formation of nano-bainite structure and the transformation induced plasticity effect of retained austenite are optimized at higher austempering temperature.

Nanostructured Materials and Nanotechnology : Overview

  • Muhammed, Mamoun;Tsakalakos, Thomas
    • Journal of the Korean Ceramic Society
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    • v.40 no.11
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    • pp.1027-1046
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    • 2003
  • Nanostructured materials can be engineered by the controlled assembly of several suitable nano-objects as the building blocks. While, materials properties are determined by their atomic and molecular constituents and structure, their functionalities emerge when the microstructure of these early ensembles is in the nanometer regime. The properties and functionalities of these ensembles may be different as their size grows from the nano-regime to the micron regime and bulk structures. Nanotechnology, offers a unique possibility to manipulate the properties through the fabrication of materials using the nano-objects as building blocks. Nanotechnology is therefore considered an enabling technology by which existing materials, virtually all man-made materials, can acquire novel properties and functionalities making them suitable for numerous novel applications varying from structural and functional to advanced biomedical in-vivo and in-vitro applications.

Fabrication and Properties of Nano-structured Ceramics

  • Ueno, Tomoyuki;Yoshimura, Masashi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.321-322
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    • 2006
  • Nano-structured ceramics, which consist of structural elements with nanometer-size crystallites, are expected to show various unusual properties. We developed the novel nano-structured ceramics which consists of $Si_3N_4$ and TiN and a self-lubricant material. The ceramics was fabricated by powder metallurgy process using mechano-chemical grinding process and short-time sintering process. Each grain size of matrix and the self-lubricant particle was under about 50 nm and a few namometer. It showed high wear resistance and low friction coefficient by controlling of microstructure.

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Hybrid Composite Nano-sized WC-Co Cemented Carbide

  • Park, Sun-Yong;Lee, Wan-Jae
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.640-641
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    • 2006
  • To improve the mechanical properties of WC-Co cemented carbides, the dual composite was studied. The compositions of granule and matrix were nano-sized WC-6 wt% Co(granule) and normal sized WC-20 wt% Co(matrix), respectively. The granules were grouped 50, 100 and $150\;{\mu}m$ and mixed with WC and Co powders as the volume fractions of granule to matrix were 50 to 50, 40 to 60 and 30 to 70. These compacts were sintered at $1380^{\circ}C$ for 10 minutes in vacuum. The microstructure, transverse rupture strength and wear resistance were investigated.

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