• 제목/요약/키워드: Nano particle

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수열흡착법을 이용한 은 점코팅된 구리 나노분말의 합성과 미세조직 (Microstructure and Synthesis of Ag Spot-coated Cu Nanopowders by Hydrothermal-attachment Method using Ag Colloid)

  • 김형철;한재길
    • 한국분말재료학회지
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    • 제18권6호
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    • pp.546-551
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    • 2011
  • Ag spot-coated Cu nanopowders were synthesized by a hydrothermal-attachment method (HA) using oleic acid capped Ag hydrosol. Cu nano powders were synthesized by pulsed wire exploding method using 0.4 mm in diameter of Cu wire (purity 99.9%). Synthesized Cu nano powders are seen with comparatively spherical shape having range in 50 nm to 150 nm in diameter. The oleic acid capped Ag hydrosol was synthesized by the precipitation-redispersion method. Oleic acid capped Ag nano particles showed the narrow size distribution and their particle size were less than 20 nm in diameter. In the case of nano Ag-spot coated Cu powders, nanosized Ag particles were adhered in the copper surface by HAA method. The components of C, O and Ag were distributed on the surface of copper powder.

Study on the Catalytic Properties of Copper Oxide Nanoparticles Synthesized by Levitational Gas Condensation (LGC) Method

  • Uhm, Y.R.;Lee, M.K.;Rhee, C.K.
    • 한국자기학회지
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    • 제17권2호
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    • pp.99-102
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    • 2007
  • The Cu oxide nano powders were synthesized by levitational gas condensation (LGC) method and their high heterogeneous catalytic effects of oxidation of 2,3,5-trimethyl-1,4-hydroquinone (TMHQ) and catalase activity were studied. The nano powders consist of mainly $Cu_2O$. The catalytic effect which was clarified by the oxidation of TMHQ and the activity of catalase, was found to depend on the amount of $Cu_2O$ phase and the particle size.

Nano Catalysts for Proton Exchange Membrane Fuel Cells

  • 김수길;황승준;임지은;유성종;이승철;임태훈
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2012년도 춘계학술발표대회
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    • pp.71.1-71.1
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    • 2012
  • Proton Exchange Membrane Fuel Cells (PEMFCs) have been of great interest particularly in the automobile industries because of their high energy density and low pollutant emission. However, some of the issues such as, the necessarily high contents of Pt catalysts and their slow kinetics of cathode oxygen reduction reaction remain as obstacles in the commercialization of the PEMFC. In this presentation, after brief explanation on basic principles of PEMFC and its application to FC vehicles, recent researches to improve the activity and durability of Pt-based nano catalysts toward oxygen reduction will be introduced. It covers size and shape control of Pt nano particle, binary and ternary Pt-M alloys, novel core-shell nano structures of Pt, and a little bit about non-Pt catalysts. Strategies and methodologies for design and synthesis of novel catalysts will also be included.

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나노 TiO2를 혼입한 시멘트 페이스트의 압축강도 연구 (The study of the compressive strength of cement pastes containing nano-TiO2)

  • 장광수;왕소용
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2018년도 춘계 학술논문 발표대회
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    • pp.214-215
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    • 2018
  • This paper has been researched that the earlier compressive strength of the cement pastes containing nano-TiO2 particle curing 1day, 3days and 7days. For the compressive strength measurements, all samples(dimensions 50×50×50mm) were prepared in accordance with ASTM C109. The compressive strength of the specimens with nano-TiO2 at the early age(1day, 3days and 7days) stage was lower than that of the reference group. Therefore, nano-TiO2 has little positive effect on the improvement of the compressive strength of cement pastes during early ages.

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噴霧熱分解 工程에 의한 인듐 酸化物 나노 粉末 製造 (Preparation of Nano-Sized Indium Oxide Powder by Spray Pyrolysis Process)

  • 유재근;박시현;손진군
    • 자원리싸이클링
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    • 제13권6호
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    • pp.16-25
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    • 2004
  • 인듐 성분을 포함하는 원료용액을 분무열분해 시켜서 평균 입자크기 100 nm 이하의 인듐 산화물 나노 분말을 제조하였으며, 용액의 농도, nozzle tip 크기 및 공기의 유입속도 변화에 따른 생성된 분말들의 특성 변화를 파악하였다. 본 연구는 폐 ITO로부터 나노 크기의 ITO 분말을 제조하기 위한 전 단계 연구로 수행되었다. 원료용액 내의 인듐 성분의 농도가 40 g/l로부터 350 g/l로 증가됨에 따라 생성된 분말의 평균 입자크기는 20~30 nm로부터 50~60 nm로 점점 증가하는 반면 입도분포는 더욱 불균일하게 나타나고 있었으며, XRD peak의 강도는 점점 증가하고 비표면적은 감소되었다. Nozzle tip의 크기가 1 mm로부터 5 mm로 증가함에 따라 분말들의 평균 입자크기는 40 nm 정도로부터 100 nm 정도까지 점점 증가하고 입도분포는 더욱 불균일하게 나타나고 있었으며, XRD peak 강도는 증가하는 반면 비표면적은 감소되었다. 반응로 내로 유입되는 공기의 압력이 0.1 kg/cm$^2$로부터 0.5 kg/cm$^2$로 증가되는 경우, 분말의 평균 입자크기는 90~100 nm로 현저한 변화를 나타내지 않았다. 반면 공기압력이 1 kg/cm$^2$ 및 3 kg/cm$^2$로 증가하는 경우에는 평균 입자크기가 50~60 nm 정도까지 감소하였으며, XRD peak 강도는 감소하고 비표면적은 증가되었다.

다양한 조건의 저압 공정 모니터링을 위한 입자 집속 장치 개발 (Development of particle focusing device to monitor various low pressure processes)

  • 김명준;김동빈;강상우;김태성
    • 한국입자에어로졸학회지
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    • 제13권2호
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    • pp.53-63
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    • 2017
  • As semiconductor process was highly integrated, particle contamination became a major issue. Because particle contamination is related with process yields directly, particles with a diameter larger than half pitch of gate should be controlled. PBMS (Particle beam mass spectrometry) is one of powerful nano particle measurement device. It can measure 5~500 nm particles at ~ 100 mtorr condition in real time by in-situ method. However its usage is restricted to research filed only, due to its big device volume and high price. Therefore aperture changeable aerodynamic lenses (ACALs) which can control particle focusing characteristics by changing its aperture diameter was proposed in this study. Unlike conventional aerodynamic lenses which changes particle focusing efficiency when operating condition is changed, ACALs can maintain particle focusing efficiency. Therefore, it can be used for a multi-monitoring system that connects one PBMS and several process chambers, which greatly improves the commercialization possibility of the PBMS. ACALs was designed based on Stokes number and evaluated by numerical method. Numerical analysis results showed aperture diameter changeable aerodynamic lenses can focus 5 to 100 nm standard particles at 0.1 to 10 torr upstream pressure.

DYE SENSITIZED SOLAR CELLS WITH HIGH PHOTO-ENERGY CONVERSION -CONTROLL OF NANO-PARTICLE SURFACES-

  • Hayase, Shuzi
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 춘계학술대회 논문집 전기기기 및 에너지변환시스템부문
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    • pp.52-56
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    • 2006
  • Some of factors affecting photo-conversion efficiency of dye sensitized solar cells (DSCs) are discussed in terms of $TiO_2$ electrodes. The first topic is on the surface modification of $TiO_2$ nano-particles, which is associated with electron traps on the surface of $TiO_2$ nano-particles. The surface is modified with dye molecules under pressurized $CO_2$ atmosphere to increase the surface coverage of $TiO_2$ nano-particles with dye molecules. This increases Jsc because of an increase in the amount of dye molecules and a decrease in the amount of trapping sites on $TiO_2$ nano-particles. In addition, the decrease in the amount of trap sites increases Voc because decreases in Voc are brought about by the recombination of $I_2$ molecules with electrons trapped on the $TiO_2$ surfaces. Selective staining for tandem cells is proposed. The second topic is on the contact between a $SnO_2$/F transparent conductive layer (TCL) and nano-particles. Polishing the TCL surfaces with silica nano-particles increases the contact, resulting in Jsc increases. The third topic is the fabrication of ion-paths in $TiO_2$ layers. Electro-spray coating of $TiO_2$ nano-particles onto TCL is shown to be effective for fabricating ion-paths in $TiO_2$ layers, which increases Jsc.

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Development of Multiple Beam Optical Tweezers

  • Lee Dong-Jin;LeBrun Thomas W.;Balijepalli Arvind;Gorman JasonJ.;Gagnon Cedric;Hong Dae-Hie;Chang Esthe rH.
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2005년도 춘계학술대회 논문집
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    • pp.1501-1506
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    • 2005
  • This paper presents the design of a multiple beam optical tweezers instrument used for manipulating micro/nano-sized components. The basic equations used in designing the optical tweezers are derived and the stable and time-sharing multiple beam optical tweezers are constructed with scanning mirrors. The laser beam passes through a series of optical components such as lenses, mirrors, and scanning mirrors, and overfills the entrance aperture of microscope objective, which gives a stable trap. By rotating the laser beam with the scanning mirror, the focal positions are translated in the specimen plane and multiple micro/nano-sized objects can be moved. The constructed optical tweezers is used to manipulate cells and liposomes simultaneously and to trap multiple nano-wires. The experiments prove that the developed optical tweezers can be a very versatile manipulation tool for studying gene therapy and nano device fabrication.

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표면처리된 나노알루미나가 첨가된 에폭시/멀티-알루미나 콤포지트의 교류절연파괴 특성 (The AC Insulation Breakdown Properties of Epoxy/Multi-Alumina Composites for Adding Surface Modified Nano Alumina)

  • 박재준
    • 전기학회논문지
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    • 제65권9호
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    • pp.1511-1517
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    • 2016
  • The aim of this study is to improve of properties for electrical AC insulation breakdown strength using epoxy/micro-nano alumina composites with adding glycerol diglycidyl ether (GDE:1,3,5g). This paper deals with the effects of GDE addition for epoxy/micro alumina contents (40,50,60wt%)+surface modified nano alumina(1_phr) composites. 14 kinds specimen were prepared with containing epoxy resins, epoxy micro composites and epoxy nano-micro alumina mixture composites. Average particle size of nano and micro alumina used were 30nm and $1{\sim}2{\mu}m$, respectively. The micro alumina used were alpha phase with Heterogeneous and nano alumina were gamma phase particles of spherical shape. The electrical AC insulation breakdown strength was evaluated by sphere to sphere electrode system and raising velocity 1kV/s. The AC breakdown strength decreased insulation properties of multi-composites according to increasing micro alumina and GDE addition contents.

나노입자를 적용한 냉장고 압축기용 오일의 윤활특성 평가 (Performance Evaluation of Nano-Lubricants at Refrigeration Oil)

  • 이광호;황유진;권래언;이재근;김석로;방선욱
    • 대한설비공학회:학술대회논문집
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    • 대한설비공학회 2008년도 하계학술발표대회 논문집
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    • pp.184-188
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    • 2008
  • It has been recognized that friction coefficient decreased with decreasing viscosity of oil in lubrication. In general, the more viscosity decreases, the more wear rate increases due to decrease load carrying capacity. It has been proposed that nano particles in oil decrease friction coefficient and wear rate. The purpose of this study is to apply oil of lower viscosity that mix with nano particles at the compressor used in a refrigerator to decrease friction coefficient keeping Load carrying capacity. Mineral oil of 8 cSt were used and mixed with nano particle. Friction coefficient was evaluated by a disk-on-disk tester. As a result, friction coefficient of nano oil decreased by 90% in comparison with raw oil. These results lead us to the conclusion that nano oil is new plan to raise efficiency of the compressor.

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